Composition and operation of hydrogen-selective amorphous alloy membranes

Catalytic membrane reactors, composed of a suitable hydrogen-selective membrane and water-gas-shift catalyst, can be used to produce a pure hydrogen stream from coal-derived syngas with high yield. The membrane must combine chemical and physical stability in the syngas environment at elevated temper...

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Published inJournal of membrane science Vol. 285; no. 1; pp. 30 - 55
Main Authors Dolan, M.D., Dave, N.C., Ilyushechkin, A.Y., Morpeth, L.D., McLennan, K.G.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.11.2006
Subjects
Amorphous alloy
Coal
Hydrogen separation
Metal membrane
Syngas
Thermal stability
Hydrogen separation
Amorphous alloy
Metal membrane
Thermal stability
Coal
Syngas
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Abstract Catalytic membrane reactors, composed of a suitable hydrogen-selective membrane and water-gas-shift catalyst, can be used to produce a pure hydrogen stream from coal-derived syngas with high yield. The membrane must combine chemical and physical stability in the syngas environment at elevated temperatures, with rapid hydrogen permeation and low cost. Amorphous alloy membranes based on a combination of early transition metals and late transition metals are an alternative to current palladium alloy membranes, offering hydrogen permeance and selectivity that is comparable to palladium alloys, plus the potential advantages of high resistance to crystalline hydride formation and lower cost. Amorphous alloy membranes have been reported that are capable of sustained operation at 400 °C, which makes them suitable for use in a CMR based on a metal-oxide catalyst. The development of membranes capable of sustained operation at 700 °C, and thus suitable for use with metallic catalysts, remains a significant technological hurdle, due to the tendency of amorphous alloys to crystallize after prolonged use at elevated temperatures, even below the measurable crystallization or glass transition temperatures. Here we provide a critical review of amorphous alloys, their manufacture and properties, and compare them with other types of membrane reactors. Economic and operational considerations are discussed in detail, which allows informed selection of amorphous alloy compositions for high-temperature separation of coal-derived syngas.
AbstractList Catalytic membrane reactors, composed of a suitable hydrogen-selective membrane and water-gas-shift catalyst, can be used to produce a pure hydrogen stream from coal-derived syngas with high yield. The membrane must combine chemical and physical stability in the syngas environment at elevated temperatures, with rapid hydrogen permeation and low cost. Amorphous alloy membranes based on a combination of early transition metals and late transition metals are an alternative to current palladium alloy membranes, offering hydrogen permeance and selectivity that is comparable to palladium alloys, plus the potential advantages of high resistance to crystalline hydride formation and lower cost. Amorphous alloy membranes have been reported that are capable of sustained operation at 400 °C, which makes them suitable for use in a CMR based on a metal-oxide catalyst. The development of membranes capable of sustained operation at 700 °C, and thus suitable for use with metallic catalysts, remains a significant technological hurdle, due to the tendency of amorphous alloys to crystallize after prolonged use at elevated temperatures, even below the measurable crystallization or glass transition temperatures. Here we provide a critical review of amorphous alloys, their manufacture and properties, and compare them with other types of membrane reactors. Economic and operational considerations are discussed in detail, which allows informed selection of amorphous alloy compositions for high-temperature separation of coal-derived syngas.
Author McLennan, K.G.
Dolan, M.D.
Morpeth, L.D.
Dave, N.C.
Ilyushechkin, A.Y.
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ID FETCH-LOGICAL-c409t-57e0defc058e896d24d0dbcd16252b25faba9389c7db56d699723efbbd2e5f8a3
IEDL.DBID AIKHN
ISSN 0376-7388
IngestDate Thu Sep 26 15:53:01 EDT 2024
Fri Feb 23 02:33:58 EST 2024
IsPeerReviewed true
IsScholarly true
Issue 1
Keywords Hydrogen separation
Amorphous alloy
Metal membrane
Thermal stability
Coal
Syngas
Language English
LinkModel DirectLink
MergedId FETCHMERGED-LOGICAL-c409t-57e0defc058e896d24d0dbcd16252b25faba9389c7db56d699723efbbd2e5f8a3
PageCount 26
ParticipantIDs crossref_primary_10_1016_j_memsci_2006_09_014
elsevier_sciencedirect_doi_10_1016_j_memsci_2006_09_014
PublicationCentury 2000
PublicationDate 2006-11-15
PublicationDateYYYYMMDD 2006-11-15
PublicationDate_xml – month: 11
  year: 2006
  text: 2006-11-15
  day: 15
PublicationDecade 2000
PublicationTitle Journal of membrane science
PublicationYear 2006
Publisher Elsevier B.V
Publisher_xml – name: Elsevier B.V
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Snippet Catalytic membrane reactors, composed of a suitable hydrogen-selective membrane and water-gas-shift catalyst, can be used to produce a pure hydrogen stream...
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SubjectTerms Amorphous alloy
Coal
Hydrogen separation
Metal membrane
Syngas
Thermal stability
Title Composition and operation of hydrogen-selective amorphous alloy membranes
URI https://dx.doi.org/10.1016/j.memsci.2006.09.014
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