Synthesis of TiO2 nanoparticles through the Gel Combustion process
Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost titanium precursor and hydrogen peroxide as combustible substance. The process led to a significant gas development and the as-synthesized nanopa...
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| Published in | Journal of materials science Vol. 43; no. 9; pp. 3274 - 3278 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.05.2008
Springer Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost titanium precursor and hydrogen peroxide as combustible substance. The process led to a significant gas development and the as-synthesized nanoparticles showed a low degree of crystallinity and mean dimension of 20 nm. Different thermal treatments were performed so as to investigate their effect on the structural properties and on the particle size of the synthesized products. The optimal temperature was set at 300 °C, giving pure anatase TiO₂ nanopowders with a good level of crystallinity, an average particle size of 50 nm and a high value of specific surface area. |
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| AbstractList | Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost titanium precursor and hydrogen peroxide as combustible substance. The process led to a significant gas development and the as-synthesized nanoparticles showed a low degree of crystallinity and mean dimension of 20 nm. Different thermal treatments were performed so as to investigate their effect on the structural properties and on the particle size of the synthesized products. The optimal temperature was set at 300 °C, giving pure anatase TiO₂ nanopowders with a good level of crystallinity, an average particle size of 50 nm and a high value of specific surface area. Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost titanium precursor and hydrogen peroxide as combustible substance. The process led to a significant gas development and the as-synthesized nanoparticles showed a low degree of crystallinity and mean dimension of 20 nm. Different thermal treatments were performed so as to investigate their effect on the structural properties and on the particle size of the synthesized products. The optimal temperature was set at 300 °C, giving pure anatase TiO2 nanopowders with a good level of crystallinity, an average particle size of 50 nm and a high value of specific surface area. Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost titanium precursor and hydrogen peroxide as combustible substance. The process led to a significant gas development and the as-synthesized nanoparticles showed a low degree of crystallinity and mean dimension of 20 nm. Different thermal treatments were performed so as to investigate their effect on the structural properties and on the particle size of the synthesized products. The optimal temperature was set at 300 °C, giving pure anatase TiO 2 nanopowders with a good level of crystallinity, an average particle size of 50 nm and a high value of specific surface area. Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost titanium precursor and hydrogen peroxide as combustible substance. The process led to a significant gas development and the as-synthesized nanoparticles showed a low degree of crystallinity and mean dimension of 20 nm. Different thermal treatments were performed so as to investigate their effect on the structural properties and on the particle size of the synthesized products. The optimal temperature was set at 300 deg C, giving pure anatase TiO2 nanopowders with a good level of crystallinity, an average particle size of 50 nm and a high value of specific surface area. |
| Author | Deorsola, F. A Vallauri, D |
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| Cites_doi | 10.1016/j.apcata.2004.04.003 10.1007/s10934-006-8022-5 10.1023/A:1026318712367 10.1016/S0167-577X(00)00246-9 10.1016/j.mseb.2006.11.011 10.1016/j.jeurceramsoc.2004.11.017 10.1016/S0921-5107(99)00152-X 10.1557/JMR.1988.1367 10.1016/S0926-3373(03)00124-3 10.1016/0021-9797(87)90018-X 10.1016/0142-9612(89)90019-7 10.1557/JMR.1995.2788 10.1007/s10853-007-1919-9 10.1038/325659a0 10.1016/S0167-577X(02)01376-9 10.1016/0965-9773(93)90048-G 10.1007/s12034-007-0046-1 10.1016/j.matlet.2003.08.032 10.3866/PKU.WHXB20050112 10.1002/1521-4095(200109)13:17<1301::AID-ADMA1301>3.0.CO;2-6 10.1016/S0965-9773(99)00046-X 10.1016/S1010-6030(97)00118-4 10.1038/nrc1566 |
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| Issue | 9 |
| Keywords | TiO2 Nanopowders Solution Combustion Synthesis Titanium Tetraisopropoxide Titanium Precursor TiO2 Scanning electron microscopy Combustion synthesis Inorganic compounds Word Oxides XRD Experimental study Ultrafine powder Heat treatments Titanium Oxides Nanoparticles Chemical preparation Gel growth |
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| Snippet | Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost... |
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| SubjectTerms | Anatase Characterization and Evaluation of Materials Chemical synthesis methods Chemistry and Materials Science Classical Mechanics Combustion Cross-disciplinary physics: materials science; rheology Crystal structure Crystallinity Crystallography and Scattering Methods Degree of crystallinity Exact sciences and technology Flammability heat treatment Hydrogen peroxide Materials Science Methods of nanofabrication Nanoparticles Nanopowders Nanoscale materials and structures: fabrication and characterization Particle size Physics Polymer Sciences Solid Mechanics surface area Synthesis temperature titanium Titanium dioxide |
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| Title | Synthesis of TiO2 nanoparticles through the Gel Combustion process |
| URI | https://link.springer.com/article/10.1007/s10853-008-2530-4 https://www.proquest.com/docview/2259654241 https://search.proquest.com/docview/32691649 |
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