Embrittlement of the martensitic steel 91 tested in liquid lead

Two potential problems are encountered in the case of intimate contact between liquid metals and metallic substrates: grain boundary wetting and liquid metal embrittlement (LME) which both induce a degradation of the mechanical properties. Tensile tests were carried out on a 9% Cr 1% Mo martensitic...

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Published inJournal of nuclear materials Vol. 296; no. 1; pp. 256 - 264
Main Authors Nicaise, G, Legris, A, Vogt, J.B, Foct, J
Format Journal Article Conference Proceeding
LanguageEnglish
Published Amsterdam Elsevier B.V 01.07.2001
Elsevier
Subjects
Applied sciences
Chemical Sciences
Exact sciences and technology
Fractures
Mechanical properties and methods of testing. Rheology. Fracture mechanics. Tribology
Metals. Metallurgy
S06
M03
C08
L03
Alloy steel
Martensitic steel
Molten metal attack
Rupture
Lead
Mechanical properties
Tensile property
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Abstract Two potential problems are encountered in the case of intimate contact between liquid metals and metallic substrates: grain boundary wetting and liquid metal embrittlement (LME) which both induce a degradation of the mechanical properties. Tensile tests were carried out on a 9% Cr 1% Mo martensitic (Grade 91) steel in a liquid lead environment at temperatures ranging between 623 and 773 K. The Grade 91 steel was submitted to heat treatments in order to modify its hardness and also to produce either ferritic or martensitic grains. Smooth and notched specimens were used. We found out that by combining adapted heat treatments and the notch effect, it is possible to create conditions severe enough that lead to LME. Our experimental observations (transgranular failure) are compatible with the expectations of traditional mechanisms based on a reduction of the surface energy and/or adsorption induced chemical bond softening at the steel surface in contact with liquid lead.
AbstractList Two potential problems are encountered in the case of intimate contact between liquid metals and metallic substrates: grain boundary wetting and liquid metal embrittlement (LME) which both induce a degradation of the mechanical properties. Tensile tests were carried out on a 9% Cr 1% Mo martensitic (Grade 91) steel in a liquid lead environment at temperatures ranging between 623 and 773 K. The Grade 91 steel was submitted to heat treatments in order to modify its hardness and also to produce either ferritic or martensitic grains. Smooth and notched specimens were used. We found out that by combining adapted heat treatments and the notch effect, it is possible to create conditions severe enough that lead to LME. Our experimental observations (transgranular failure) are compatible with the expectations of traditional mechanisms based on a reduction of the surface energy and/or adsorption induced chemical bond softening at the steel surface in contact with liquid lead.
Author Legris, A
Foct, J
Nicaise, G
Vogt, J.B
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Issue 1
Keywords S06
M03
C08
L03
Alloy steel
Martensitic steel
Molten metal attack
Rupture
Lead
Mechanical properties
Tensile property
Language English
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  year: 1999
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  publication-title: Eur. Phys. J. A.P.
  doi: 10.1051/epjap:1999108
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  start-page: 2553
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  ident: 10.1016/S0022-3115(01)00525-6_BIB11
  publication-title: AIME Trans.
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Snippet Two potential problems are encountered in the case of intimate contact between liquid metals and metallic substrates: grain boundary wetting and liquid metal...
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SubjectTerms Applied sciences
Chemical Sciences
Exact sciences and technology
Fractures
Mechanical properties and methods of testing. Rheology. Fracture mechanics. Tribology
Metals. Metallurgy
Title Embrittlement of the martensitic steel 91 tested in liquid lead
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