Synthesis of TiO2 nanoparticles through the Gel Combustion process

• Published in: Journal of materials science Vol. 43; no. 9; pp. 3274 - 3278
• Main Authors: Deorsola, F. A, Vallauri, D
• Format: Journal Article
• Language: English
• Published: New York Springer US 01.05.2008; Springer; Springer Nature B.V
• Subjects: Anatase; Characterization and Evaluation of Materials; Chemical synthesis methods; Chemistry and Materials Science; Classical Mechanics; Combustion; Cross-disciplinary physics: materials science; rheology; Crystal structure; Crystallinity; Crystallography and Scattering Methods; Degree of crystallinity; Exact sciences and technology; Flammability; heat treatment; Hydrogen peroxide; Materials Science; Methods of nanofabrication; Nanoparticles; Nanopowders; Nanoscale materials and structures: fabrication and characterization; Particle size; Physics; Polymer Sciences; Solid Mechanics; surface area; Synthesis; temperature; titanium; Titanium dioxide; TiO2 Nanopowders; Solution Combustion Synthesis; Titanium Tetraisopropoxide; Titanium Precursor; TiO2; Scanning electron microscopy; Combustion synthesis; Inorganic compounds; Word; Oxides; XRD; Experimental study; Ultrafine powder; Heat treatments; Titanium Oxides; Nanoparticles; Chemical preparation; Gel growth
• ISSN: 0022-2461; 1573-4803
• DOI: 10.1007/s10853-008-2530-4

Nanosized titania particles have been synthesized through the Gel Combustion process. The synthesis was carried out by starting from a common and low-cost titanium precursor and hydrogen peroxide as combustible substance. The process led to a significant gas development and the as-synthesized nanoparticles showed a low degree of crystallinity and mean dimension of 20 nm. Different thermal treatments were performed so as to investigate their effect on the structural properties and on the particle size of the synthesized products. The optimal temperature was set at 300 °C, giving pure anatase TiO₂ nanopowders with a good level of crystallinity, an average particle size of 50 nm and a high value of specific surface area.