Porous Ni5P4 as a promising cocatalyst for boosting the photocatalytic hydrogen evolution reaction performance
[Display omitted] •Porous and carnation-like Ni5P4 was synthesized using phosphorization process.•Ni5P4 was used as cocatalyst to construct a Schottky-junction with g-C3N4.•Ni5P4 cocatalyst with lower adsorption behavior is favor for H2 production.•Ni5P4 cocatalyst can accelerate the separation of t...
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| Published in | Applied catalysis. B, Environmental Vol. 275; p. 119144 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
15.10.2020
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0926-3373 1873-3883 |
| DOI | 10.1016/j.apcatb.2020.119144 |
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| Abstract | [Display omitted]
•Porous and carnation-like Ni5P4 was synthesized using phosphorization process.•Ni5P4 was used as cocatalyst to construct a Schottky-junction with g-C3N4.•Ni5P4 cocatalyst with lower adsorption behavior is favor for H2 production.•Ni5P4 cocatalyst can accelerate the separation of the light-induced carriers.
Nonmetallic cocatalysts have demonstrated unprecedented potential for accelerating photocatalytic hydrogen evolution reaction (HER). In this study, a nickel phosphide compound, namely Ni5P4, with porous carnation-like superstructure has been target-synthesized and then employed as HER cocatalyst to in-situ build a hybrid with protonated g-C3N4 nanosheets via an electrostatic self-assembly method. Owing to the synergistic advantages of the excellent metallic conductivity and porous carnation-like superstructure of Ni5P4, the as-obtained HCN/Ni5P4 Schottky-junction with abundant active sites, low H* atom adsorption energy and efficient charge carrier transport channel, affords the photocatalytic H2 production rate of 1157.5 μmol g−1 h−1 when exposed to visible light (λ > 420 nm). This photocatalytic H2 production rate was much higher than those of the corresponding reference cocatalysts, namely Ni2P and NiS2 (169.1 and 593.1 μmol g−1 h−1, respectively), both of which were derived from the same Ni(OH)2 precursor. This study provides a new idea for the design of highly active noble-metal-free materials for the photocatalytic HER. |
|---|---|
| AbstractList | [Display omitted]
•Porous and carnation-like Ni5P4 was synthesized using phosphorization process.•Ni5P4 was used as cocatalyst to construct a Schottky-junction with g-C3N4.•Ni5P4 cocatalyst with lower adsorption behavior is favor for H2 production.•Ni5P4 cocatalyst can accelerate the separation of the light-induced carriers.
Nonmetallic cocatalysts have demonstrated unprecedented potential for accelerating photocatalytic hydrogen evolution reaction (HER). In this study, a nickel phosphide compound, namely Ni5P4, with porous carnation-like superstructure has been target-synthesized and then employed as HER cocatalyst to in-situ build a hybrid with protonated g-C3N4 nanosheets via an electrostatic self-assembly method. Owing to the synergistic advantages of the excellent metallic conductivity and porous carnation-like superstructure of Ni5P4, the as-obtained HCN/Ni5P4 Schottky-junction with abundant active sites, low H* atom adsorption energy and efficient charge carrier transport channel, affords the photocatalytic H2 production rate of 1157.5 μmol g−1 h−1 when exposed to visible light (λ > 420 nm). This photocatalytic H2 production rate was much higher than those of the corresponding reference cocatalysts, namely Ni2P and NiS2 (169.1 and 593.1 μmol g−1 h−1, respectively), both of which were derived from the same Ni(OH)2 precursor. This study provides a new idea for the design of highly active noble-metal-free materials for the photocatalytic HER. Nonmetallic cocatalysts have demonstrated unprecedented potential for accelerating photocatalytic hydrogen evolution reaction (HER). In this study, a nickel phosphide compound, namely Ni5P4, with porous carnation-like superstructure has been target-synthesized and then employed as HER cocatalyst to in-situ build a hybrid with protonated g-C3N4 nanosheets via an electrostatic self-assembly method. Owing to the synergistic advantages of the excellent metallic conductivity and porous carnation-like superstructure of Ni5P4, the as-obtained HCN/Ni5P4 Schottky-junction with abundant active sites, low H* atom adsorption energy and efficient charge carrier transport channel, affords the photocatalytic H2 production rate of 1157.5 μmol g−1 h−1 when exposed to visible light (λ > 420 nm). This photocatalytic H2 production rate was much higher than those of the corresponding reference cocatalysts, namely Ni2P and NiS2 (169.1 and 593.1 μmol g−1 h−1, respectively), both of which were derived from the same Ni(OH)2 precursor. This study provides a new idea for the design of highly active noble-metal-free materials for the photocatalytic HER. |
| ArticleNumber | 119144 |
| Author | Yang, Xiaofei Zhang, Tierui Liu, Qinqin Li, Youyong Zhao, Yunxuan Tang, Hua Yu, Xiaohui Liu, Xin |
| Author_xml | – sequence: 1 givenname: Xin surname: Liu fullname: Liu, Xin organization: School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013, China – sequence: 2 givenname: Yunxuan surname: Zhao fullname: Zhao, Yunxuan organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190, China – sequence: 3 givenname: Xiaofei surname: Yang fullname: Yang, Xiaofei organization: College of Science, Institute of Materials Physics and Chemistry, Nanjing Forestry University, Nanjing 210037, China – sequence: 4 givenname: Qinqin surname: Liu fullname: Liu, Qinqin email: qqliu@ujs.edu.cn organization: School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013, China – sequence: 5 givenname: Xiaohui surname: Yu fullname: Yu, Xiaohui organization: School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013, China – sequence: 6 givenname: Youyong surname: Li fullname: Li, Youyong organization: Institute of Nanoscience and Technology, Soochow University, Soochow 215000, China – sequence: 7 givenname: Hua surname: Tang fullname: Tang, Hua email: huatang79@163.com organization: School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013, China – sequence: 8 givenname: Tierui orcidid: 0000-0002-7948-9413 surname: Zhang fullname: Zhang, Tierui organization: Key Laboratory of Photochemical Conversion and Optoelectronic Materials, Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190, China |
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•Porous and carnation-like Ni5P4 was synthesized using phosphorization process.•Ni5P4 was used as cocatalyst to construct a Schottky-junction... Nonmetallic cocatalysts have demonstrated unprecedented potential for accelerating photocatalytic hydrogen evolution reaction (HER). In this study, a nickel... |
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| SubjectTerms | Carbon nitride Carrier transport Charge transport Cocatalyst Current carriers Dianthus caryophyllus Energy charge HCN Hydrogen evolution reactions Hydrogen production Nickel Noble metals Phosphides Photocatalysis Photocatalytic H2 evolution Porous carnation-like Ni5P4 Self-assembly Superstructures |
| Title | Porous Ni5P4 as a promising cocatalyst for boosting the photocatalytic hydrogen evolution reaction performance |
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