In Situ Growth of CoS Nanosheets on Carbon Fiber Surfaces to Enhance the Interfacial Properties of Carbon Fiber/Norbornene Polyimide Composites
This study presents a novel method for altering the surface properties of carbon fiber (CF) to improve the bonding strength at its interface with norbornene–polyimide (PI-NA) resin. Cobaltous sulfide (CoS) nanosheets were successfully synthesized on the CF surface using a solvothermal method combine...
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| Published in | Materials Vol. 18; no. 10; p. 2334 |
|---|---|
| Main Authors | , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
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17.05.2025
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| ISSN | 1996-1944 1996-1944 |
| DOI | 10.3390/ma18102334 |
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| Abstract | This study presents a novel method for altering the surface properties of carbon fiber (CF) to improve the bonding strength at its interface with norbornene–polyimide (PI-NA) resin. Cobaltous sulfide (CoS) nanosheets were successfully synthesized on the CF surface using a solvothermal method combined with a chemical sulfidation process. The modification increased the specific surface area and surface roughness of the CFs, enhancing the interfacial mechanical lock-in effect between the fibers and the resin. This facilitated effective load transfer between the resin and the fibers, thereby significantly improving the interfacial strength of CF-reinforced polymers (CFRPs). The experimental findings showed that after solvothermal treatment with a precursor solution of 0.006 g/mL for 4.5 h, vertical CoS nanosheets were successfully grown on the CF surface. The interlaminar shear strength (ILSS) and interfacial shear strength (IFSS) of the modified CF reached 60.03 MPa and 83.27 MPa, respectively, representing increases of 19.49% and 27.01% compared to untreated fiber composites. This research demonstrates that this method is simple to apply and promising in terms of industrial scalability. |
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| AbstractList | This study presents a novel method for altering the surface properties of carbon fiber (CF) to improve the bonding strength at its interface with norbornene–polyimide (PI-NA) resin. Cobaltous sulfide (CoS) nanosheets were successfully synthesized on the CF surface using a solvothermal method combined with a chemical sulfidation process. The modification increased the specific surface area and surface roughness of the CFs, enhancing the interfacial mechanical lock-in effect between the fibers and the resin. This facilitated effective load transfer between the resin and the fibers, thereby significantly improving the interfacial strength of CF-reinforced polymers (CFRPs). The experimental findings showed that after solvothermal treatment with a precursor solution of 0.006 g/mL for 4.5 h, vertical CoS nanosheets were successfully grown on the CF surface. The interlaminar shear strength (ILSS) and interfacial shear strength (IFSS) of the modified CF reached 60.03 MPa and 83.27 MPa, respectively, representing increases of 19.49% and 27.01% compared to untreated fiber composites. This research demonstrates that this method is simple to apply and promising in terms of industrial scalability. This study presents a novel method for altering the surface properties of carbon fiber (CF) to improve the bonding strength at its interface with norbornene-polyimide (PI-NA) resin. Cobaltous sulfide (CoS) nanosheets were successfully synthesized on the CF surface using a solvothermal method combined with a chemical sulfidation process. The modification increased the specific surface area and surface roughness of the CFs, enhancing the interfacial mechanical lock-in effect between the fibers and the resin. This facilitated effective load transfer between the resin and the fibers, thereby significantly improving the interfacial strength of CF-reinforced polymers (CFRPs). The experimental findings showed that after solvothermal treatment with a precursor solution of 0.006 g/mL for 4.5 h, vertical CoS nanosheets were successfully grown on the CF surface. The interlaminar shear strength (ILSS) and interfacial shear strength (IFSS) of the modified CF reached 60.03 MPa and 83.27 MPa, respectively, representing increases of 19.49% and 27.01% compared to untreated fiber composites. This research demonstrates that this method is simple to apply and promising in terms of industrial scalability.This study presents a novel method for altering the surface properties of carbon fiber (CF) to improve the bonding strength at its interface with norbornene-polyimide (PI-NA) resin. Cobaltous sulfide (CoS) nanosheets were successfully synthesized on the CF surface using a solvothermal method combined with a chemical sulfidation process. The modification increased the specific surface area and surface roughness of the CFs, enhancing the interfacial mechanical lock-in effect between the fibers and the resin. This facilitated effective load transfer between the resin and the fibers, thereby significantly improving the interfacial strength of CF-reinforced polymers (CFRPs). The experimental findings showed that after solvothermal treatment with a precursor solution of 0.006 g/mL for 4.5 h, vertical CoS nanosheets were successfully grown on the CF surface. The interlaminar shear strength (ILSS) and interfacial shear strength (IFSS) of the modified CF reached 60.03 MPa and 83.27 MPa, respectively, representing increases of 19.49% and 27.01% compared to untreated fiber composites. This research demonstrates that this method is simple to apply and promising in terms of industrial scalability. |
| Audience | Academic |
| Author | Wang, Qifen Kong, Guoqiang Zhu, Bo Ren, Xin Feng, Jianshun Hou, Xuejun Yu, Qiubing Liu, Wenbo Li, Dayong Qi, Fengjie Yuan, Wenjie Shao, Meng Zhao, Xiang Yu, Guang |
| AuthorAffiliation | 1 Shandong Institute of Nonmetallic Materials, Jinan 250031, China 2 Key Laboratory for Liquid Solid Structural Evolution and Processing of Materials (Ministry of Education), School of Materials Science and Engineering, Shandong University, Jinan 250061, China |
| AuthorAffiliation_xml | – name: 2 Key Laboratory for Liquid Solid Structural Evolution and Processing of Materials (Ministry of Education), School of Materials Science and Engineering, Shandong University, Jinan 250061, China – name: 1 Shandong Institute of Nonmetallic Materials, Jinan 250031, China |
| Author_xml | – sequence: 1 givenname: Guoqiang surname: Kong fullname: Kong, Guoqiang – sequence: 2 givenname: Jianshun surname: Feng fullname: Feng, Jianshun – sequence: 3 givenname: Fengjie surname: Qi fullname: Qi, Fengjie – sequence: 4 givenname: Meng surname: Shao fullname: Shao, Meng – sequence: 5 givenname: Qiubing surname: Yu fullname: Yu, Qiubing – sequence: 6 givenname: Guang surname: Yu fullname: Yu, Guang – sequence: 7 givenname: Xin surname: Ren fullname: Ren, Xin – sequence: 8 givenname: Wenjie surname: Yuan fullname: Yuan, Wenjie – sequence: 9 givenname: Qifen surname: Wang fullname: Wang, Qifen – sequence: 10 givenname: Wenbo surname: Liu fullname: Liu, Wenbo – sequence: 11 givenname: Xiang surname: Zhao fullname: Zhao, Xiang – sequence: 12 givenname: Dayong surname: Li fullname: Li, Dayong – sequence: 13 givenname: Xuejun surname: Hou fullname: Hou, Xuejun – sequence: 14 givenname: Bo surname: Zhu fullname: Zhu, Bo |
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| Keywords | CoS nanosheet carbon fiber interfacial strength PI-NA mechanical lock-in effect |
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| SubjectTerms | Analysis Carbon fibers Composite materials Epoxy resins Fiber composites Interfacial bonding Interfacial properties Interfacial shear strength Interfacial strength Load transfer Nanomaterials Nanoparticles Nanosheets Oxidation Polyimide resins Polymers Shear strength Sulfidation Sulfides Surface properties Surface roughness Zinc oxides |
| Title | In Situ Growth of CoS Nanosheets on Carbon Fiber Surfaces to Enhance the Interfacial Properties of Carbon Fiber/Norbornene Polyimide Composites |
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