Ultrathin g-C3N4 with enriched surface carbon vacancies enables highly efficient photocatalytic nitrogen fixation
[Display omitted] An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling methods. Its composition, morphological characteristics, surface defect types and electrochemical properties have been measured. After atomic scale...
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| Published in | Journal of colloid and interface science Vol. 553; pp. 530 - 539 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Inc
01.10.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling methods. Its composition, morphological characteristics, surface defect types and electrochemical properties have been measured. After atomic scale structure control and surface defects construction, the photocatalytic activity of prepared g-C3N4-V for ammonia conversion from dinitrogen can be greatly improved in contrast with bulk g-C3N4. Under visible light irradiation, the defective g-C3N4-V can produce 54 µmol/L NH3 within 100 min without any cocatalyst and sacrificial agent. The relationship between morphology characteristics and activity of defective ultrathin g-C3N4 materials was analyzed in detail. Benefiting from thin layer structure and more surface carbon vacancies, the effective charge separation from both bulk and surface can be achieved. Notably, the engineered carbon vacancies greatly facilitate the adsorption and activation of dinitrogen molecule, extremely improving the nitrogen fixation activity for the defective ultrathin g-C3N4-V materials. This work affords novel insights into the design of photocatalyst with defective ultrathin structure towards nitrogen fixation. |
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| AbstractList | An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling methods. Its composition, morphological characteristics, surface defect types and electrochemical properties have been measured. After atomic scale structure control and surface defects construction, the photocatalytic activity of prepared g-C₃N₄-V for ammonia conversion from dinitrogen can be greatly improved in contrast with bulk g-C₃N₄. Under visible light irradiation, the defective g-C₃N₄-V can produce 54 µmol/L NH₃ within 100 min without any cocatalyst and sacrificial agent. The relationship between morphology characteristics and activity of defective ultrathin g-C₃N₄ materials was analyzed in detail. Benefiting from thin layer structure and more surface carbon vacancies, the effective charge separation from both bulk and surface can be achieved. Notably, the engineered carbon vacancies greatly facilitate the adsorption and activation of dinitrogen molecule, extremely improving the nitrogen fixation activity for the defective ultrathin g-C₃N₄-V materials. This work affords novel insights into the design of photocatalyst with defective ultrathin structure towards nitrogen fixation. [Display omitted] An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling methods. Its composition, morphological characteristics, surface defect types and electrochemical properties have been measured. After atomic scale structure control and surface defects construction, the photocatalytic activity of prepared g-C3N4-V for ammonia conversion from dinitrogen can be greatly improved in contrast with bulk g-C3N4. Under visible light irradiation, the defective g-C3N4-V can produce 54 µmol/L NH3 within 100 min without any cocatalyst and sacrificial agent. The relationship between morphology characteristics and activity of defective ultrathin g-C3N4 materials was analyzed in detail. Benefiting from thin layer structure and more surface carbon vacancies, the effective charge separation from both bulk and surface can be achieved. Notably, the engineered carbon vacancies greatly facilitate the adsorption and activation of dinitrogen molecule, extremely improving the nitrogen fixation activity for the defective ultrathin g-C3N4-V materials. This work affords novel insights into the design of photocatalyst with defective ultrathin structure towards nitrogen fixation. An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling methods. Its composition, morphological characteristics, surface defect types and electrochemical properties have been measured. After atomic scale structure control and surface defects construction, the photocatalytic activity of prepared g-C3N4-V for ammonia conversion from dinitrogen can be greatly improved in contrast with bulk g-C3N4. Under visible light irradiation, the defective g-C3N4-V can produce 54 µmol/L NH3 within 100 min without any cocatalyst and sacrificial agent. The relationship between morphology characteristics and activity of defective ultrathin g-C3N4 materials was analyzed in detail. Benefiting from thin layer