Room temperature synthesis of CsPbX3 (X = Cl, Br, I) perovskite quantum dots by water-induced surface crystallization of glass
Currently, the mainstream method for preparing perovskite quantum dots in glass is a heat treatment method. Here, a new method for the preparation of CsPbX3 (X = Cl, Br, I) quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphates glass has been developed. A plausible water...
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| Published in | Journal of alloys and compounds Vol. 818; p. 152872 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Lausanne
Elsevier B.V
25.03.2020
Elsevier BV |
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| Abstract | Currently, the mainstream method for preparing perovskite quantum dots in glass is a heat treatment method. Here, a new method for the preparation of CsPbX3 (X = Cl, Br, I) quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphates glass has been developed. A plausible water-induced surface crystallization mechanism has been proposed, revealing that water can reduce the non-uniform nucleation barrier to induce crystallization. Through changing the ratio of Cl/Br/I halogen elements in the raw material, a whole-family of CsPbX3 QDs in tin fluorophosphate glass can be obtained, covering the entire visible band from 414 nm to 713 nm. Besides, the proposed material technology may exert a vital role in the field of anti-counterfeiting technology shortly.
A new method for the preparation of CsPbBr3 quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphates glass has been developed, which may exert a vital role in the field of anti-counterfeiting technology. [Display omitted]
•A completely new method for the preparation of CsPbX3 (X = Cl, Br, I) quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphate glass has been developed.•A plausible water-induced surface crystallization mechanism has been proposed, revealing that the activation energy decrease in the presence of hydroxyls was attributed to the breaking of [P–O–P] bonds of the glass structure by water. |
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| AbstractList | Currently, the mainstream method for preparing perovskite quantum dots in glass is a heat treatment method. Here, a new method for the preparation of CsPbX3 (X = Cl, Br, I) quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphates glass has been developed. A plausible water-induced surface crystallization mechanism has been proposed, revealing that water can reduce the non-uniform nucleation barrier to induce crystallization. Through changing the ratio of Cl/Br/I halogen elements in the raw material, a whole-family of CsPbX3 QDs in tin fluorophosphate glass can be obtained, covering the entire visible band from 414 nm to 713 nm. Besides, the proposed material technology may exert a vital role in the field of anti-counterfeiting technology shortly. Currently, the mainstream method for preparing perovskite quantum dots in glass is a heat treatment method. Here, a new method for the preparation of CsPbX3 (X = Cl, Br, I) quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphates glass has been developed. A plausible water-induced surface crystallization mechanism has been proposed, revealing that water can reduce the non-uniform nucleation barrier to induce crystallization. Through changing the ratio of Cl/Br/I halogen elements in the raw material, a whole-family of CsPbX3 QDs in tin fluorophosphate glass can be obtained, covering the entire visible band from 414 nm to 713 nm. Besides, the proposed material technology may exert a vital role in the field of anti-counterfeiting technology shortly. A new method for the preparation of CsPbBr3 quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphates glass has been developed, which may exert a vital role in the field of anti-counterfeiting technology. [Display omitted] •A completely new method for the preparation of CsPbX3 (X = Cl, Br, I) quantum dots (QDs) by water-induced surface crystallization in tin fluorophosphate glass has been developed.•A plausible water-induced surface crystallization mechanism has been proposed, revealing that the activation energy decrease in the presence of hydroxyls was attributed to the breaking of [P–O–P] bonds of the glass structure by water. |
| ArticleNumber | 152872 |
| Author | Wang, Yajie Zhang, Renli Chen, Danping Yue, Yu Zhang, Liyan Yan, Sasa |
| Author_xml | – sequence: 1 givenname: Yajie surname: Wang fullname: Wang, Yajie organization: Key Laboratory of Materials for High Power Laser, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai, 201800, China – sequence: 2 givenname: Renli surname: Zhang fullname: Zhang, Renli organization: Key Laboratory of Materials for High Power Laser, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai, 201800, China – sequence: 3 givenname: Yu surname: Yue fullname: Yue, Yu organization: College of Science, Shandong Jianzhu University, Jinan, 250101, China – sequence: 4 givenname: Sasa surname: Yan fullname: Yan, Sasa organization: Key Laboratory of Materials for High Power Laser, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai, 201800, China – sequence: 5 givenname: Liyan orcidid: 0000-0003-0269-7959 surname: Zhang fullname: Zhang, Liyan email: jndxzly@hotmail.com organization: Key Laboratory of Materials for High Power Laser, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai, 201800, China – sequence: 6 givenname: Danping surname: Chen fullname: Chen, Danping email: dpchen2008@aliyun.com organization: Key Laboratory of Materials for High Power Laser, Shanghai Institute of Optics and Fine Mechanics, Chinese Academy of Sciences, Shanghai, 201800, China |
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| Snippet | Currently, the mainstream method for preparing perovskite quantum dots in glass is a heat treatment method. Here, a new method for the preparation of CsPbX3... Currently, the mainstream method for preparing perovskite quantum dots in glass is a heat treatment method. Here, a new method for the preparation of CsPbX3 (X... |
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| SubjectTerms | Crystallization CsPbX3 Glass Heat treatment Nucleation Perovskites Quantum dots Room temperature Surface crystallization Water-induced |
| Title | Room temperature synthesis of CsPbX3 (X = Cl, Br, I) perovskite quantum dots by water-induced surface crystallization of glass |
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