Microstructural evolution of a nickel-based superalloy during hot deformation

[Display omitted] •Deformation parameters have significant influences on the grain microstructure.•The dislocation substructure is also very sensitive to the deformation parameters.•The bulging of initial grain boundaries is the main nucleation mechanism of DRX.•The complete DRX domains are determin...

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Published inMaterials in engineering Vol. 77; pp. 41 - 49
Main Authors Chen, Xiao-Min, Lin, Y.C., Chen, Ming-Song, Li, Hong-Bin, Wen, Dong-Xu, Zhang, Jin-Long, He, Min
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 15.07.2015
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Abstract [Display omitted] •Deformation parameters have significant influences on the grain microstructure.•The dislocation substructure is also very sensitive to the deformation parameters.•The bulging of initial grain boundaries is the main nucleation mechanism of DRX.•The complete DRX domains are determined by DRX volume fractions contour map. Hot compressive tests of a nickel-based superalloy are performed under the strain rate range of 0.001–1s−1 and deformation temperature range of 920–1040°C. Optical microscopy (OM) and transmission electron microscopy (TEM) are employed to investigate the evolution of dynamic recrystallized (DRX) grain and dislocation substructure. It is found that the effects of deformation degree, strain rate and deformation temperature on DRX grain are significant. When the deformation degree or temperature is increased, the number of DRX grains rapidly increases. But, the increase of strain rate reduces the number of DRX grains. The dislocation substructure is also very sensitive to the deformation degree, strain rate and deformation temperature. With the increase of deformation degree, the evolution of dislocation substructure can be characterized as: high dislocation density→dislocation network→subgrain→DRX grain. Under high deformation temperatures or low strain rates, the dislocation substructure can be easily annihilated and rearranged because of the occurrence of DRX. Based on the evaluated DRX volume fractions, the contour map is constructed to optimize the hot deformation parameters.
AbstractList Hot compressive tests of a nickel-based superalloy are performed under the strain rate range of 0.001-1s- 1 and deformation temperature range of 920-1040 degree C. Optical microscopy (OM) and transmission electron microscopy (TEM) are employed to investigate the evolution of dynamic recrystallized (DRX) grain and dislocation substructure. It is found that the effects of deformation degree, strain rate and deformation temperature on DRX grain are significant. When the deformation degree or temperature is increased, the number of DRX grains rapidly increases. But, the increase of strain rate reduces the number of DRX grains. The dislocation substructure is also very sensitive to the deformation degree, strain rate and deformation temperature. With the increase of deformation degree, the evolution of dislocation substructure can be characterized as: high dislocation density arrow right dislocation network arrow right subgrain arrow right DRX grain. Under high deformation temperatures or low strain rates, the dislocation substructure can be easily annihilated and rearranged because of the occurrence of DRX. Based on the evaluated DRX volume fractions, the contour map is constructed to optimize the hot deformation parameters.
[Display omitted] •Deformation parameters have significant influences on the grain microstructure.•The dislocation substructure is also very sensitive to the deformation parameters.•The bulging of initial grain boundaries is the main nucleation mechanism of DRX.•The complete DRX domains are determined by DRX volume fractions contour map. Hot compressive tests of a nickel-based superalloy are performed under the strain rate range of 0.001–1s−1 and deformation temperature range of 920–1040°C. Optical microscopy (OM) and transmission electron microscopy (TEM) are employed to investigate the evolution of dynamic recrystallized (DRX) grain and dislocation substructure. It is found that the effects of deformation degree, strain rate and deformation temperature on DRX grain are significant. When the deformation degree or temperature is increased, the number of DRX grains rapidly increases. But, the increase of strain rate reduces the number of DRX grains. The dislocation substructure is also very sensitive to the deformation degree, strain rate and deformation temperature. With the increase of deformation degree, the evolution of dislocation substructure can be characterized as: high dislocation density→dislocation network→subgrain→DRX grain. Under high deformation temperatures or low strain rates, the dislocation substructure can be easily annihilated and rearranged because of the occurrence of DRX. Based on the evaluated DRX volume fractions, the contour map is constructed to optimize the hot deformation parameters.
Author Wen, Dong-Xu
He, Min
Chen, Ming-Song
Chen, Xiao-Min
Zhang, Jin-Long
Li, Hong-Bin
Lin, Y.C.
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  surname: Chen
  fullname: Chen, Xiao-Min
  organization: School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China
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  givenname: Y.C.
  surname: Lin
  fullname: Lin, Y.C.
  email: yclin@csu.edu.cn, linyongcheng@163.com
  organization: School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China
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  givenname: Ming-Song
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  fullname: Chen, Ming-Song
  organization: School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China
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  givenname: Hong-Bin
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  organization: College of Metallurgy and Energy, Hebei United University, Tangshan 063009, China
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  givenname: Jin-Long
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  givenname: Min
  surname: He
  fullname: He, Min
  organization: School of Mechanical and Electrical Engineering, Central South University, Changsha 410083, China
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SSID ssj0017112
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Snippet [Display omitted] •Deformation parameters have significant influences on the grain microstructure.•The dislocation substructure is also very sensitive to the...
Hot compressive tests of a nickel-based superalloy are performed under the strain rate range of 0.001-1s- 1 and deformation temperature range of 920-1040...
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SubjectTerms Alloy
Deformation
Dislocations
Dynamic recrystallization
Evolution
Grains
Hot deformation
Microstructural evolution
Nickel base alloys
Strain rate
Substructures
Superalloys
Title Microstructural evolution of a nickel-based superalloy during hot deformation
URI https://dx.doi.org/10.1016/j.matdes.2015.04.004
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