Reactive Extraction of Nicotinic Acid with Trialkylamine in n-Octanol
The distributions of nicotinic acid （NA） between water and trialkylamine （N235） dissolved in n-octanol was studied. The complexes of N235 and NA were investigated by Fourier transformation infrared spectrometry to deduce the reaction mechanism. It was found that N235/n-octanol was an efficient extra...
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| Published in | Chinese journal of chemical engineering Vol. 20; no. 5; pp. 843 - 848 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.10.2012
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| Abstract | The distributions of nicotinic acid （NA） between water and trialkylamine （N235） dissolved in n-octanol was studied. The complexes of N235 and NA were investigated by Fourier transformation infrared spectrometry to deduce the reaction mechanism. It was found that N235/n-octanol was an efficient extractant for extracting nicotinic acid. The favorable operation conditions were equilibrium aqueous pH 4.2 to 5.5 and initial N235 concentration〈0.42 mol·L-1 . The reaction processes included the reaction between neutral N235 and neutral NA and the reaction between protonated N235 and anionic NA. Based on the mass action law and some assumptions, an expression for distribution coefficient D was proposed. The apparent extraction equilibrium constants were calculated by fitting the experimental data and the results were satisfactory. |
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| AbstractList | The distributions of nicotinic acid (NA) between water and trialkylamine (N235) dissolved in n-octanol was studied. The complexes of N235 and NA were investigated by Fourier transformation infrared spectrometry to deduce the reaction mechanism. It was found that N235/n-octanol was an efficient extractant for extracting nicotinic acid. The favorable operation conditions were equilibrium aqueous pH 4.2 to 5.5 and initial N235 concentration<0.42 molADTL-1. The reaction processes included the reaction between neutral N235 and neutral NA and the reaction between protonated N235 and anionic NA. Based on the mass action law and some assumptions, an expression for distribution coefficient D was proposed. The apparent extraction equilibrium constants were calculated by fitting the experimental data and the results were satisfactory. The distributions of nicotinic acid (NA) between water and trialkylamine (N235) dissolved in n-octanol was studied. The complexes of N235 and NA were investigated by Fourier transformation infrared spectrometry to deduce the reaction mechanism. It was found that N235/n-octanol was an efficient extractant for extracting nicotinic acid. The favorable operation conditions were equilibrium aqueous pH 4.2 to 5.5 and initial N235 concentration<0.42 molADTLa1. The reaction processes included the reaction between neutral N235 and neutral NA and the reaction between protonated N235 and anionic NA. Based on the mass action law and some assumptions, an expression for distribution coefficient D was proposed. The apparent extraction equilibrium constants were calculated by fitting the experimental data and the results were satisfactory. The distributions of nicotinic acid （NA） between water and trialkylamine （N235） dissolved in n-octanol was studied. The complexes of N235 and NA were investigated by Fourier transformation infrared spectrometry to deduce the reaction mechanism. It was found that N235/n-octanol was an efficient extractant for extracting nicotinic acid. The favorable operation conditions were equilibrium aqueous pH 4.2 to 5.5 and initial N235 concentration〈0.42 mol·L-1 . The reaction processes included the reaction between neutral N235 and neutral NA and the reaction between protonated N235 and anionic NA. Based on the mass action law and some assumptions, an expression for distribution coefficient D was proposed. The apparent extraction equilibrium constants were calculated by fitting the experimental data and the results were satisfactory. The distributions of nicotinic acid (NA) between water and trialkylamine (N235) dissolved in n-octanol was studied. The complexes of N235 and NA were investigated by Fourier transformation infrared spectrometry to deduce the reaction mechanism. It was found that N235/n-octanol was an efficient extractant for extracting nicotinic acid. The favorable operation conditions were equilibrium aqueous pH 4.2 to 5.5 and initial N235 concentration<0.42 mol·L−1. The reaction processes included the reaction between neutral N235 and neutral NA and the reaction between protonated N235 and anionic NA. Based on the mass action law and some assumptions, an expression for distribution coefficient D was proposed. The apparent extraction equilibrium constants were calculated by fitting the experimental data and the results were satisfactory. |
| Author | 李德亮 于飞 常志显 |
| AuthorAffiliation | Institute of Environmental and Analytical Sciences, College of Chemistry and Chemical Engineering, Henan University, Kaifeng 475004, China |
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| CitedBy_id | crossref_primary_10_1080_00032719_2024_2310646 crossref_primary_10_1002_jctb_6972 crossref_primary_10_1016_j_aca_2015_02_049 crossref_primary_10_1021_je500280j crossref_primary_10_1016_j_cherd_2019_04_017 crossref_primary_10_1016_j_cjche_2019_04_019 crossref_primary_10_1016_j_matpr_2022_07_265 |
| Cites_doi | 10.1016/S1369-703X(00)00096-6 10.1002/ceat.200800245 10.1081/SS-100107915 10.1081/SS-100100763 10.1016/S1004-9541(09)60227-5 10.1016/j.fluid.2009.01.014 10.1021/ie00103a035 10.1080/01496390500267681 10.1021/je0601412 10.1016/S1385-8947(00)00236-9 10.1016/S0168-1656(02)00057-3 10.1016/S1004-9541(07)60109-8 10.1016/j.cej.2009.03.037 10.1016/S1004-9541(09)60007-0 10.1016/S1383-5866(01)00137-X 10.1021/je8008914 10.1021/je900205h 10.1002/1097-0290(20000905)69:5<469::AID-BIT1>3.0.CO;2-M 10.1016/S0009-2509(99)00070-6 10.1021/je034124d 10.1080/01496390601069937 10.1080/15363830701313578 10.1021/je015526t 10.1016/j.seppur.2008.04.012 10.1081/SS-100100234 |
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| Keywords | reactive extraction trialkylamine proton-transfer nicotinic acid |
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| Notes | LI Dehang , YU Fei and CHANG Zhixian Institute of Environmental and Analytical Sciences, College of Chemistry and Chemical Engineering, Henan University, Kaifeng 475004, China nicotinic acid, reactive extraction, trlalkylamlne, proton-transter 11-3270/TQ The distributions of nicotinic acid （NA） between water and trialkylamine （N235） dissolved in n-octanol was studied. The complexes of N235 and NA were investigated by Fourier transformation infrared spectrometry to deduce the reaction mechanism. It was found that N235/n-octanol was an efficient extractant for extracting nicotinic acid. The favorable operation conditions were equilibrium aqueous pH 4.2 to 5.5 and initial N235 concentration〈0.42 mol·L-1 . The reaction processes included the reaction between neutral N235 and neutral NA and the reaction between protonated N235 and anionic NA. Based on the mass action law and some assumptions, an expression for distribution coefficient D was proposed. The apparent extraction equilibrium constants were calculated by fitting the experimental data and the results were satisfactory. ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| Snippet | The distributions of nicotinic acid （NA） between water and trialkylamine （N235） dissolved in n-octanol was studied. The complexes of N235 and NA were... The distributions of nicotinic acid (NA) between water and trialkylamine (N235) dissolved in n-octanol was studied. The complexes of N235 and NA were... |
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| SubjectTerms | Chemical engineering Extraction Fittings Fourier transformation Infrared Mathematical analysis N235 Nicotinic acid proton-transfer reactive extraction Spectrometry trialkylamine 三烷基胺 傅立叶变换红外光谱仪 反应萃取 正辛醇 烟酸 表观萃取平衡常数 质量作用定律 |
| Title | Reactive Extraction of Nicotinic Acid with Trialkylamine in n-Octanol |
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