Microstructure and strengthening mechanisms in an FCC structured single-phase nanocrystalline Co25Ni25Fe25Al7.5Cu17.5 high-entropy alloy
We report on a study of the design, phase formation, microstructure, mechanical behavior and strengthening mechanisms of a novel single-phase Co25Ni25Fe25Al7.5Cu17.5 (at.%) high-entropy alloy (HEA). In this investigation, a bulk nanocrystalline (nc) Co25Ni25Fe25Al7.5Cu17.5 HEA with the face-centered...
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| Published in | Acta materialia Vol. 107; pp. 59 - 71 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.04.2016
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| Subjects | |
| Online Access | Get full text |
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| Abstract | We report on a study of the design, phase formation, microstructure, mechanical behavior and strengthening mechanisms of a novel single-phase Co25Ni25Fe25Al7.5Cu17.5 (at.%) high-entropy alloy (HEA). In this investigation, a bulk nanocrystalline (nc) Co25Ni25Fe25Al7.5Cu17.5 HEA with the face-centered cubic (FCC) crystal structure was fabricated by mechanical alloying (MA) followed by consolidation via spark plasma sintering (SPS). The X-ray diffraction (XRD) and transmission electron microscopy (TEM) results revealed that a single FCC solid-solution phase with an average grain diameter of 24 nm was produced following MA. Following SPS, bulk samples exhibiting a bimodal microstructure with both nanoscale grains and ultra-fine grains (UFGs) and with an average grain diameter of 95 nm were obtained, possessing a single FCC solid-solution phase identical to that in the milled powders. The single-phase feature of the Co25Ni25Fe25Al7.5Cu17.5 HEA principally resulted from remarkably high mutual solubility in most binary atom-pairs of the constituent elements, which appears to correspond to a high entropy of mixing. Approximately 5 vol.% of nanoscale twins were observed in the bulk nc samples. The bulk nc Co25Ni25Fe25Al7.5Cu17.5 HEA exhibits a compressive yield strength of 1795 MPa with a hardness of 454 Hv, which is dramatically higher than the yield strength of most previously reported FCC structured HEAs (∼130–700 MPa). Compared to those of the bulk coarse-grained (CG) Co25Ni25Fe25Al7.5Cu17.5 HEA fabricated by arc-melting, the yield strength and Vickers hardness values of the bulk nc samples increased by 834.9% and 251.9%, respectively. Quantitative calculations of the respective contributions from each strengthening mechanism demonstrate that grain boundary strengthening and dislocation strengthening are principally responsible for the measured ultra-high strength of the bulk nc Co25Ni25Fe25Al7.5Cu17.5 HEA.
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| AbstractList | We report on a study of the design, phase formation, microstructure, mechanical behavior and strengthening mechanisms of a novel single-phase Co25Ni25Fe25Al7.5Cu17.5 (at.%) high-entropy alloy (HEA). In this investigation, a bulk nanocrystalline (nc) Co25Ni25Fe25Al7.5Cu17.5 HEA with the face-centered cubic (FCC) crystal structure was fabricated by mechanical alloying (MA) followed by consolidation via spark plasma sintering (SPS). The X-ray diffraction (XRD) and transmission electron microscopy (TEM) results revealed that a single FCC solid-solution phase with an average grain diameter of 24 nm was produced following MA. Following SPS, bulk samples exhibiting a bimodal microstructure with both nanoscale grains and ultra-fine grains (UFGs) and with an average grain diameter of 95 nm were obtained, possessing a single FCC solid-solution phase identical to that in the milled powders. The single-phase feature of the Co25Ni25Fe25Al7.5Cu17.5 HEA principally resulted from remarkably high mutual solubility in most binary atom-pairs of the constituent elements, which appears to correspond to a high entropy of mixing. Approximately 5 vol.% of nanoscale twins were observed in the bulk nc samples. The bulk nc Co25Ni25Fe25Al7.5Cu17.5 HEA exhibits a compressive yield strength of 1795 MPa with a hardness of 454 Hv, which is dramatically higher than the yield strength of most previously reported FCC structured HEAs (130-700 MPa). Compared to those of the bulk coarse-grained (CG) Co25Ni25Fe25Al7.5Cu17.5 HEA fabricated by arc-melting, the yield strength and Vickers hardness values of the bulk nc samples increased by 834.9% and 251.9%, respectively. Quantitative calculations of the respective contributions from each strengthening mechanism demonstrate that grain boundary strengthening and dislocation strengthening are principally responsible for the measured ultra-high strength of the bulk nc Co25Ni25Fe25Al7.5Cu17.5 HEA. We report on a study of the design, phase formation, microstructure, mechanical behavior and strengthening mechanisms of a novel single-phase Co25Ni25Fe25Al7.5Cu17.5 (at.