Developments in single-drop microextraction

Single-drop microextraction (SDME) has become a very popular liquid-phase microextraction technique because it is inexpensive, easy to operate and nearly solvent-free. Essentially, SDME combines extraction (and conceivably, cleanup) and concentration in a minimum number of steps, and thereafter, dir...

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Published inJournal of Chromatography A Vol. 1152; no. 1; pp. 184 - 192
Main Authors Xu, Li, Basheer, Chanbasha, Lee, Hian Kee
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 08.06.2007
Subjects
Online AccessGet full text
ISSN0021-9673
DOI10.1016/j.chroma.2006.10.073

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Abstract Single-drop microextraction (SDME) has become a very popular liquid-phase microextraction technique because it is inexpensive, easy to operate and nearly solvent-free. Essentially, SDME combines extraction (and conceivably, cleanup) and concentration in a minimum number of steps, and thereafter, direct extract introduction into an analytical system. In this review, in order to encourage further development of SDME, we focus on its recent developments in its various guises. Its applications when used in combination with different analytical techniques, such as gas chromatography, high-performance liquid chromatography, inductively-coupled plasma mass spectrometry, capillary electrophoresis, mass spectrometry and electrothermal atomic absorption spectrometry, are summarized. SDME does have some limitations, and these are also discussed as well. Finally, an outlook on the future of the technique is given.
AbstractList Single-drop microextraction (SDME) has become a very popular liquid-phase microextraction technique because it is inexpensive, easy to operate and nearly solvent-free. Essentially, SDME combines extraction (and conceivably, cleanup) and concentration in a minimum number of steps, and thereafter, direct extract introduction into an analytical system. In this review, in order to encourage further development of SDME, we focus on its recent developments in its various guises. Its applications when used in combination with different analytical techniques, such as gas chromatography, high-performance liquid chromatography, inductively-coupled plasma mass spectrometry, capillary electrophoresis, mass spectrometry and electrothermal atomic absorption spectrometry, are summarized. SDME does have some limitations, and these are also discussed as well. Finally, an outlook on the future of the technique is given.
Single-drop microextraction (SDME) has become a very popular liquid-phase microextraction technique because it is inexpensive, easy to operate and nearly solvent-free. Essentially, SDME combines extraction (and conceivably, cleanup) and concentration in a minimum number of steps, and thereafter, direct extract introduction into an analytical system. In this review, in order to encourage further development of SDME, we focus on its recent developments in its various guises. Its applications when used in combination with different analytical techniques, such as gas chromatography, high-performance liquid chromatography, inductively-coupled plasma mass spectrometry, capillary electrophoresis, mass spectrometry and electrothermal atomic absorption spectrometry, are summarized. SDME does have some limitations, and these are also discussed as well. Finally, an outlook on the future of the technique is given.Single-drop microextraction (SDME) has become a very popular liquid-phase microextraction technique because it is inexpensive, easy to operate and nearly solvent-free. Essentially, SDME combines extraction (and conceivably, cleanup) and concentration in a minimum number of steps, and thereafter, direct extract introduction into an analytical system. In this review, in order to encourage further development of SDME, we focus on its recent developments in its various guises. Its applications when used in combination with different analytical techniques, such as gas chromatography, high-performance liquid chromatography, inductively-coupled plasma mass spectrometry, capillary electrophoresis, mass spectrometry and electrothermal atomic absorption spectrometry, are summarized. SDME does have some limitations, and these are also discussed as well. Finally, an outlook on the future of the technique is given.
Author Basheer, Chanbasha
Xu, Li
Lee, Hian Kee
Author_xml – sequence: 1
  givenname: Li
  surname: Xu
  fullname: Xu, Li
– sequence: 2
  givenname: Chanbasha
  surname: Basheer
  fullname: Basheer, Chanbasha
– sequence: 3
  givenname: Hian Kee
  surname: Lee
  fullname: Lee, Hian Kee
  email: chmleehk@nus.edu.sg
BackLink https://www.ncbi.nlm.nih.gov/pubmed/17097670$$D View this record in MEDLINE/PubMed
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Snippet Single-drop microextraction (SDME) has become a very popular liquid-phase microextraction technique because it is inexpensive, easy to operate and nearly...
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SubjectTerms Analytic Sample Preparation Methods - methods
Chromatography, Gas - methods
Chromatography, High Pressure Liquid - methods
Electrophoresis, Capillary - methods
Liquid-phase microextraction
Mass Spectrometry - methods
Microchemistry - methods
Single-drop microextraction
Solvent-minimized extractions
Title Developments in single-drop microextraction
URI https://dx.doi.org/10.1016/j.chroma.2006.10.073
https://www.ncbi.nlm.nih.gov/pubmed/17097670
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