Cyclic voltammetry electrodeposition of well-dispersed Pd nanoparticles on carbon paper as a flow-through anode for microfluidic direct formate fuel cells
The preparation of low-loading and high-performance Pd-based electrodes is required for direct formate fuel cells. In this study, cyclic voltammetry electrodeposition is used to electrodeposit Pd nanoparticles on carbon paper (Pd/CP) and achieve excellent activity and promising stability toward the...
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| Published in | Nanoscale Vol. 12; no. 39; pp. 227 - 2278 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cambridge
Royal Society of Chemistry
15.10.2020
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The preparation of low-loading and high-performance Pd-based electrodes is required for direct formate fuel cells. In this study, cyclic voltammetry electrodeposition is used to electrodeposit Pd nanoparticles on carbon paper (Pd/CP) and achieve excellent activity and promising stability toward the formate oxidation reaction (FOR). The prepared electrode shows a thin layer of hemispherical and well-dispersed Pd nanoparticles on the fibers of the carbon paper. The open structure and uniform catalyst distribution make the Pd/CP electrode show 2.56-fold higher active area and stability in the FOR as compared with those of commercial Pd/C catalysts. An air-breathing microfluidic direct formate fuel cell (μDFFC) with a Pd/CP electrode used as a flow-through anode is constructed to further assess electrode performance. The Pd/CP electrode with low Pd loading, 0.105 mg cm
−2
, delivers a peak power density and limiting current density of 46.6 mW cm
−2
(443.8 mW mg
−1
Pd
) and 288.4 mA cm
−2
, respectively. The performance of the μDFFC is superior to those of most others reported in the literature, further boosting the commercialization of this direct formate fuel cell to power next-generation portable electronics.
Cyclic voltammetry electrodeposition of palladium nanoparticles on carbon paper results in high catalytic performance, catalyst utilization and stability for their use in microfluidic direct formate fuel cells. |
|---|---|
| AbstractList | The preparation of low-loading and high-performance Pd-based electrodes is required for direct formate fuel cells. In this study, cyclic voltammetry electrodeposition is used to electrodeposit Pd nanoparticles on carbon paper (Pd/CP) and achieve excellent activity and promising stability toward the formate oxidation reaction (FOR). The prepared electrode shows a thin layer of hemispherical and well-dispersed Pd nanoparticles on the fibers of the carbon paper. The open structure and uniform catalyst distribution make the Pd/CP electrode show 2.56-fold higher active area and stability in the FOR as compared with those of commercial Pd/C catalysts. An air-breathing microfluidic direct formate fuel cell (μDFFC) with a Pd/CP electrode used as a flow-through anode is constructed to further assess electrode performance. The Pd/CP electrode with low Pd loading, 0.105 mg cm
−2
, delivers a peak power density and limiting current density of 46.6 mW cm
−2
(443.8 mW mg
−1
Pd
) and 288.4 mA cm
−2
, respectively. The performance of the μDFFC is superior to those of most others reported in the literature, further boosting the commercialization of this direct formate fuel cell to power next-generation portable electronics.
Cyclic voltammetry electrodeposition of palladium nanoparticles on carbon paper results in high catalytic performance, catalyst utilization and stability for their use in microfluidic direct formate fuel cells. The preparation of low-loading and high-performance Pd-based electrodes is required for direct formate fuel cells. In this study, cyclic voltammetry electrodeposition is used to electrodeposit Pd nanoparticles on carbon paper (Pd/CP) and achieve excellent activity and promising stability toward the formate oxidation reaction (FOR). The prepared electrode shows a thin layer of hemispherical and well-dispersed Pd nanoparticles on the fibers of the carbon paper. The open structure and uniform catalyst distribution make the Pd/CP electrode show 2.56-fold higher active area and stability in the FOR as compared with those of commercial Pd/C catalysts. An air-breathing microfluidic direct formate fuel cell (μDFFC) with a Pd/CP electrode used as a flow-through anode is constructed to further assess electrode performance. The Pd/CP electrode with low Pd loading, 0.105 mg cm-2, delivers a peak power density and limiting current density of 46.6 mW cm-2 (443.8 mW mg-1Pd) and 288.4 mA cm-2, respectively. The performance of the μDFFC is superior to those of most others reported in the literature, further boosting the commercialization of this direct formate fuel cell to power next-generation portable electronics.The preparation of low-loading and high-performance Pd-based electrodes is required for direct formate fuel cells. In this study, cyclic