%) high-entropy alloy (HEA). In this investigation, a bulk nanocrystalline (nc) Co25Ni25Fe25Al7.5Cu17.5 HEA with the face-centered cubic (FCC) crystal structure was fabricated by mechanical alloying (MA) followed by consolidation via spark plasma sintering (SPS). The X-ray diffraction (XRD) and transmission electron microscopy (TEM) results revealed that a single FCC solid-solution phase with an average grain diameter of 24 nm was produced following MA. Following SPS, bulk samples exhibiting a bimodal microstructure with both nanoscale grains and ultra-fine grains (UFGs) and with an average grain diameter of 95 nm were obtained, possessing a single FCC solid-solution phase identical to that in the milled powders. The single-phase feature of the Co25Ni25Fe25Al7.5Cu17.5 HEA principally resulted from remarkably high mutual solubility in most binary atom-pairs of the constituent elements, which appears to correspond to a high entropy of mixing. Approximately 5 vol.% of nanoscale twins were observed in the bulk nc samples. The bulk nc Co25Ni25Fe25Al7.5Cu17.5 HEA exhibits a compressive yield strength of 1795 MPa with a hardness of 454 Hv, which is dramatically higher than the yield strength of most previously reported FCC structured HEAs (∼130–700 MPa). Compared to those of the bulk coarse-grained (CG) Co25Ni25Fe25Al7.5Cu17.5 HEA fabricated by arc-melting, the yield strength and Vickers hardness values of the bulk nc samples increased by 834.9% and 251.9%, respectively. Quantitative calculations of the respective contributions from each strengthening mechanism demonstrate that grain boundary strengthening and dislocation strengthening are principally responsible for the measured ultra-high strength of the bulk nc Co25Ni25Fe25Al7.5Cu17.5 HEA. [Display omitted] |
| Author | Chen, Weiping Zhang, Dalong Wen, Haiming Fu, Zhiqiang Chen, Zhen Zhou, Yizhang Zheng, Baolong Lavernia, Enrique J. |
| Author_xml | – sequence: 1 givenname: Zhiqiang surname: Fu fullname: Fu, Zhiqiang email: fzqfu@ucdavis.edu organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong, 510640, China – sequence: 2 givenname: Weiping surname: Chen fullname: Chen, Weiping organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong, 510640, China – sequence: 3 givenname: Haiming surname: Wen fullname: Wen, Haiming email: wenhaim@isu.edu organization: Department of Nuclear Engineering and Health Physics, Idaho State University, Idaho Falls, ID, 83402, USA – sequence: 4 givenname: Dalong surname: Zhang fullname: Zhang, Dalong organization: Department of Chemical Engineering and Materials Science, University of California, Davis, Davis, CA, 95616, USA – sequence: 5 givenname: Zhen surname: Chen fullname: Chen, Zhen organization: School of Mechanical and Automotive Engineering, South China University of Technology, Guangzhou, Guangdong, 510640, China – sequence: 6 givenname: Baolong surname: Zheng fullname: Zheng, Baolong organization: Department of Chemical Engineering and Materials Science, University of California, Davis, Davis, CA, 95616, USA – sequence: 7 givenname: Yizhang surname: Zhou fullname: Zhou, Yizhang organization: Department of Chemical Engineering and Materials Science, University of California, Davis, Davis, CA, 95616, USA – sequence: 8 givenname: Enrique J. surname: Lavernia fullname: Lavernia, Enrique J. email: lavernia@uci.edu organization: Department of Chemical Engineering and Materials Science, University of California, Davis, Davis, CA, 95616, USA |
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| SubjectTerms | Bulk sampling Face centered cubic lattice Grains High-entropy alloys Microstructure Nanocrystalline Nanostructure Single-phase Spark plasma sintering Strengthening Strengthening mechanism Transmission electron microscopy |
| Title | Microstructure and strengthening mechanisms in an FCC structured single-phase nanocrystalline Co25Ni25Fe25Al7.5Cu17.5 high-entropy alloy |
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