Facile and scalable preparation of cage-like mesoporous carbon from lignin-based phenolic resin and its application in supercapacitor electrodes
Due to the similarity in chemical structure, lignin has presented great potential in the synthesis of bio-based phenolic resin. Herein, a facile and scalable synthesis strategy for a novel cage-like lignin-based phenolic resin was proposed through direct spray drying of the mixture of phenolic resin...
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| Published in | Carbon (New York) Vol. 196; pp. 819 - 827 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
30.08.2022
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| Subjects | |
| Online Access | Get full text |
| ISSN | 0008-6223 1873-3891 |
| DOI | 10.1016/j.carbon.2022.05.053 |
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| Abstract | Due to the similarity in chemical structure, lignin has presented great potential in the synthesis of bio-based phenolic resin. Herein, a facile and scalable synthesis strategy for a novel cage-like lignin-based phenolic resin was proposed through direct spray drying of the mixture of phenolic resin and unmodified lignin. The as-prepared lignin-based phenolic resin was pre-carbonized and carbonized using KOH to produce mesoporous carbon materials (LPRAC) that were further employed as supercapacitor electrodes. The results revealed that the lignin addition led to the noticeable change of the resin shape from perfect sphere to cage-like structure owing to the surfactivity and hydrophilicity of lignin. The cage-like structure promoted the KOH-activated pore generation and expansion in the carbonization process, resulting in the significantly increased specific surface area of the phenolic carbon and the intensified mesoporous formation. The electrochemical performance determination indicated that the specific capacitance of LPRAC-20% (20% lignin addition) was 217.3 F/g at 0.5 A/g, which was considerably higher than that of the lignin-free phenolic carbon (122.6 F/g). Moreover, the LPRAC-20% also exhibited preferable capacitance retention and excellent cycling stability. Accordingly, the present work offers a simple and scalable approach to prepare cage-like mesoporous carbon with excellent electrochemical performance from lignin-based phenolic resin and thus provides a promising route for lignin valorization in energy storage materials.
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| AbstractList | Due to the similarity in chemical structure, lignin has presented great potential in the synthesis of bio-based phenolic resin. Herein, a facile and scalable synthesis strategy for a novel cage-like lignin-based phenolic resin was proposed through direct spray drying of the mixture of phenolic resin and unmodified lignin. The as-prepared lignin-based phenolic resin was pre-carbonized and carbonized using KOH to produce mesoporous carbon materials (LPRAC) that were further employed as supercapacitor electrodes. The results revealed that the lignin addition led to the noticeable change of the resin shape from perfect sphere to cage-like structure owing to the surfactivity and hydrophilicity of lignin. The cage-like structure promoted the KOH-activated pore generation and expansion in the carbonization process, resulting in the significantly increased specific surface area of the phenolic carbon and the intensified mesoporous formation. The electrochemical performance determination indicated that the specific capacitance of LPRAC-20% (20% lignin addition) was 217.3 F/g at 0.5 A/g, which was considerably higher than that of the lignin-free phenolic carbon (122.6 F/g). Moreover, the LPRAC-20% also exhibited preferable capacitance retention and excellent cycling stability. Accordingly, the present work offers a simple and scalable approach to prepare cage-like mesoporous carbon with excellent electrochemical performance from lignin-based phenolic resin and thus provides a promising route for lignin valorization in energy storage materials. Due to the similarity in chemical structure, lignin has presented great potential in the synthesis of bio-based phenolic resin. Herein, a facile and scalable synthesis strategy for a novel cage-like lignin-based phenolic resin was proposed through direct spray drying of the mixture of phenolic resin and unmodified lignin. The as-prepared lignin-based phenolic resin was pre-carbonized and carbonized using KOH to produce mesoporous carbon materials (LPRAC) that were further employed as supercapacitor electrodes. The results revealed that the lignin addition led to the noticeable change of the resin shape from perfect sphere to cage-like structure owing to the surfactivity and hydrophilicity of lignin. The cage-like structure promoted the KOH-activated pore generation and expansion in the carbonization process, resulting in the significantly increased specific surface area of the phenolic carbon and the intensified mesoporous formation. The electrochemical performance determination indicated that the specific capacitance of LPRAC-20% (20% lignin addition) was 217.3 F/g at 0.5 A/g, which was considerably higher than that of the lignin-free phenolic carbon (122.6 F/g). Moreover, the LPRAC-20% also exhibited preferable capacitance retention and excellent cycling stability. Accordingly, the present work offers a simple and scalable approach to prepare cage-like mesoporous carbon with excellent electrochemical performance from lignin-based phenolic resin and thus provides a promising route for lignin valorization in energy storage materials. [Display omitted] |
| Author | Si, Chuanling Li, Zhifang Li, Wei Parvez, Ashak Mahmud Sui, Wenjie Wang, Guanhua Xu, Ting |
| Author_xml | – sequence: 1 givenname: Wei surname: Li fullname: Li, Wei organization: Tianjin Key Laboratory of Pulp and Paper, College of Light Industry Science and Engineering, Tianjin University of Science and Technology, Tianjin, 300457, China – sequence: 2 givenname: Guanhua surname: Wang fullname: Wang, Guanhua email: ghwang@tust.edu.cn organization: Tianjin Key Laboratory of Pulp and Paper, College of Light Industry Science and Engineering, Tianjin University of Science and Technology, Tianjin, 300457, China – sequence: 3 givenname: Wenjie surname: Sui fullname: Sui, Wenjie organization: State Key Laboratory of Food Nutrition and Safety, College of Food Science and Engineering, Tianjin University of Science & Technology, Tianjin, 300457, China – sequence: 4 givenname: Ting surname: Xu fullname: Xu, Ting organization: Tianjin Key Laboratory of Pulp and Paper, College of Light Industry Science and Engineering, Tianjin University of Science and Technology, Tianjin, 300457, China – sequence: 5 givenname: Zhifang surname: Li fullname: Li, Zhifang organization: Shandong Shengquan New Materials Co., LTD, Shandong, 250204, China – sequence: 6 givenname: Ashak Mahmud surname: Parvez fullname: Parvez, Ashak Mahmud organization: Department of Mechanical Engineering, University of New Brunswick, Fredericton, NB, E3B 5A3, Canada – sequence: 7 givenname: Chuanling orcidid: 0000-0003-1630-7800 surname: Si fullname: Si, Chuanling email: sichli@tust.edu.cn organization: Tianjin Key Laboratory of Pulp and Paper, College of Light Industry Science and Engineering, Tianjin University of Science and Technology, Tianjin, 300457, China |
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| Keywords | Electrochemical performance KOH activation Supercapacitor electrodes Lignin-based phenolic resin Cage-like mesoporous carbon |
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| SubjectTerms | Cage-like mesoporous carbon capacitance carbon carbonization chemical structure electrochemical capacitors Electrochemical performance electrochemistry energy hydrophilicity KOH activation lignin Lignin-based phenolic resin phenolic resins porous media Supercapacitor electrodes surface area |
| Title | Facile and scalable preparation of cage-like mesoporous carbon from lignin-based phenolic resin and its application in supercapacitor electrodes |
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