Ultrasound-Assisted Synthesis of High-Entropy Materials for Enhanced Oxygen Evolution Electrocatalysis
High-entropy materials (HEMs) play a significant role in the electrocatalytic oxygen evolution reaction (OER) due to their unique properties. However, there are still challenges in the preparation of HEMs for OER catalysts. In this study, the FeCoNiMnCr catalyst is synthesized for the first time usi...
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| Published in | Metals (Basel ) Vol. 14; no. 4; p. 384 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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MDPI AG
01.04.2024
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| ISSN | 2075-4701 2075-4701 |
| DOI | 10.3390/met14040384 |
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| Abstract | High-entropy materials (HEMs) play a significant role in the electrocatalytic oxygen evolution reaction (OER) due to their unique properties. However, there are still challenges in the preparation of HEMs for OER catalysts. In this study, the FeCoNiMnCr catalyst is synthesized for the first time using the ultrasonic hydrothermal-sintering technique and exhibits excellent performance for OER electrocatalysis. There is an optimal ultrasonic hydrothermal time and power for achieving the best OER performance. The results demonstrate that the performance of FeCoNiMnCr catalysts prepared through ultrasonic hydrothermal sintering (US-FeCoNiMnCr) is significantly improved compared with the traditional hydrothermal-sintering method. The US-FeCoNiMnCr catalyst exhibits an overpotential of 228 mV at the current density of 10 mA cm−2 and a Tafel slope as low as 45.39 mV dec−1 in an alkaline medium. Moreover, the US-FeCoNiMnCr catalyst demonstrates remarkable stability in electrocatalytic OER with a minimal potential increase observed even after 48 h. This work not only provides valuable insights into high-entropy material synthesis, but also presents a powerful electrocatalyst for water electrolysis. |
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| AbstractList | High-entropy materials (HEMs) play a significant role in the electrocatalytic oxygen evolution reaction (OER) due to their unique properties. However, there are still challenges in the preparation of HEMs for OER catalysts. In this study, the FeCoNiMnCr catalyst is synthesized for the first time using the ultrasonic hydrothermal-sintering technique and exhibits excellent performance for OER electrocatalysis. There is an optimal ultrasonic hydrothermal time and power for achieving the best OER performance. The results demonstrate that the performance of FeCoNiMnCr catalysts prepared through ultrasonic hydrothermal sintering (US-FeCoNiMnCr) is significantly improved compared with the traditional hydrothermal-sintering method. The US-FeCoNiMnCr catalyst exhibits an overpotential of 228 mV at the current density of 10 mA cm−2 and a Tafel slope as low as 45.39 mV dec−1 in an alkaline medium. Moreover, the US-FeCoNiMnCr catalyst demonstrates remarkable stability in electrocatalytic OER with a minimal potential increase observed even after 48 h. This work not only provides valuable insights into high-entropy material synthesis, but also presents a powerful electrocatalyst for water electrolysis. High-entropy materials (HEMs) play a significant role in the electrocatalytic oxygen evolution reaction (OER) due to their unique properties. However, there are still challenges in the preparation of HEMs for OER catalysts. In this study, the FeCoNiMnCr catalyst is synthesized for the first time using the ultrasonic hydrothermal-sintering technique and exhibits excellent performance for OER electrocatalysis. There is an optimal ultrasonic hydrothermal time and power for achieving the best OER performance. The results demonstrate that the performance of FeCoNiMnCr catalysts prepared through ultrasonic hydrothermal sintering (US-FeCoNiMnCr) is significantly improved compared with the traditional hydrothermal-sintering method. The US-FeCoNiMnCr catalyst exhibits an overpotential of 228 mV at the current density of 10 mA cm[sup.−2] and a Tafel slope as low as 45.39 mV dec[sup.−1] in an alkaline medium. Moreover, the US-FeCoNiMnCr catalyst demonstrates remarkable stability in electrocatalytic OER with a minimal potential increase observed even after 48 h. This work not only provides valuable insights into high-entropy material synthesis, but also presents a powerful electrocatalyst for water electrolysis. |
| Audience | Academic |
| Author | Hu, Jue Zhang, Yue Wang, Zhiyuan Zhang, Chengxu |
| Author_xml | – sequence: 1 givenname: Zhiyuan surname: Wang fullname: Wang, Zhiyuan – sequence: 2 givenname: Chengxu surname: Zhang fullname: Zhang, Chengxu – sequence: 3 givenname: Yue surname: Zhang fullname: Zhang, Yue – sequence: 4 givenname: Jue surname: Hu fullname: Hu, Jue |
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| CitedBy_id | crossref_primary_10_1016_j_apcata_2024_119851 crossref_primary_10_1002_slct_202401953 crossref_primary_10_1016_j_jallcom_2025_178833 crossref_primary_10_1016_j_ccr_2025_216435 |
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| Snippet | High-entropy materials (HEMs) play a significant role in the electrocatalytic oxygen evolution reaction (OER) due to their unique properties. However, there... |
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| SubjectTerms | Alloys Carbon Catalysis Catalysts Cavitation Chemical synthesis Clean technology Efficiency Electrocatalysis Electrocatalysts Electrolysis Energy consumption Entropy Fossil fuels Green technology high-entropy materials Hydrogen Hydrogen as fuel in situ Raman Intermetallic compounds Microscopy Nanoparticles oxygen evolution reaction Oxygen evolution reactions Sintering Temperature ultrasonic hydrothermal-sintering method Ultrasonic imaging |
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| Title | Ultrasound-Assisted Synthesis of High-Entropy Materials for Enhanced Oxygen Evolution Electrocatalysis |
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