Facile preparation and characterization of poly(vinyl alcohol)/chitosan/graphene oxide biocomposite nanofibers
Poly(vinyl alcohol) (PVA)/chitosan (CS)/graphene oxide (GO) biocomposite nanofibers have been successfully prepared using aqueous solution by electrospinning. CS colloidal gel in 1% acetic acid can be changed to homogeneous solution by using electron beam irradiation (EBI). The uniform distributions...
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| Published in | Journal of industrial and engineering chemistry (Seoul, Korea) Vol. 20; no. 6; pp. 4415 - 4420 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
25.11.2014
한국공업화학회 |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Poly(vinyl alcohol) (PVA)/chitosan (CS)/graphene oxide (GO) biocomposite nanofibers have been successfully prepared using aqueous solution by electrospinning. CS colloidal gel in 1% acetic acid can be changed to homogeneous solution by using electron beam irradiation (EBI). The uniform distributions of GO sheets in the nanofibers were investigated by field emission scanning electron microscopy (FESEM) and Raman spectroscopy. FESEM images illustrated that the spread single GO sheet embedding into nanofibers was formed via self-assembly of GO sheet and PVA/CS chains. And the average diameters of the biocomposite nanofibers decreased (200, 173, 160 and 123nm) with increasing the contents of GO (0.05, 0.2, 0.4 and 0.6wt%). Raman spectra verified the presence of GO in the biocomposite nanofibrous mats. The mechanical properties of as-prepared materials related with GO contents. It revealed that the highest tensile strength was 2.78MPa, which was 25% higher than that of neat PVA/CS nanofibers. Antibacterial test demonstrated that the addition of GO to PVA/CS nanofiber had great ability to increase inhibition zone till 8.6mm. Overall, these features of PVA/CS/GO nanofibers which were prepared by eco-friendly solvent can be a promising candidate material in tissue engineering, wound healing and drug delivery system. |
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| AbstractList | Poly(vinyl alcohol) (PVA)/chitosan (CS)/graphene oxide (GO) biocomposite nanofibers have been successfully prepared using aqueous solution by electrospinning. CS colloidal gel in 1% acetic acid can be changed to homogeneous solution by using electron beam irradiation (EBI). The uniform distributions of GO sheets in the nanofibers were investigated by field emission scanning electron microscopy (FESEM) and Raman spectroscopy. FESEM images illustrated that the spread single GO sheet embedding into nanofibers was formed via self-assembly of GO sheet and PVA/CS chains. And the average diameters of the biocomposite nanofibers decreased (200, 173, 160 and 123nm) with increasing the contents of GO (0.05, 0.2, 0.4 and 0.6wt%). Raman spectra verified the presence of GO in the biocomposite nanofibrous mats. The mechanical properties of as-prepared materials related with GO contents. It revealed that the highest tensile strength was 2.78MPa, which was 25% higher than that of neat PVA/CS nanofibers. Antibacterial test demonstrated that the addition of GO to PVA/CS nanofiber had great ability to increase inhibition zone till 8.6mm. Overall, these features of PVA/CS/GO nanofibers which were prepared by eco-friendly solvent can be a promising candidate material in tissue engineering, wound healing and drug delivery system. Poly(vinyl alcohol) (PVA)/chitosan (CS)/graphene oxide (GO) biocomposite nanofibers have beensuccessfully prepared using aqueous solution by electrospinning. CS colloidal gel in 1% acetic acid can bechanged to homogeneous solution by using electron beam irradiation (EBI). The uniform distributions ofGO sheets in the nanofibers were investigated by field emission scanning electron microscopy (FESEM)and Raman spectroscopy. FESEM images