Removal of atrazine and its by-products from water using electrochemical advanced oxidation processes
Atrazine (ATZ) is one of the most common pesticides detected in surface water in Quebec (Canada). The present study was mainly focused on the degradation of ATZ and its by-products using electrochemical advanced oxidation processes such as photo-electro-Fenton (PEF), electro-Fenton (EF) and anodic-o...
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Published in | Water research (Oxford) Vol. 125; pp. 91 - 103 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
England
Elsevier Ltd
15.11.2017
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Abstract | Atrazine (ATZ) is one of the most common pesticides detected in surface water in Quebec (Canada). The present study was mainly focused on the degradation of ATZ and its by-products using electrochemical advanced oxidation processes such as photo-electro-Fenton (PEF), electro-Fenton (EF) and anodic-oxidation with simultaneous H2O2 formation (AO - H2O2). The comparison of these processes showed that PEF process was found to be the most effective process in removing ATZ and its by-products from both synthetic solution (ATZ0 = 100 μg L−1) and real agricultural surface water enriched with ATZ (ATZ0 = 10 μg L−1). Different operating parameters, including wavelength of the light, pH, current density and the presence of natural organic matter (humic acids) were investigated for PEF process using boron-doped diamond (BDD) anode and graphite cathode. The current density and the wavelength of the light were the most important parameters in the ATZ degradation efficiency. The best operating conditions were recorded for the synthetic samples at a current density of 18.2 mA cm−2, a pH of 3.0 and treatment time of 45 min. Results showed that atrazine-desethyl-desisopropyl (DEDIA) was the most important by-product recorded. More than 99% of ATZ oxidation was recorded after 15 min of treatment and all the concentrations of major by-products were less than the limit of detection after 45 min of treatment. The PEF process was also tested for real surface water contaminated by ATZ: i) with and without addition of iron; ii) without pH adjustment (pH ∼ 6.7) and with pH adjustment (pH ∼ 3.1). In spite of the presence of radical scavenger and iron complexation the PEF process was more effective to remove ATZ from real surface water when the pH value was adjusted near to 3.0. The ATZ removal was 96.0% with 0.01 mM of iron (kapp = 0.13 min−1) and 100% with 0.1 mM of iron (kapp = 0.17 min−1).
[Display omitted]
•PEF process is a feasible technology for the treatment of water contaminated by ATZ.•More than 99% of ATZ oxidation was recorded after 15 min of treatment in synthetic effluent.•Atrazine-desethyl-desisopropyl (DEDIA) was the most important by-product recorded.•100% of ATZ was removed from surface water in spite of the presence of radical scavengers. |
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AbstractList | Atrazine (ATZ) is one of the most common pesticides detected in surface water in Quebec (Canada). The present study was mainly focused on the degradation of ATZ and its by-products using electrochemical advanced oxidation processes such as photo-electro-Fenton (PEF), electro-Fenton (EF) and anodic-oxidation with simultaneous H
O
formation (AO - H
O
). The comparison of these processes showed that PEF process was found to be the most effective process in removing ATZ and its by-products from both synthetic solution (ATZ
= 100 μg L
) and real agricultural surface water enriched with ATZ (ATZ
= 10 μg L
). Different operating parameters, including wavelength of the light, pH, current density and the presence of natural organic matter (humic acids) were investigated for PEF process using boron-doped diamond (BDD) anode and graphite cathode. The current density and the wavelength of the light were the most important parameters in the ATZ degradation efficiency. The best operating conditions were recorded for the synthetic samples at a current density of 18.2 mA cm
, a pH of 3.0 and treatment time of 45 min. Results showed that atrazine-desethyl-desisopropyl (DEDIA) was the most important by-product recorded. More than 99% of ATZ oxidation was recorded after 15 min of treatment and all the concentrations of major by-products were less than the limit of detection after 45 min of treatment. The PEF process was also tested for real surface water contaminated by ATZ: i) with and without addition of iron; ii) without pH adjustment (pH ∼ 6.7) and with pH adjustment (pH ∼ 3.1). In spite of the presence of radical scavenger and iron complexation the PEF process was more effective to remove ATZ from real surface water when the pH value was adjusted near to 3.0. The ATZ removal was 96.0% with 0.01 mM of iron (k
= 0.13 min
) and 100% with 0.1 mM of iron (k
= 0.17 min
). Atrazine (ATZ) is one of the most common pesticides detected in surface water in Quebec (Canada). The present study was mainly focused on the degradation of ATZ and its by-products using electrochemical advanced oxidation processes such as photo-electro-Fenton (PEF), electro-Fenton (EF) and anodic-oxidation with simultaneous H2O2 formation (AO - H2O2). The comparison of these processes showed that PEF process was found to be the most effective process in removing ATZ and its by-products from both synthetic solution (ATZ0 = 100 μg L-1) and real agricultural surface water enriched with ATZ (ATZ0 = 10 μg L-1). Different operating parameters, including wavelength of the light, pH, current density and the presence of natural organic matter (humic acids) were investigated for PEF process using boron-doped diamond (BDD) anode and graphite cathode. The current density and the wavelength of the light were the most important parameters in the ATZ degradation efficiency. The best operating conditions were recorded for the synthetic