Effect of thienyl units in cyanoacrylic acid derivatives toward dye-sensitized solar cells
A series of heterocyclic donor-acceptor systems were synthesized and well characterized by using 1H, 13C NMR, FT-IR, and elemental analysis. They were designed to investigate the effect of thiophene and cyanoacrylic acid number units on the thermal, optical, electrochemical and finally photovoltaic...
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Published in | Journal of photochemistry and photobiology. B, Biology Vol. 197; p. 111555 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
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Switzerland
Elsevier B.V
01.08.2019
Elsevier BV |
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Abstract | A series of heterocyclic donor-acceptor systems were synthesized and well characterized by using 1H, 13C NMR, FT-IR, and elemental analysis. They were designed to investigate the effect of thiophene and cyanoacrylic acid number units on the thermal, optical, electrochemical and finally photovoltaic properties of dye-sensitized solar cells prepared with the selected compounds. The effect of chemical structure on their properties was demonstrated. They showed the beginning of thermal decomposition between 230 and 270 °C. The compounds absorbed the radiation in the range of 300–500 nm or 200–400 nm. They were electrochemically active and varied in energy band gap from 3.40 to 1.58 eV. Additionally, their optimized geometry, HOMO–LUMO levels, ionization potential, and electron affinity were evaluated using density functional theory. The photovoltaic devices based on TiO2 sensitized with the obtained molecules exhibited low power conversion efficiency, which was the highest for the device containing the symmetrical molecule with bithiophene structure. Under co-sensitization, the cell made of the same compound gave significant enhancement of efficiency of 6.3% being higher to that of the individual device prepared from dye N719 (5.75%). Moreover, the effects of immersion time of TiO2 electrode in the dye solution and co-sensitization methods were tested. The surface morphology of photoanode was investigated using atomic force microscopy.
[Display omitted]
•A series of cyanoacrylic acid derivatives with thienyl units were synthesized.•The effect of chemical structure on their properties was demonstrated.•The selected compounds were tested in dye-sensitized solar cells.•The highest PCE exhibited cell with symmetrical molecule contains bithiophene core.•Co-sensitization enhanced efficiency to 6.3% being higher than with a neat N719. |
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AbstractList | A series of heterocyclic donor-acceptor systems were synthesized and well characterized by using
H,
C NMR, FT-IR, and elemental analysis. They were designed to investigate the effect of thiophene and cyanoacrylic acid number units on the thermal, optical, electrochemical and finally photovoltaic properties of dye-sensitized solar cells prepared with the selected compounds. The effect of chemical structure on their properties was demonstrated. They showed the beginning of thermal decomposition between 230 and 270 °C. The compounds absorbed the radiation in the range of 300-500 nm or 200-400 nm. They were electrochemically active and varied in energy band gap from 3.40 to 1.58 eV. Additionally, their optimized geometry, HOMO-LUMO levels, ionization potential, and electron affinity were evaluated using density functional theory. The photovoltaic devices based on TiO
sensitized with the obtained molecules exhibited low power conversion efficiency, which was the highest for the device containing the symmetrical molecule with bithiophene structure. Under co-sensitization, the cell made of the same compound gave significant enhancement of efficiency of 6.3% being higher to that of the individual device prepared from dye N719 (5.75%). Moreover, the effects of immersion time of TiO
electrode in the dye solution and co-sensitization methods were tested. The surface morphology of photoanode was investigated using atomic force microscopy. A series of heterocyclic donor-acceptor systems were synthesized and well characterized by using 1H, 13C NMR, FT-IR, and elemental analysis. They were designed to investigate the effect of thiophene and cyanoacrylic acid number units on the thermal, optical, electrochemical and finally photovoltaic properties of dye-sensitized solar cells prepared with the selected compounds. The effect of chemical structure on their properties was demonstrated. They showed the beginning of thermal decomposition between 230 and 270 °C. The compounds absorbed the