Sonoelectrochemical treatment of water polluted with trichloroacetic acid: From sonovoltammetry to pre-pilot plant scale

The sonoelectrochemical treatment of aqueous solutions of trichloroacetic acid (TCAA) has been scaled-up from the voltammetric analysis to pre-pilot stage. The degradation in absence of ultrasound field has yield to a poor performance which has been improved in presence of ultrasound. The sonovoltam...

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Published inUltrasonics sonochemistry Vol. 17; no. 6; pp. 1010 - 1020
Main Authors Esclapez, M.D., Sáez, V., Milán-Yáñez, D., Tudela, I., Louisnard, O., González-García, J.
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 01.08.2010
Elsevier
Subjects
Cavitation
Current distribution
Electrocatalysis
Electrochemistry
Engineering Sciences
Feasibility Studies
Fluid flow
Green Chemistry Technology
Pilot Projects
Sonication - economics
Sonication - methods
Trichloroacetic Acid - chemistry
Trichloroacetic Acid - isolation & purification
Ultrasound
Water - chemistry
Water Pollutants, Chemical - chemistry
Water Pollutants, Chemical - isolation & purification
Water Purification - economics
Water Purification - methods
DCAA
j w
PP
DE
ρ
D
E
F
E a
Fluid flow
I
UV-VIS
ω
I a
S-CV
Electrocatalysis
MCAA
S-LSV
S
d e-h
V
IC
THMs
Ultrasound
EC
HPLC
sono-LSV
П
CE
TCAA
R-CV
R-LSV
Cavitation
c l
LSV
E cw
p
α
CV
sono-CV
t
X-MBE
Electrochemistry
Current distribution
FC
Online AccessGet full text

Cover

Abstract The sonoelectrochemical treatment of aqueous solutions of trichloroacetic acid (TCAA) has been scaled-up from the voltammetric analysis to pre-pilot stage. The degradation in absence of ultrasound field has yield to a poor performance which has been improved in presence of ultrasound. The sonovoltametry study has provided the range of potentials and/or current densities to be used with the lowest current efficiency penalty. Sonoelectrolyses at batch scale (carried out with a horn-transducer 24 kHz positioned at about 3 cm from the surface of the electrode) achieved little improvement in the degradation. However, when a specifically designed sonoelectrochemical reactor (not optimized) was used during the scale-up, the presence of ultrasound field provided better results (fractional conversion 97%, degradation efficiency 26%, selectivity 0.92 and current efficiency 8%) at lower ultrasonic intensities and volumetric flow.
AbstractList The sonoelectrochemical treatment of aqueous solutions of trichloroacetic acid (TCAA) has been scaled-up from the voltammetric analysis to pre-pilot stage. The degradation in absence of ultrasound field has yield to a poor performance which has been improved in presence of ultrasound. The sonovoltametry study has provided the range of potentials and/or current densities to be used with the lowest current efficiency penalty. Sonoelectrolyses at batch scale (carried out with a horn-transducer 24 kHz positioned at about 3 cm from the surface of the electrode) achieved little improvement in the degradation. However, when a specifically designed sonoelectrochemical reactor (not optimized) was used during the scale-up, the presence of ultrasound field provided better results (fractional conversion 97%, degradation efficiency 26%, selectivity 0.92 and current efficiency 8%) at lower ultrasonic intensities and volumetric flow.
The sonoelectrochemical treatment of aqueous solutions of trichloroacetic acid (TCAA) has been scaled-up from the voltammetric analysis to pre-pilot stage. The degradation in absence of ultrasound field has yield to a poor performance which has been improved in presence of ultrasound. The sonovoltametry study has provided the range of potentials and/or current densities to be used with the lowest current efficiency penalty. Sonoelectrolyses at batch scale (carried out with a horn-transducer 24 kHz positioned at about 3 cm from the surface of the electrode) achieved little improvement in the degradation. However, when a specifically designed sonoelectrochemical reactor (not optimized) was used during the scale-up, the presence of ultrasound field provided better results (fractional conversion 97%, degradation efficiency 26%, selectivity 0.92 and current efficiency 8%) at lower ultrasonic intensities and volumetric flow.
Author Tudela, I.
Esclapez, M.D.
González-García, J.
Sáez, V.
Milán-Yáñez, D.
Louisnard, O.
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  givenname: J.
  surname: González-García
  fullname: González-García, J.
  email: jose.gonzalez@ua.es
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Issue 6
Keywords DCAA
j w
PP
DE
ρ
D
E
F
E a
Fluid flow
I
UV-VIS
ω
I a
S-CV
Electrocatalysis
MCAA
S-LSV
S
d e-h
V
IC
THMs
Ultrasound
EC
HPLC
sono-LSV
П
CE
TCAA
R-CV
R-LSV
Cavitation
c l
LSV
E cw
p
α
CV
sono-CV
t
X-MBE
Electrochemistry
Current distribution
FC
Language English
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Snippet The sonoelectrochemical treatment of aqueous solutions of trichloroacetic acid (TCAA) has been scaled-up from the voltammetric analysis to pre-pilot stage. The...
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SubjectTerms Cavitation
Current distribution
Electrocatalysis
Electrochemistry
Engineering Sciences
Feasibility Studies
Fluid flow
Green Chemistry Technology
Pilot Projects
Sonication - economics
Sonication - methods
Trichloroacetic Acid - chemistry
Trichloroacetic Acid - isolation & purification
Ultrasound
Water - chemistry
Water Pollutants, Chemical - chemistry
Water Pollutants, Chemical - isolation & purification
Water Purification - economics
Water Purification - methods
Title Sonoelectrochemical treatment of water polluted with trichloroacetic acid: From sonovoltammetry to pre-pilot plant scale
URI https://dx.doi.org/10.1016/j.ultsonch.2009.11.009
https://www.ncbi.nlm.nih.gov/pubmed/20022544
https://search.proquest.com/docview/733293478
https://hal.science/hal-01717674
Volume 17
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