samples at a current density of 18.2 mA cm-2, a pH of 3.0 and treatment time of 45 min. Results showed that atrazine-desethyl-desisopropyl (DEDIA) was the most important by-product recorded. More than 99% of ATZ oxidation was recorded after 15 min of treatment and all the concentrations of major by-products were less than the limit of detection after 45 min of treatment. The PEF process was also tested for real surface water contaminated by ATZ: i) with and without addition of iron; ii) without pH adjustment (pH ∼ 6.7) and with pH adjustment (pH ∼ 3.1). In spite of the presence of radical scavenger and iron complexation the PEF process was more effective to remove ATZ from real surface water when the pH value was adjusted near to 3.0. The ATZ removal was 96.0% with 0.01 mM of iron (kapp = 0.13 min-1) and 100% with 0.1 mM of iron (kapp = 0.17 min-1). Atrazine (ATZ) is one of the most common pesticides detected in surface water in Quebec (Canada). The present study was mainly focused on the degradation of ATZ and its by-products using electrochemical advanced oxidation processes such as photo-electro-Fenton (PEF), electro-Fenton (EF) and anodic-oxidation with simultaneous H2O2 formation (AO - H2O2). The comparison of these processes showed that PEF process was found to be the most effective process in removing ATZ and its by-products from both synthetic solution (ATZ0 = 100 μg L−1) and real agricultural surface water enriched with ATZ (ATZ0 = 10 μg L−1). Different operating parameters, including wavelength of the light, pH, current density and the presence of natural organic matter (humic acids) were investigated for PEF process using boron-doped diamond (BDD) anode and graphite cathode. The current density and the wavelength of the light were the most important parameters in the ATZ degradation efficiency. The best operating conditions were recorded for the synthetic samples at a current density of 18.2 mA cm−2, a pH of 3.0 and treatment time of 45 min. Results showed that atrazine-desethyl-desisopropyl (DEDIA) was the most important by-product recorded. More than 99% of ATZ oxidation was recorded after 15 min of treatment and all the concentrations of major by-products were less than the limit of detection after 45 min of treatment. The PEF process was also tested for real surface water contaminated by ATZ: i) with and without addition of iron; ii) without pH adjustment (pH ∼ 6.7) and with pH adjustment (pH ∼ 3.1). In spite of the presence of radical scavenger and iron complexation the PEF process was more effective to remove ATZ from real surface water when the pH value was adjusted near to 3.0. The ATZ removal was 96.0% with 0.01 mM of iron (kapp = 0.13 min−1) and 100% with 0.1 mM of iron (kapp = 0.17 min−1). [Display omitted] •PEF process is a feasible technology for the treatment of water contaminated by ATZ.•More than 99% of ATZ oxidation was recorded after 15 min of treatment in synthetic effluent.•Atrazine-desethyl-desisopropyl (DEDIA) was the most important by-product recorded.•100% of ATZ was removed from surface water in spite of the presence of radical scavengers. |
Author | Dirany, Ahmad Komtchou, Simon Lafrance, Pierre Robert, Didier Drogui, Patrick |
Author_xml | – sequence: 1 givenname: Simon surname: Komtchou fullname: Komtchou, Simon email: simon.komtchou@ete.inrs.ca organization: Institut National de la Recherche Scientifique (INRS-Centre Eau, Terre et Environnement), Université du Québec, 490 rue de la Couronne, Québec, QC, G1K 9A9, Canada – sequence: 2 givenname: Ahmad surname: Dirany fullname: Dirany, Ahmad email: ahmad.dirany@ete.inrs.ca organization: Institut National de la Recherche Scientifique (INRS-Centre Eau, Terre et Environnement), Université du Québec, 490 rue de la Couronne, Québec, QC, G1K 9A9, Canada – sequence: 3 givenname: Patrick surname: Drogui fullname: Drogui, Patrick email: patrick.drogui@ete.inrs.ca organization: Institut National de la Recherche Scientifique (INRS-Centre Eau, Terre et Environnement), Université du Québec, 490 rue de la Couronne, Québec, QC, G1K 9A9, Canada – sequence: 4 givenname: Didier surname: Robert fullname: Robert, Didier email: d.robert@unistra.fr organization: Institut de Chimie et Procédés pour l'Énergie, l'Environnement et la Santé (ICPEES), CNRS, Université de Strasbourg, rue Victor Demange, 57500, Saint-Avold, France – sequence: 5 givenname: Pierre surname: Lafrance fullname: Lafrance, Pierre email: pierre.lafrance@ete.inrs.ca organization: Institut National de la Recherche Scientifique (INRS-Centre Eau, Terre et Environnement), Université du Québec, 490 rue de la Couronne, Québec, QC, G1K 9A9, Canada |
BackLink | https://www.ncbi.nlm.nih.gov/pubmed/28837868$$D View this record in MEDLINE/PubMed |
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Keywords | Degradation Hydroxyl radicals Energy consumption Photoelectro-Fenton Atrazine |
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Snippet | Atrazine (ATZ) is one of the most common pesticides detected in surface water in Quebec (Canada). The present study was mainly focused on the degradation of... |
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SubjectTerms | Atrazine Atrazine - chemistry Atrazine - isolation & purification Boron Degradation Electrochemical Techniques - instrumentation Electrochemical Techniques - methods Electrodes Energy consumption Graphite - chemistry Hydrogen Peroxide - chemistry Hydroxyl radicals Iron - chemistry Oxidation-Reduction Pesticide Residues - chemistry Pesticide Residues - isolation & purification Photoelectro-Fenton Quebec Water Pollutants, Chemical - chemistry Water Pollutants, Chemical - isolation & purification Water Purification - instrumentation Water Purification - methods |
Title | Removal of atrazine and its by-products from water using electrochemical advanced oxidation processes |
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