radiation in the range of 300–500 nm or 200–400 nm. They were electrochemically active and varied in energy band gap from 3.40 to 1.58 eV. Additionally, their optimized geometry, HOMO–LUMO levels, ionization potential, and electron affinity were evaluated using density functional theory. The photovoltaic devices based on TiO2 sensitized with the obtained molecules exhibited low power conversion efficiency, which was the highest for the device containing the symmetrical molecule with bithiophene structure. Under co-sensitization, the cell made of the same compound gave significant enhancement of efficiency of 6.3% being higher to that of the individual device prepared from dye N719 (5.75%). Moreover, the effects of immersion time of TiO2 electrode in the dye solution and co-sensitization methods were tested. The surface morphology of photoanode was investigated using atomic force microscopy. A series of heterocyclic donor-acceptor systems were synthesized and well characterized by using 1H, 13C NMR, FT-IR, and elemental analysis. They were designed to investigate the effect of thiophene and cyanoacrylic acid number units on the thermal, optical, electrochemical and finally photovoltaic properties of dye-sensitized solar cells prepared with the selected compounds. The effect of chemical structure on their properties was demonstrated. They showed the beginning of thermal decomposition between 230 and 270 °C. The compounds absorbed the radiation in the range of 300–500 nm or 200–400 nm. They were electrochemically active and varied in energy band gap from 3.40 to 1.58 eV. Additionally, their optimized geometry, HOMO–LUMO levels, ionization potential, and electron affinity were evaluated using density functional theory. The photovoltaic devices based on TiO2 sensitized with the obtained molecules exhibited low power conversion efficiency, which was the highest for the device containing the symmetrical molecule with bithiophene structure. Under co-sensitization, the cell made of the same compound gave significant enhancement of efficiency of 6.3% being higher to that of the individual device prepared from dye N719 (5.75%). Moreover, the effects of immersion time of TiO2 electrode in the dye solution and co-sensitization methods were tested. The surface morphology of photoanode was investigated using atomic force microscopy. [Display omitted] •A series of cyanoacrylic acid derivatives with thienyl units were synthesized.•The effect of chemical structure on their properties was demonstrated.•The selected compounds were tested in dye-sensitized solar cells.•The highest PCE exhibited cell with symmetrical molecule contains bithiophene core.•Co-sensitization enhanced efficiency to 6.3% being higher than with a neat N719. |
ArticleNumber | 111555 |
Author | Schab-Balcerzak, Ewa Bujak, Karolina Gnida, Paweł Fabiańczyk, Aleksandra Kula, Sławomir Szlapa-Kula, Agata Libera, Marcin Siwy, Mariola |
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BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31326844$$D View this record in MEDLINE/PubMed |
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Keywords | Thiophene derivatives Dye-sensitized solar cells (DSSCs) Cyanoacrylic acid derivatives Knoevenagel condensation |
Language | English |
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Snippet | A series of heterocyclic donor-acceptor systems were synthesized and well characterized by using 1H, 13C NMR, FT-IR, and elemental analysis. They were designed... A series of heterocyclic donor-acceptor systems were synthesized and well characterized by using H, C NMR, FT-IR, and elemental analysis. They were designed to... |
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SubjectTerms | Acids Atomic force microscopy Chemical analysis Chemical compounds Coloring Agents - chemistry Cyanoacrylates - chemical synthesis Cyanoacrylates - chemistry Cyanoacrylic acid derivatives Density Functional Theory Dye-sensitized solar cells Dye-sensitized solar cells (DSSCs) Dyes Electric Power Supplies Electrochemistry Electron affinity Energy conversion efficiency Energy gap Infrared analysis Ionization Ionization potentials Knoevenagel condensation Microscopy Microscopy, Atomic Force Molecular orbitals Molecular structure Morphology NMR Nuclear magnetic resonance Optical properties Organic chemistry Oxidation-Reduction Photovoltaic cells Photovoltaics Solar cells Solar Energy Submerging Thermal decomposition Thiophene derivatives Titanium - chemistry Titanium dioxide |
Title | Effect of thienyl units in cyanoacrylic acid derivatives toward dye-sensitized solar cells |
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