Studies on synergistic solvent extraction of rare earth elements from nitrate medium by mixtures of 8-hydroxyquinoline with Cyanex 301 or Cyanex 302
Synergistic solvent extraction of rare earth elements （REEs） from nitrate medium was investigated with mixtures of 8-hydroxyquinoline （HQ） and acidic organophosphorus extractants, bis（2,4,4-trimethylpentyl） dithiophosphinic acid （Cyanex 301） and bis（2,4,4-trimethylpentyl） monothiophosphinic acid （Cy...
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| Published in | Journal of rare earths Vol. 31; no. 6; pp. 604 - 608 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.06.2013
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1002-0721 2509-4963 |
| DOI | 10.1016/S1002-0721(12)60328-7 |
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| Abstract | Synergistic solvent extraction of rare earth elements （REEs） from nitrate medium was investigated with mixtures of 8-hydroxyquinoline （HQ） and acidic organophosphorus extractants, bis（2,4,4-trimethylpentyl） dithiophosphinic acid （Cyanex 301） and bis（2,4,4-trimethylpentyl） monothiophosphinic acid （Cyanex 302）. The extraction behavior of Cyanex 301/Cyanex 302 and their binary mixtures with HQ towards several lanthanoids （La, Nd, Sm, Tb, Ho, Tm） and yttrium （Y） was investigated. The separation ability of REEs was studied according to the various extraction effects. The extraction mechanisms for yttrium were studied with the methods of slope analysis and constant moles in the synergistic systems. The extracted compounds, the equilibrium constants, and thermodynamic functions were also determined. |
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| AbstractList | Synergistic solvent extraction of rare earth elements (REEs) from nitrate medium was investigated with mixtures of 8-hydroxyquinoline (HQ) and acidic organophosphorus extractants, bis(2,4,4-trimethylpentyl) dithiophosphinic acid (Cyanex 301) and bis(2,4,4-trimethylpentyl) monothiophosphinic acid (Cyanex 302). The extraction behavior of Cyanex 301/Cyanex 302 and their binary mixtures with HQ towards several lanthanoids (La, Nd, Sm, Tb, Ho, Tm) and yttrium (Y) was investigated. The separation ability of REEs was studied according to the various extraction effects. The extraction mechanisms for yttrium were studied with the methods of slope analysis and constant moles in the synergistic systems. The extracted compounds, the equilibrium constants, and thermodynamic functions were also determined.
Relationship between stripping concentration of HNO3 and stripping ratio (▪ 0.012 mol/L HQ+0.008 mol/L C301; • 0.012 mol/L HQ+ 0.008 mol/L C302) Synergistic solvent extraction of rare earth elements (REEs) from nitrate medium was investigated with mixtures of 8-hydroxyquinoline (HQ) and acidic organophosphorus extractants, bis(2,4,4-trimethylpentyl) dithiophosphinic acid (Cyanex 301) and bis(2,4,4-trimethylpentyl) monothiophosphinic acid (Cyanex 302). The extraction behavior of Cyanex 301/Cyanex 302 and their binary mixtures with HQ towards several lanthanoids (La, Nd, Sm, Tb, Ho, Tm) and yttrium (Y) was investigated. The separation ability of REEs was studied according to the various extraction effects. The extraction mechanisms for yttrium were studied with the methods of slope analysis and constant moles in the synergistic systems. The extracted compounds, the equilibrium constants, and thermodynamic functions were also determined. Synergistic solvent extraction of rare earth elements （REEs） from nitrate medium was investigated with mixtures of 8-hydroxyquinoline （HQ） and acidic organophosphorus extractants, bis（2,4,4-trimethylpentyl） dithiophosphinic acid （Cyanex 301） and bis（2,4,4-trimethylpentyl） monothiophosphinic acid （Cyanex 302）. The extraction behavior of Cyanex 301/Cyanex 302 and their binary mixtures with HQ towards several lanthanoids （La, Nd, Sm, Tb, Ho, Tm） and yttrium （Y） was investigated. The separation ability of REEs was studied according to the various extraction effects. The extraction mechanisms for yttrium were studied with the methods of slope analysis and constant moles in the synergistic systems. The extracted compounds, the equilibrium constants, and thermodynamic functions were also determined. |
| Author | 田苗苗 贾琼 廖伍平 |
| AuthorAffiliation | College of Chemistry, Jilin University, Changchun 130012, China State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China |
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| Keywords | 8-hydroxyquinoline extraction Cyanex 301 rare earth elements Cyanex 302 |
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| Notes | Synergistic solvent extraction of rare earth elements （REEs） from nitrate medium was investigated with mixtures of 8-hydroxyquinoline （HQ） and acidic organophosphorus extractants, bis（2,4,4-trimethylpentyl） dithiophosphinic acid （Cyanex 301） and bis（2,4,4-trimethylpentyl） monothiophosphinic acid （Cyanex 302）. The extraction behavior of Cyanex 301/Cyanex 302 and their binary mixtures with HQ towards several lanthanoids （La, Nd, Sm, Tb, Ho, Tm） and yttrium （Y） was investigated. The separation ability of REEs was studied according to the various extraction effects. The extraction mechanisms for yttrium were studied with the methods of slope analysis and constant moles in the synergistic systems. The extracted compounds, the equilibrium constants, and thermodynamic functions were also determined. 11-2788/TF extraction; rare earth elements; 8-hydroxyquinoline; Cyanex 301; Cyanex 302 TIAN Miaomiao, JIA Qiong , LIAO Wuping （1. College of Chemistry, Jilin University, Changchun 130012, China; 2. State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun 130022, China） ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 ObjectType-Article-1 ObjectType-Feature-2 |
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| SubjectTerms | 8-hydroxyquinoline Constants Cyanex Cyanex 301 Cyanex 302 extraction Moles Nitrates Rare earth elements Rare earth metals Samarium Slopes Solvent extraction Thermodynamics Yttrium 二元混合物 协同系统 溶剂萃取 硝酸介质 稀土元素 羟基喹啉 |
| Title | Studies on synergistic solvent extraction of rare earth elements from nitrate medium by mixtures of 8-hydroxyquinoline with Cyanex 301 or Cyanex 302 |
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