Influence of wall number and surface functionalization of carbon nanotubes on their antioxidant behavior in high density polyethylene
Carbon nanotubes (CNTs) are extensively incorporated as reinforcement into polymeric materials due to their extraordinary properties. The antioxidant ability of CNTs in high density polyethylene (HDPE) was studied. Single-walled carbon nanotubes (SWCNTs), multi-walled carbon nanotubes (MWCNTs), and...
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| Published in | Carbon (New York) Vol. 50; no. 3; pp. 1005 - 1013 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
01.03.2012
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Carbon nanotubes (CNTs) are extensively incorporated as reinforcement into polymeric materials due to their extraordinary properties. The antioxidant ability of CNTs in high density polyethylene (HDPE) was studied. Single-walled carbon nanotubes (SWCNTs), multi-walled carbon nanotubes (MWCNTs), and hydroxylated multi-walled carbon nanotubes (MWCNTs-OH) were involved to investigate the influence of wall number and surface functionalization of CNTs on their antioxidant behavior in HDPE. Based on measurements of the oxidation induction temperature and oxidation induction time of CNT/HDPE composites, it is found that the antioxidant ability of the three kinds of CNTs is in the following order: MWCNTs-OH
>
MWCNTs
>
SWCNTs. The antioxidant ability and mechanism of CNTs are further examined by electron spin resonance spectra and Raman spectra. It is observed that the antioxidant behavior of CNTs obeys a free radical scavenging mechanism. The order of the radical scavenging efficiency and the defect concentration for CNTs are in good agreement with that of their antioxidant ability in HDPE. With more walls and surface hydroxyl groups, the CNTs have more structural defects and exhibit higher antioxidant ability. The study raises the possibility that CNTs can improve antioxidant properties as well as mechanical properties of polymer matrix. |
|---|---|
| AbstractList | Carbon nanotubes (CNTs) are extensively incorporated as reinforcement into polymeric materials due to their extraordinary properties. The antioxidant ability of CNTs in high density polyethylene (HDPE) was studied. Single-walled carbon nanotubes (SWCNTs), multi-walled carbon nanotubes (MWCNTs), and hydroxylated multi-walled carbon nanotubes (MWCNTs-OH) were involved to investigate the influence of wall number and surface functionalization of CNTs on their antioxidant behavior in HDPE. Based on measurements of the oxidation induction temperature and oxidation induction time of CNT/HDPE composites, it is found that the antioxidant ability of the three kinds of CNTs is in the following order: MWCNTs-OH
>
MWCNTs
>
SWCNTs. The antioxidant ability and mechanism of CNTs are further examined by electron spin resonance spectra and Raman spectra. It is observed that the antioxidant behavior of CNTs obeys a free radical scavenging mechanism. The order of the radical scavenging efficiency and the defect concentration for CNTs are in good agreement with that of their antioxidant ability in HDPE. With more walls and surface hydroxyl groups, the CNTs have more structural defects and exhibit higher antioxidant ability. The study raises the possibility that CNTs can improve antioxidant properties as well as mechanical properties of polymer matrix. Carbon nanotubes (CNTs) are extensively incorporated as reinforcement into polymeric materials due to their extraordinary properties. The antioxidant ability of CNTs in high density polyethylene (HDPE) was studied. Single-walled carbon nanotubes (SWCNTs), multi-walled carbon nanotubes (MWCNTs), and hydroxylated multi-walled carbon nanotubes (MWCNTs-OH) were involved to investigate the influence of wall number and surface functionalization of CNTs on their antioxidant behavior in HDPE. Based on measurements of the oxidation induction temperature and oxidation induction time of CNT/HDPE composites, it is found that the antioxidant ability of the three kinds of CNTs is in the following order: MWCNTs-OH>MWCNTs>SWCNTs. The antioxidant ability and mechanism of CNTs are further examined by electron spin resonance spectra and Raman spectra. It is observed that the antioxidant behavior of CNTs obeys a free radical scavenging mechanism. The order of the radical scavenging efficiency and the defect concentration for CNTs are in good agreement with that of their antioxidant ability in HDPE. With more walls and surface hydroxyl groups, the CNTs have more structural defects and exhibit higher antioxidant ability. The study raises the possibility that CNTs can improve antioxidant properties as well as mechanical properties of polymer matrix. |
| Author | Jiang, Binbo Yang, Yongrong Wang, Jingdai Shi, Xiaomei |
| Author_xml | – sequence: 1 givenname: Xiaomei surname: Shi fullname: Shi, Xiaomei – sequence: 2 givenname: Binbo surname: Jiang fullname: Jiang, Binbo – sequence: 3 givenname: Jingdai surname: Wang fullname: Wang, Jingdai email: unilabzju@hotmail.com – sequence: 4 givenname: Yongrong surname: Yang fullname: Yang, Yongrong |
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| Keywords | Polyethylenes Free radicals Spin Carbon nanotubes Mechanical properties Raman spectroscopy Carbon Density Defects Singlewalled nanotube Composite materials Functionalization Multiwalled nanotube Efficiency Radical mechanism Hydroxyl group Oxidation Resonance Polymers Electrons |
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| SubjectTerms | antioxidant activity Antioxidants carbon Carbon nanotubes Cross-disciplinary physics: materials science; rheology electron paramagnetic resonance spectroscopy Exact sciences and technology free radical scavengers Fullerenes and related materials; diamonds, graphite High density Materials science mechanical properties Multi wall carbon nanotubes oxidation Physics polyethylene Polyethylenes Scavenging Single wall carbon nanotubes Specific materials temperature Walls |
| Title | Influence of wall number and surface functionalization of carbon nanotubes on their antioxidant behavior in high density polyethylene |
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