Investigation on magnetic properties of mechanically alloyed τ-MnAlC with Fe addition

•High purity of τ-Mn51-xFexAl47C2 (x = 0, 0.5, 1, 2, and 4) up to 98% was obtained.•Thermal stability of both ε and τ phases was enhanced by the addition of Fe.•Ms and TC of Fe doped τ-MnAlC showed a reduction compared to iron free τ-MnAlC.•Calculation showed a smaller magnetic moment of Fe compared...

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Published inJournal of magnetism and magnetic materials Vol. 546; p. 168892
Main Authors Nguyen, Van Tang, Mazaleyrat, Frédéric, Calvayrac, Florent, Ngo, Quang Minh, Randrianantoandro, Nirina
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 15.03.2022
Elsevier BV
Elsevier
Subjects
Coercivity
Computational Physics
Crystallography
Curie temperature
High temperature
Iron
Magnetic moments
Magnetic properties
Magnetism
Manganese
Mechanical alloying
MnFeAlC alloy
Physics
Reduction
Temperature
Thermal stability
Thermal Stability, Magnetic properties
Transformation temperature
Thermal Stability, Magnetic properties
Mechanical alloying
MnFeAlC alloy
Thermal Stability
Magnetic properties
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Abstract •High purity of τ-Mn51-xFexAl47C2 (x = 0, 0.5, 1, 2, and 4) up to 98% was obtained.•Thermal stability of both ε and τ phases was enhanced by the addition of Fe.•Ms and TC of Fe doped τ-MnAlC showed a reduction compared to iron free τ-MnAlC.•Calculation showed a smaller magnetic moment of Fe compared to Mn in τ-Mn(Fe)AlC. The influence of Fe addition on thermal stability, crystallography, and magnetic properties of τ-Mn51Al47C2 was investigated. Alloys with composition Mn51-xFexAl47C2 (x = 0, 0.5, 1, 2, and 4) were synthesized by mechanical alloying method. High purity of τ-Mn(Fe)AlC up to 98% could be obtained after 10 h of milling, then annealed at 1050 °C for 1 h, and followed by an aging process at appropriate temperatures from 515 to 540 °C for 50 min. It was found that the thermal stability of both ε and τ phases was enhanced by the addition of Fe up to 4 at.% into MnAlC alloy through a shifting of ε-to-τ transformation temperature to high temperature region and a reduction in c/a ratio of Fe doped τ-MnAlC compared to iron free τ-MnAlC. While the magnetization and Curie temperature of Fe doped τ-MnAlC showed a reduction compared to iron free τ-Mn51Al47C2, coercivity seems not to be significantly affected. Ab initio calculation showed a lower magnetic moment of Fe (μFe = 1.77 μB) compared to Mn (μMn_average = 2.36 μB) in τ-Mn(Fe)AlC when Fe substituted Mn position at 1a site.
AbstractList The influence of Fe addition on thermal stability, crystallography, and magnetic properties of τ-Mn51Al47C2 was investigated. Alloys with composition Mn51-xFexAl47C2 (x = 0, 0.5, 1, 2, and 4) were synthesized by mechanical alloying method. High purity of τ-Mn(Fe)AlC up to 98% could be obtained after 10 h of milling, then annealed at 1050 °C for 1 h, and followed by an aging process at appropriate temperatures from 515 to 540 °C for 50 min. It was found that the thermal stability of both ε and τ phases was enhanced by the addition of Fe up to 4 at.% into MnAlC alloy through a shifting of ε-to-τ transformation temperature to high temperature region and a reduction in c/a ratio of Fe doped τ-MnAlC compared to iron free τ-MnAlC. While the magnetization and Curie temperature of Fe doped τ-MnAlC showed a reduction compared to iron free τ-Mn51Al47C2, coercivity seems not to be significantly affected. Ab initio calculation showed a lower magnetic moment of Fe (μFe = 1.77 μB) compared to Mn (μMn_average = 2.36 μB) in τ-Mn(Fe)AlC when Fe substituted Mn position at 1a site.
•High purity of τ-Mn51-xFexAl47C2 (x = 0, 0.5, 1, 2, and 4) up to 98% was obtained.•Thermal stability of both ε and τ phases was enhanced by the addition of Fe.•Ms and TC of Fe doped τ-MnAlC showed a reduction compared to iron free τ-MnAlC.•Calculation showed a smaller magnetic moment of Fe compared to Mn in τ-Mn(Fe)AlC. The influence of Fe addition on thermal stability, crystallography, and magnetic properties of τ-Mn51Al47C2 was investigated. Alloys with composition Mn51-xFexAl47C2 (x = 0, 0.5, 1, 2, and 4) were synthesized by mechanical alloying method. High purity of τ-Mn(Fe)AlC up to 98% could be obtained after 10 h of milling, then annealed at 1050 °C for 1 h, and followed by an aging process at appropriate temperatures from 515 to 540 °C for 50 min. It was found that the thermal stability of both ε and τ phases was enhanced by the addition of Fe up to 4 at.% into MnAlC alloy through a shifting of ε-to-τ transformation temperature to high temperature region and a reduction in c/a ratio of Fe doped τ-MnAlC compared to iron free τ-MnAlC. While the magnetization and Curie temperature of Fe doped τ-MnAlC showed a reduction compared to iron free τ-Mn51Al47C2, coercivity seems not to be significantly affected. Ab initio calculation showed a lower magnetic moment of Fe (μFe = 1.77 μB) compared to Mn (μMn_average = 2.36 μB) in τ-Mn(Fe)AlC when Fe substituted Mn position at 1a site.
ArticleNumber 168892
Author Ngo, Quang Minh
Randrianantoandro, Nirina
Calvayrac, Florent
Nguyen, Van Tang
Mazaleyrat, Frédéric
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  givenname: Frédéric
  surname: Mazaleyrat
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  givenname: Florent
  surname: Calvayrac
  fullname: Calvayrac, Florent
  organization: Institut des Molécules et Matériaux du Mans – UMR CNRS n°6283, Le Mans Université, Avenue Olivier Messiaen, 72085 LE MANS Cedex 9, France
– sequence: 4
  givenname: Quang Minh
  surname: Ngo
  fullname: Ngo, Quang Minh
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  givenname: Nirina
  surname: Randrianantoandro
  fullname: Randrianantoandro, Nirina
  organization: Institut des Molécules et Matériaux du Mans – UMR CNRS n°6283, Le Mans Université, Avenue Olivier Messiaen, 72085 LE MANS Cedex 9, France
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Keywords Thermal Stability, Magnetic properties
Mechanical alloying
MnFeAlC alloy
Thermal Stability
Magnetic properties
Language English
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Snippet •High purity of τ-Mn51-xFexAl47C2 (x = 0, 0.5, 1, 2, and 4) up to 98% was obtained.•Thermal stability of both ε and τ phases was enhanced by the addition of...
The influence of Fe addition on thermal stability, crystallography, and magnetic properties of τ-Mn51Al47C2 was investigated. Alloys with composition...
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StartPage 168892
SubjectTerms Coercivity
Computational Physics
Crystallography
Curie temperature
High temperature
Iron
Magnetic moments
Magnetic properties
Magnetism
Manganese
Mechanical alloying
MnFeAlC alloy
Physics
Reduction
Temperature
Thermal stability
Thermal Stability, Magnetic properties
Transformation temperature
Title Investigation on magnetic properties of mechanically alloyed τ-MnAlC with Fe addition
URI https://dx.doi.org/10.1016/j.jmmm.2021.168892
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https://univ-lemans.hal.science/hal-03454133
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