structure and more surface carbon vacancies, the effective charge separation from both bulk and surface can be achieved. Notably, the engineered carbon vacancies greatly facilitate the adsorption and activation of dinitrogen molecule, extremely improving the nitrogen fixation activity for the defective ultrathin g-C3N4-V materials. This work affords novel insights into the design of photocatalyst with defective ultrathin structure towards nitrogen fixation.An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling methods. Its composition, morphological characteristics, surface defect types and electrochemical properties have been measured. After atomic scale structure control and surface defects construction, the photocatalytic activity of prepared g-C3N4-V for ammonia conversion from dinitrogen can be greatly improved in contrast with bulk g-C3N4. Under visible light irradiation, the defective g-C3N4-V can produce 54 µmol/L NH3 within 100 min without any cocatalyst and sacrificial agent. The relationship between morphology characteristics and activity of defective ultrathin g-C3N4 materials was analyzed in detail. Benefiting from thin layer structure and more surface carbon vacancies, the effective charge separation from both bulk and surface can be achieved. Notably, the engineered carbon vacancies greatly facilitate the adsorption and activation of dinitrogen molecule, extremely improving the nitrogen fixation activity for the defective ultrathin g-C3N4-V materials. This work affords novel insights into the design of photocatalyst with defective ultrathin structure towards nitrogen fixation. |
| Author | Xia, Jiexiang Ding, Penghui Chen, Xiaoliu Li, Huaming Zhang, Yi Di, Jun Zhao, Junze Yan, Cheng Yin, Sheng Gu, Kaizhi |
| Author_xml | – sequence: 1 givenname: Yi surname: Zhang fullname: Zhang, Yi organization: School of Chemistry and Chemical Engineering, Institute for Energy Research, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, PR China – sequence: 2 givenname: Jun orcidid: 0000-0001-7890-9319 surname: Di fullname: Di, Jun organization: Center for Programmable Materials, School of Materials Science & Engineering, Nanyang Technological University, Singapore 639798, Singapore – sequence: 3 givenname: Penghui surname: Ding fullname: Ding, Penghui organization: School of Chemistry and Chemical Engineering, Institute for Energy Research, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, PR China – sequence: 4 givenname: Junze surname: Zhao fullname: Zhao, Junze organization: School of Chemistry and Chemical Engineering, Institute for Energy Research, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, PR China – sequence: 5 givenname: Kaizhi surname: Gu fullname: Gu, Kaizhi organization: School of Chemistry and Molecular Engineering, East China University of Science and Technology, Shanghai 200237, PR China – sequence: 6 givenname: Xiaoliu surname: Chen fullname: Chen, Xiaoliu organization: School of Chemistry and Chemical Engineering, Institute for Energy Research, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, PR China – sequence: 7 givenname: Cheng orcidid: 0000-0002-6232-6466 surname: Yan fullname: Yan, Cheng organization: Center for Programmable Materials, School of Materials Science & Engineering, Nanyang Technological University, Singapore 639798, Singapore – sequence: 8 givenname: Sheng surname: Yin fullname: Yin, Sheng organization: School of Chemistry and Chemical Engineering, Institute for Energy Research, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, PR China – sequence: 9 givenname: Jiexiang orcidid: 0000-0002-7394-1130 surname: Xia fullname: Xia, Jiexiang email: xjx@ujs.edu.cn organization: School of Chemistry and Chemical Engineering, Institute for Energy Research, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, PR China – sequence: 10 givenname: Huaming orcidid: 0000-0002-7875-4318 surname: Li fullname: Li, Huaming email: lhm@ujs.edu.cn organization: School of Chemistry and Chemical Engineering, Institute for Energy Research, Jiangsu University, 301 Xuefu Road, Zhenjiang 212013, PR China |
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An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling... An ultra-thin carbon nitride with loose structure and more carbon defects on the surface was achieved through high-temperature peeling methods. Its... |
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| SubjectTerms | adsorption ammonia carbon carbon nitride Carbon vacancies electrochemistry g-C3N4 irradiation light nitrogen Nitrogen fixation peeling photocatalysis photocatalysts Photocatalytic |
| Title | Ultrathin g-C3N4 with enriched surface carbon vacancies enables highly efficient photocatalytic nitrogen fixation |
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