Fouling of inorganic membranes during whey ultrafiltration: Analytical methodology
Ultrafiltration of various types of whey was carried out through an inorganic membrane (M 4 Carbosep, 20000 Da cut-off). Fouling was evaluated as a hydraulic resistance ( R f) and analysed with infrared (IR) and X -ray photoelectron ( XPS) spectroscopies, giving complementary results. Spectroscopic...
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| Published in | Journal of membrane science Vol. 51; no. 3; pp. 293 - 307 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
01.08.1990
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Ultrafiltration of various types of whey was carried out through an inorganic membrane (M
4 Carbosep, 20000 Da cut-off). Fouling was evaluated as a hydraulic resistance (
R
f) and analysed with infrared (IR) and X -ray photoelectron ( XPS) spectroscopies, giving complementary results. Spectroscopic data are in a very good agreement with UF flux variations and
R
f values: the higher the transmembrane pressure or the whey protein content, the higher the fouling protein content. Proteins are found in the bulk of the membrane as well as on its surface, their concentration being higher in the latter case, whereas the phosphate/protein ratio lies often in the range 25–45% whatever the whey type or the operating conditions. Qualitatively, phosphate organization involves at least adsorbed hydrogen-phosphates and apatite structures resulting from several interactions between phosphate, protein, calcium and membrane. Only when the pH is increased up to 6.9 does PO
4 organization typically reach the apatite lattice. Its level is highest in the bulk of the membrane (4.1% relative to ZrO
2), representing nearly 85% of the protein content. |
|---|---|
| AbstractList | Ultrafiltration of various types of whey was carried out through an inorganic membrane (M
4 Carbosep, 20000 Da cut-off). Fouling was evaluated as a hydraulic resistance (
R
f) and analysed with infrared (IR) and X -ray photoelectron ( XPS) spectroscopies, giving complementary results. Spectroscopic data are in a very good agreement with UF flux variations and
R
f values: the higher the transmembrane pressure or the whey protein content, the higher the fouling protein content. Proteins are found in the bulk of the membrane as well as on its surface, their concentration being higher in the latter case, whereas the phosphate/protein ratio lies often in the range 25–45% whatever the whey type or the operating conditions. Qualitatively, phosphate organization involves at least adsorbed hydrogen-phosphates and apatite structures resulting from several interactions between phosphate, protein, calcium and membrane. Only when the pH is increased up to 6.9 does PO
4 organization typically reach the apatite lattice. Its level is highest in the bulk of the membrane (4.1% relative to ZrO
2), representing nearly 85% of the protein content. |
| Author | Michel, F. Labbe, J.P. Daufin, G. Quemerais, A. |
| Author_xml | – sequence: 1 givenname: J.P. surname: Labbe fullname: Labbe, J.P. organization: Ecole Nationale Supérieure de Chimie de Paris, 11, rue P. et M. Curie, 75231 Paris Cédex 05 France – sequence: 2 givenname: A. surname: Quemerais fullname: Quemerais, A. organization: Université de Rennes 1, Avenue du Général Leclerc, Campus de Beaulieu, 35042 Rennes Cédex France – sequence: 3 givenname: F. surname: Michel fullname: Michel, F. – sequence: 4 givenname: G. surname: Daufin fullname: Daufin, G. |
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| Issue | 3 |
| Keywords | Phosphates Infrared spectrometry Ultrafiltration Zirconium IV Oxides Membrane Photoelectron spectrometry X ray Selectivity Permeability Experimental study Mass transfer SPECTROSCOPIE IR TENEUR EN PROTEINE |
| Language | English |
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| Snippet | Ultrafiltration of various types of whey was carried out through an inorganic membrane (M
4 Carbosep, 20000 Da cut-off). Fouling was evaluated as a hydraulic... |
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| SubjectTerms | Biochemistry, Molecular Biology Biophysics Chemistry Colloidal gels. Colloidal sols Colloidal state and disperse state Exact sciences and technology General and physical chemistry Life Sciences |
| Title | Fouling of inorganic membranes during whey ultrafiltration: Analytical methodology |
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