voltammetry electrodeposition is used to electrodeposit Pd nanoparticles on carbon paper (Pd/CP) and achieve excellent activity and promising stability toward the formate oxidation reaction (FOR). The prepared electrode shows a thin layer of hemispherical and well-dispersed Pd nanoparticles on the fibers of the carbon paper. The open structure and uniform catalyst distribution make the Pd/CP electrode show 2.56-fold higher active area and stability in the FOR as compared with those of commercial Pd/C catalysts. An air-breathing microfluidic direct formate fuel cell (μDFFC) with a Pd/CP electrode used as a flow-through anode is constructed to further assess electrode performance. The Pd/CP electrode with low Pd loading, 0.105 mg cm-2, delivers a peak power density and limiting current density of 46.6 mW cm-2 (443.8 mW mg-1Pd) and 288.4 mA cm-2, respectively. The performance of the μDFFC is superior to those of most others reported in the literature, further boosting the commercialization of this direct formate fuel cell to power next-generation portable electronics. The preparation of low-loading and high-performance Pd-based electrodes is required for direct formate fuel cells. In this study, cyclic voltammetry electrodeposition is used to electrodeposit Pd nanoparticles on carbon paper (Pd/CP) and achieve excellent activity and promising stability toward the formate oxidation reaction (FOR). The prepared electrode shows a thin layer of hemispherical and well-dispersed Pd nanoparticles on the fibers of the carbon paper. The open structure and uniform catalyst distribution make the Pd/CP electrode show 2.56-fold higher active area and stability in the FOR as compared with those of commercial Pd/C catalysts. An air-breathing microfluidic direct formate fuel cell (μDFFC) with a Pd/CP electrode used as a flow-through anode is constructed to further assess electrode performance. The Pd/CP electrode with low Pd loading, 0.105 mg cm −2 , delivers a peak power density and limiting current density of 46.6 mW cm −2 (443.8 mW mg −1 Pd ) and 288.4 mA cm −2 , respectively. The performance of the μDFFC is superior to those of most others reported in the literature, further boosting the commercialization of this direct formate fuel cell to power next-generation portable electronics. The preparation of low-loading and high-performance Pd-based electrodes is required for direct formate fuel cells. In this study, cyclic voltammetry electrodeposition is used to electrodeposit Pd nanoparticles on carbon paper (Pd/CP) and achieve excellent activity and promising stability toward the formate oxidation reaction (FOR). The prepared electrode shows a thin layer of hemispherical and well-dispersed Pd nanoparticles on the fibers of the carbon paper. The open structure and uniform catalyst distribution make the Pd/CP electrode show 2.56-fold higher active area and stability in the FOR as compared with those of commercial Pd/C catalysts. An air-breathing microfluidic direct formate fuel cell (μDFFC) with a Pd/CP electrode used as a flow-through anode is constructed to further assess electrode performance. The Pd/CP electrode with low Pd loading, 0.105 mg cm−2, delivers a peak power density and limiting current density of 46.6 mW cm−2 (443.8 mW mg−1Pd) and 288.4 mA cm−2, respectively. The performance of the μDFFC is superior to those of most others reported in the literature, further boosting the commercialization of this direct formate fuel cell to power next-generation portable electronics. |
| Author | Chen, Rong Ye, Ding-Ding Zhu, Xun Zhang, Tong Liao, Qiang Zhou, Yuan |
| AuthorAffiliation | Chongqing University Ministry of Education Institute of Engineering Thermophysics School of Energy and Power Engineering Key Laboratory of Low-grade Energy Utilization Technologies and Systems (Chongqing University) |
| AuthorAffiliation_xml | – name: Institute of Engineering Thermophysics – name: Ministry of Education – name: Chongqing University – name: Key Laboratory of Low-grade Energy Utilization Technologies and Systems (Chongqing University) – name: School of Energy and Power Engineering |
| Author_xml | – sequence: 1 givenname: Tong surname: Zhang fullname: Zhang, Tong – sequence: 2 givenname: Xun surname: Zhu fullname: Zhu, Xun – sequence: 3 givenname: Ding-Ding surname: Ye fullname: Ye, Ding-Ding – sequence: 4 givenname: Rong surname: Chen fullname: Chen, Rong – sequence: 5 givenname: Yuan surname: Zhou fullname: Zhou, Yuan – sequence: 6 givenname: Qiang surname: Liao fullname: Liao, Qiang |
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| SubjectTerms | Anodes Carbon Catalysts Commercialization Dispersion Electrodeposition Electrodes Fuel cells Microfluidics Nanoparticles Oxidation Stability Voltammetry |
| Title | Cyclic voltammetry electrodeposition of well-dispersed Pd nanoparticles on carbon paper as a flow-through anode for microfluidic direct formate fuel cells |
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