illustrated that the spread single GO sheet embedding intonanofibers was formed via self-assembly of GO sheet and PVA/CS chains. And the average diameters ofthe biocomposite nanofibers decreased (200, 173, 160 and 123 nm) with increasing the contents of GO(0.05, 0.2, 0.4 and 0.6 wt%). Raman spectra verified the presence of GO in the biocomposite nanofibrousmats. The mechanical properties of as-prepared materials related with GO contents. It revealed that thehighest tensile strength was 2.78 MPa, which was 25% higher than that of neat PVA/CS nanofibers. Antibacterial test demonstrated that the addition of GO to PVA/CS nanofiber had great ability to increaseinhibition zone till 8.6 mm. Overall, these features of PVA/CS/GO nanofibers which were prepared byeco-friendly solvent can be a promising candidate material in tissue engineering, wound healing anddrug delivery system. KCI Citation Count: 89 |
| Author | Choi, Jawun Park, Yong Wan Park, Soo-Jin Pant, Bishweshwar Kim, Hak-Yong Lee, Jun Youb Park, Mira Liu, Yanan Shin, Hye Kyoung |
| Author_xml | – sequence: 1 givenname: Yanan surname: Liu fullname: Liu, Yanan organization: Department of BIN Fusion Technology, Chonbuk National University, Jeonju 561-756, Republic of Korea – sequence: 2 givenname: Mira surname: Park fullname: Park, Mira organization: Department of Organic Materials and Fiber Engineering, Chonbuk National University, Jeonju 561-756, Republic of Korea – sequence: 3 givenname: Hye Kyoung surname: Shin fullname: Shin, Hye Kyoung organization: Department of Chemistry, Inha University, 100 Inharo, Incheon 402-751, Republic of Korea – sequence: 4 givenname: Bishweshwar surname: Pant fullname: Pant, Bishweshwar organization: Department of BIN Fusion Technology, Chonbuk National University, Jeonju 561-756, Republic of Korea – sequence: 5 givenname: Jawun surname: Choi fullname: Choi, Jawun organization: Department of BIN Fusion Technology, Chonbuk National University, Jeonju 561-756, Republic of Korea – sequence: 6 givenname: Yong Wan surname: Park fullname: Park, Yong Wan organization: Korea Institute for Knit Industry, 639 Sukam-dong, Iksan-si, Jeollabuk-do 570-330, Republic of Korea – sequence: 7 givenname: Jun Youb surname: Lee fullname: Lee, Jun Youb organization: Department of Organic Materials and Fiber Engineering, Chonbuk National University, Jeonju 561-756, Republic of Korea – sequence: 8 givenname: Soo-Jin surname: Park fullname: Park, Soo-Jin email: sjpark@inha.ac.kr, psjin@krict.re.kr organization: Department of Chemistry, Inha University, 100 Inharo, Incheon 402-751, Republic of Korea – sequence: 9 givenname: Hak-Yong surname: Kim fullname: Kim, Hak-Yong email: khy@jbnu.ac.kr organization: Department of BIN Fusion Technology, Chonbuk National University, Jeonju 561-756, Republic of Korea |
| BackLink | https://www.kci.go.kr/kciportal/ci/sereArticleSearch/ciSereArtiView.kci?sereArticleSearchBean.artiId=ART001929842$$DAccess content in National Research Foundation of Korea (NRF) |
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| Keywords | Electrospinning Poly(vinyl alcohol) Graphene oxide Chitosan Nanofibers Biomaterials |
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| Snippet | Poly(vinyl alcohol) (PVA)/chitosan (CS)/graphene oxide (GO) biocomposite nanofibers have been successfully prepared using aqueous solution by electrospinning.... Poly(vinyl alcohol) (PVA)/chitosan (CS)/graphene oxide (GO) biocomposite nanofibers have beensuccessfully prepared using aqueous solution by electrospinning.... |
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| SubjectTerms | Biomaterials Chitosan Electrospinning Graphene oxide Nanofibers Poly(vinyl alcohol) 화학공학 |
| Title | Facile preparation and characterization of poly(vinyl alcohol)/chitosan/graphene oxide biocomposite nanofibers |
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