Processing and characterization of low-cost electrospun carbon fibers from organosolv lignin/polyacrylonitrile blends
The esterification of lignin with butyric anhydride decreases both the viscosity of lignin/PAN blend spinning solutions and their glass-transition temperature compared to unmodified lignin/PAN blends. The effect of blending PAN with lignin before or after butyration on the electrospinnability, misci...
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| Published in | Carbon (New York) Vol. 100; pp. 126 - 136 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.04.2016
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The esterification of lignin with butyric anhydride decreases both the viscosity of lignin/PAN blend spinning solutions and their glass-transition temperature compared to unmodified lignin/PAN blends. The effect of blending PAN with lignin before or after butyration on the electrospinnability, miscibility and thermal stability of precursor blend fibers was investigated by morphological, rheological, and thermal analysis. The micromorphology, carbon structure, and mechanical properties of resultant carbonized fibers (CFs) were further evaluated. This study reveals a new approach to controlling inter-fiber bonding of lignin-based carbon nanofiber mats by manipulating the molecular structure of lignin while following a standard procedure of thermo-stabilization and carbonization treatment. Characterization results indicate that inter-fiber bonding in electrospun CF mats, induced by the high thermal mobility of butyrated lignin, favorably affected their mechanical properties. |
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| AbstractList | The esterification of lignin with butyric anhydride decreases both the viscosity of lignin/PAN blend spinning solutions and their glass-transition temperature compared to unmodified lignin/PAN blends. The effect of blending PAN with lignin before or after butyration on the electrospinnability, miscibility and thermal stability of precursor blend fibers was investigated by morphological, rheological, and thermal analysis. The micromorphology, carbon structure, and mechanical properties of resultant carbonized fibers (CFs) were further evaluated. This study reveals a new approach to controlling inter-fiber bonding of lignin-based carbon nanofiber mats by manipulating the molecular structure of lignin while following a standard procedure of thermo-stabilization and carbonization treatment. Characterization results indicate that inter-fiber bonding in electrospun CF mats, induced by the high thermal mobility of butyrated lignin, favorably affected their mechanical properties. |
| Author | Ding, Rui Thunga, Mahendra Kessler, Michael R. Bowler, Nicola Wu, Hongchao |
| Author_xml | – sequence: 1 givenname: Rui surname: Ding fullname: Ding, Rui organization: Department of Materials Science and Engineering, Iowa State University, Ames IA, USA – sequence: 2 givenname: Hongchao surname: Wu fullname: Wu, Hongchao organization: Department of Materials Science and Engineering, Iowa State University, Ames IA, USA – sequence: 3 givenname: Mahendra surname: Thunga fullname: Thunga, Mahendra organization: Department of Materials Science and Engineering, Iowa State University, Ames IA, USA – sequence: 4 givenname: Nicola surname: Bowler fullname: Bowler, Nicola organization: Department of Materials Science and Engineering, Iowa State University, Ames IA, USA – sequence: 5 givenname: Michael R. orcidid: 0000-0001-8436-3447 surname: Kessler fullname: Kessler, Michael R. email: michaelr.kessler@wsu.edu organization: School of Mechanical and Materials Engineering, Washington State University, Pullman WA, USA |
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| Snippet | The esterification of lignin with butyric anhydride decreases both the viscosity of lignin/PAN blend spinning solutions and their glass-transition temperature... |
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| SubjectTerms | carbon carbon fibers carbon nanofibers carbonization chemical structure esterification glass transition temperature lignin mechanical properties microstructure mixing polyacrylonitrile spinning thermal analysis thermal stability viscosity |
| Title | Processing and characterization of low-cost electrospun carbon fibers from organosolv lignin/polyacrylonitrile blends |
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