On the oxidation mechanism of refractory high entropy alloys
•The formation of CrTaO4 after a short incubation period decreased the oxidation kinetics of Ta-containing alloys.•Activation energies for scale growth comparable to those of Cr2O3 and CrTaO4 forming Ni-based superalloys were found.•The oxygen inward diffusion was found to be rate determining in CrT...
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| Published in | Corrosion science Vol. 159; p. 108161 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier Ltd
01.10.2019
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | •The formation of CrTaO4 after a short incubation period decreased the oxidation kinetics of Ta-containing alloys.•Activation energies for scale growth comparable to those of Cr2O3 and CrTaO4 forming Ni-based superalloys were found.•The oxygen inward diffusion was found to be rate determining in CrTaO4 forming alloys.•In Nb-containing alloys, the formation of Nb2O5 caused a porous oxide scale as well as severe oxide spallation.•Ti had a positive effect on the high-temperature oxidation behaviour because it supports the formation of protective CrTaO4.
The high-temperature oxidation mechanism of a series of refractory high entropy alloys: TaMoCrTiAl, NbMoCrTiAl, NbMoCrAl and TaMoCrAl at 1000 °C in air was studied. A complex protective oxide layer consisting of Al2O3, Cr2O3 and CrTaO4 oxides was observed for the quinary Ta-containing alloy. The formation of CrTaO4 in this alloy after a short incubation period decreased the oxidation kinetics from a parabolic to a quartic rate law. Ti was found to support the formation of CrTaO4. In the Nb-containing alloys, the formation of different Nb2O5 polytypes near the metal/oxide interface caused a highly porous oxide scale and severe oxide spallation. |
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| AbstractList | •The formation of CrTaO4 after a short incubation period decreased the oxidation kinetics of Ta-containing alloys.•Activation energies for scale growth comparable to those of Cr2O3 and CrTaO4 forming Ni-based superalloys were found.•The oxygen inward diffusion was found to be rate determining in CrTaO4 forming alloys.•In Nb-containing alloys, the formation of Nb2O5 caused a porous oxide scale as well as severe oxide spallation.•Ti had a positive effect on the high-temperature oxidation behaviour because it supports the formation of protective CrTaO4.
The high-temperature oxidation mechanism of a series of refractory high entropy alloys: TaMoCrTiAl, NbMoCrTiAl, NbMoCrAl and TaMoCrAl at 1000 °C in air was studied. A complex protective oxide layer consisting of Al2O3, Cr2O3 and CrTaO4 oxides was observed for the quinary Ta-containing alloy. The formation of CrTaO4 in this alloy after a short incubation period decreased the oxidation kinetics from a parabolic to a quartic rate law. Ti was found to support the formation of CrTaO4. In the Nb-containing alloys, the formation of different Nb2O5 polytypes near the metal/oxide interface caused a highly porous oxide scale and severe oxide spallation. The high-temperature oxidation mechanism of a series of refractory high entropy alloys: TaMoCrTiAl, NbMoCrTiAl, NbMoCrAl and TaMoCrAl at 1000 °C in air was studied. A complex protective oxide layer consisting of Al2O3, Cr2O3 and CrTaO4 oxides was observed for the quinary Ta-containing alloy. The formation of CrTaO4 in this alloy after a short incubation period decreased the oxidation kinetics from a parabolic to a quartic rate law. Ti was found to support the formation of CrTaO4. In the Nb-containing alloys, the formation of different Nb2O5 polytypes near the metal/oxide interface caused a highly porous oxide scale and severe oxide spallation. |
| ArticleNumber | 108161 |
| Author | Müller, Franz Müller, Julian Chen, Hans Kauffmann, Alexander Christ, Hans-Jürgen Heilmaier, Martin Butz, Benjamin Gorr, Bronislava |
| Author_xml | – sequence: 1 givenname: Franz surname: Müller fullname: Müller, Franz email: franz.mueller@uni-siegen.de organization: Institut für Werkstofftechnik, Universität Siegen, Siegen, Germany – sequence: 2 givenname: Bronislava surname: Gorr fullname: Gorr, Bronislava organization: Institut für Werkstofftechnik, Universität Siegen, Siegen, Germany – sequence: 3 givenname: Hans-Jürgen surname: Christ fullname: Christ, Hans-Jürgen organization: Institut für Werkstofftechnik, Universität Siegen, Siegen, Germany – sequence: 4 givenname: Julian surname: Müller fullname: Müller, Julian organization: Institut für Werkstofftechnik, Universität Siegen, Siegen, Germany – sequence: 5 givenname: Benjamin surname: Butz fullname: Butz, Benjamin organization: Institut für Werkstofftechnik, Universität Siegen, Siegen, Germany – sequence: 6 givenname: Hans surname: Chen fullname: Chen, Hans organization: Institut für Angewandte Materialien, Karlsruher Institut für Technologie (KIT), Karlsruhe, Germany – sequence: 7 givenname: Alexander surname: Kauffmann fullname: Kauffmann, Alexander organization: Institut für Angewandte Materialien, Karlsruher Institut für Technologie (KIT), Karlsruhe, Germany – sequence: 8 givenname: Martin surname: Heilmaier fullname: Heilmaier, Martin organization: Institut für Angewandte Materialien, Karlsruher Institut für Technologie (KIT), Karlsruhe, Germany |
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| Keywords | Compositionally complex alloy Quartic rate law Refractory high entropy alloy High temperature corrosion CrTaO4 formation |
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| Snippet | •The formation of CrTaO4 after a short incubation period decreased the oxidation kinetics of Ta-containing alloys.•Activation energies for scale growth... The high-temperature oxidation mechanism of a series of refractory high entropy alloys: TaMoCrTiAl, NbMoCrTiAl, NbMoCrAl and TaMoCrAl at 1000 °C in air was... |
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| SubjectTerms | Alloys Aluminum oxide Compositionally complex alloy CrTaO4 formation Heat resistant alloys High entropy alloys High temperature High temperature corrosion Niobium oxides Oxidation Polytypes Quartic rate law Reaction kinetics Refractory alloys Refractory high entropy alloy Refractory materials Scale (corrosion) Spallation Tantalum Titanium |
| Title | On the oxidation mechanism of refractory high entropy alloys |
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