Polymerization-induced self-assembly of acrylonitrile via ICAR ATRP

Polymerization-induced self-assembly (PISA) has attracted growing interest as facile fabrication process of polymer-based nanomaterials. However, PISA of acrylonitrile (AN) by atom transfer radical polymerization (ATRP) has remained an outstanding challenge due to the high activity of AN and poor so...

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Published inPolymer (Guilford) Vol. 129; pp. 57 - 67
Main Authors Wang, Guowei, Wang, Zongyu, Lee, Bongjoon, Yuan, Rui, Lu, Zhao, Yan, Jiajun, Pan, Xiangcheng, Song, Yang, Bockstaller, Michael R., Matyjaszewski, Krzysztof
Format Journal Article
LanguageEnglish
Published Kidlington Elsevier Ltd 27.10.2017
Elsevier BV
Subjects
Acrylonitrile
ATRP
Chemical precipitation
Chemical synthesis
Esterification
Ethylene oxide
Fabrication
Initiators
Molecular structure
Molecular weight
Nanomaterials
Nanotechnology
PISA
Polyacrylonitrile
Polyethylene oxide
Polymerization
Polymers
Regeneration
Self-assembly
Acrylonitrile
PISA
ATRP
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Abstract Polymerization-induced self-assembly (PISA) has attracted growing interest as facile fabrication process of polymer-based nanomaterials. However, PISA of acrylonitrile (AN) by atom transfer radical polymerization (ATRP) has remained an outstanding challenge due to the high activity of AN and poor solubility of polyacrylonitrile (PAN) in AN monomer. Here the application of PISA by using an initiators for continuous activator regeneration (ICAR) ATRP for the synthesis of PAN-based nano-objects is demonstrated. A highly active ATRP macroinitiator, methoxy-poly(ethylene oxide) 2-bromo-2-phenylacetate (mPEO-BPA) was synthesized by esterification and used also as a stabilizer. The molecular weight of the macroinitiator was found to determine the structure of self-assembled nano-objects. The high molecular macroinitiator (mPEO113-BPA) formed nano-objects with spherical or worm-like morphology, while the lower molecular weight analogue (mPEO45-BPA) resulted in precipitation in most cases due to insufficient stabilization of the nano-objects. [Display omitted] •Polymerization-induced self-assembly (PISA) of acrylonitrile (AN) successfully accomplished by atom transfer radical polymerization (ATRP).•Initiators for continuous activator regeneration (ICAR) ATRP with low ppm Cu used for synthesis of PAN-based nano-objects demonstrated.•A highly active ATRP macroinitiator, mPEO-BPA was used as both macroinitiator and stabilizer.•The molecular weight of the macroinitiator determined the structure of self-assembled objects.
AbstractList Polymerization-induced self-assembly (PISA) has attracted growing interest as facile fabrication process of polymer-based nanomaterials. However, PISA of acrylonitrile (AN) by atom transfer radical polymerization (ATRP) has remained an outstanding challenge due to the high activity of AN and poor solubility of polyacrylonitrile (PAN) in AN monomer. Here the application of PISA by using an initiators for continuous activator regeneration (ICAR) ATRP for the synthesis of PAN-based nano-objects is demonstrated. A highly active ATRP macroinitiator, methoxy-poly(ethylene oxide) 2-bromo-2-phenylacetate (mPEO-BPA) was synthesized by esterification and used also as a stabilizer. The molecular weight of the macroinitiator was found to determine the structure of self-assembled nano-objects. The high molecular macroinitiator (mPEO113-BPA) formed nano-objects with spherical or worm-like morphology, while the lower molecular weight analogue (mPEO45-BPA) resulted in precipitation in most cases due to insufficient stabilization of the nano-objects.
Polymerization-induced self-assembly (PISA) has attracted growing interest as facile fabrication process of polymer-based nanomaterials. However, PISA of acrylonitrile (AN) by atom transfer radical polymerization (ATRP) has remained an outstanding challenge due to the high activity of AN and poor solubility of polyacrylonitrile (PAN) in AN monomer. Here the application of PISA by using an initiators for continuous activator regeneration (ICAR) ATRP for the synthesis of PAN-based nano-objects is demonstrated. A highly active ATRP macroinitiator, methoxy-poly(ethylene oxide) 2-bromo-2-phenylacetate (mPEO-BPA) was synthesized by esterification and used also as a stabilizer. The molecular weight of the macroinitiator was found to determine the structure of self-assembled nano-objects. The high molecular macroinitiator (mPEO113-BPA) formed nano-objects with spherical or worm-like morphology, while the lower molecular weight analogue (mPEO45-BPA) resulted in precipitation in most cases due to insufficient stabilization of the nano-objects. [Display omitted] •Polymerization-induced self-assembly (PISA) of acrylonitrile (AN) successfully accomplished by atom transfer radical polymerization (ATRP).•Initiators for continuous activator regeneration (ICAR) ATRP with low ppm Cu used for synthesis of PAN-based nano-objects demonstrated.•A highly active ATRP macroinitiator, mPEO-BPA was used as both macroinitiator and stabilizer.•The molecular weight of the macroinitiator determined the structure of self-assembled objects.
Author Bockstaller, Michael R.
Matyjaszewski, Krzysztof
Wang, Guowei
Yuan, Rui
Song, Yang
Wang, Zongyu
Lu, Zhao
Pan, Xiangcheng
Lee, Bongjoon
Yan, Jiajun
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  givenname: Zongyu
  surname: Wang
  fullname: Wang, Zongyu
  organization: Department of Chemistry, Carnegie Mellon University, 4400 Fifth Avenue, Pittsburgh, PA 15213, United States
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  surname: Lee
  fullname: Lee, Bongjoon
  organization: Department of Materials Science & Engineering, Carnegie Mellon University, 5000 Forbes Avenue, Pittsburgh, PA 15213, United States
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  surname: Yuan
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  organization: Department of Chemistry, Carnegie Mellon University, 4400 Fifth Avenue, Pittsburgh, PA 15213, United States
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  givenname: Zhao
  surname: Lu
  fullname: Lu, Zhao
  organization: Department of Materials Science & Engineering, Carnegie Mellon University, 5000 Forbes Avenue, Pittsburgh, PA 15213, United States
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  givenname: Jiajun
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  fullname: Yan, Jiajun
  organization: Department of Chemistry, Carnegie Mellon University, 4400 Fifth Avenue, Pittsburgh, PA 15213, United States
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  surname: Pan
  fullname: Pan, Xiangcheng
  organization: Department of Chemistry, Carnegie Mellon University, 4400 Fifth Avenue, Pittsburgh, PA 15213, United States
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  organization: Department of Chemistry, Carnegie Mellon University, 4400 Fifth Avenue, Pittsburgh, PA 15213, United States
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  givenname: Michael R.
  surname: Bockstaller
  fullname: Bockstaller, Michael R.
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  givenname: Krzysztof
  orcidid: 0000-0003-1960-3402
  surname: Matyjaszewski
  fullname: Matyjaszewski, Krzysztof
  email: km3b@andrew.cmu.edu
  organization: Department of Chemistry, Carnegie Mellon University, 4400 Fifth Avenue, Pittsburgh, PA 15213, United States
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Snippet Polymerization-induced self-assembly (PISA) has attracted growing interest as facile fabrication process of polymer-based nanomaterials. However, PISA of...
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SubjectTerms Acrylonitrile
ATRP
Chemical precipitation
Chemical synthesis
Esterification
Ethylene oxide
Fabrication
Initiators
Molecular structure
Molecular weight
Nanomaterials
Nanotechnology
PISA
Polyacrylonitrile
Polyethylene oxide
Polymerization
Polymers
Regeneration
Self-assembly
Title Polymerization-induced self-assembly of acrylonitrile via ICAR ATRP
URI https://dx.doi.org/10.1016/j.polymer.2017.09.029
https://www.proquest.com/docview/1966850902
Volume 129
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