Structure inheritance strategy from MOF to edge-enriched NiFe-LDH array for enhanced oxygen evolution reaction
[Display omitted] •A structure inheritance strategy to synthesize edge-enriched nanostructures is reported.•An edge-enriched NiFe-LDH nanoarray with high OER activity is successfully synthesized.•The roles of the edges in NiFe-LDH for OER is unraveled. The rational design of advanced nanostructures...
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| Published in | Applied catalysis. B, Environmental Vol. 298; p. 120580 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
05.12.2021
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•A structure inheritance strategy to synthesize edge-enriched nanostructures is reported.•An edge-enriched NiFe-LDH nanoarray with high OER activity is successfully synthesized.•The roles of the edges in NiFe-LDH for OER is unraveled.
The rational design of advanced nanostructures for catalysts to fully expose the edge or corner sites is highly desirable to optimize their electrocatalytic performance. In this work, we report an edge-enriched (EE) NiFe-layer double hydroxide (LDH) nanoarray with abundant coordinatively unsaturated sites, which was synthesized by a structure inheritance strategy using metal-organic framework (MOF) nanosheet array as a structure-directing template. Impressively, the obtained EE-NiFe-LDH nanosheet array offers high electrocatalytic activity in oxygen evolution reaction (OER) with an overpotential of only 205 mV to reach a current density of 10 mA cm−2, outperforming all reported NiFe-LDH nanostructures. X-ray absorption spectroscopy and density functional theory calculations demonstrate that the exposed edges in EE-NiFe-LDH contain abundant iron and oxygen vacancies, which optimized the electronic state of the NiFe-LDH and enhanced the adsorption of oxygenated intermediates, resulting in the high catalytic activity for OER. |
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| AbstractList | The rational design of advanced nanostructures for catalysts to fully expose the edge or corner sites is highly desirable to optimize their electrocatalytic performance. In this work, we report an edge-enriched (EE) NiFe-layer double hydroxide (LDH) nanoarray with abundant coordinatively unsaturated sites, which was synthesized by a structure inheritance strategy using metal-organic framework (MOF) nanosheet array as a structure-directing template. Impressively, the obtained EE-NiFe-LDH nanosheet array offers high electrocatalytic activity in oxygen evolution reaction (OER) with an overpotential of only 205 mV to reach a current density of 10 mA cm−2, outperforming all reported NiFe-LDH nanostructures. X-ray absorption spectroscopy and density functional theory calculations demonstrate that the exposed edges in EE-NiFe-LDH contain abundant iron and oxygen vacancies, which optimized the electronic state of the NiFe-LDH and enhanced the adsorption of oxygenated intermediates, resulting in the high catalytic activity for OER. [Display omitted] •A structure inheritance strategy to synthesize edge-enriched nanostructures is reported.•An edge-enriched NiFe-LDH nanoarray with high OER activity is successfully synthesized.•The roles of the edges in NiFe-LDH for OER is unraveled. The rational design of advanced nanostructures for catalysts to fully expose the edge or corner sites is highly desirable to optimize their electrocatalytic performance. In this work, we report an edge-enriched (EE) NiFe-layer double hydroxide (LDH) nanoarray with abundant coordinatively unsaturated sites, which was synthesized by a structure inheritance strategy using metal-organic framework (MOF) nanosheet array as a structure-directing template. Impressively, the obtained EE-NiFe-LDH nanosheet array offers high electrocatalytic activity in oxygen evolution reaction (OER) with an overpotential of only 205 mV to reach a current density of 10 mA cm−2, outperforming all reported NiFe-LDH nanostructures. X-ray absorption spectroscopy and density functional theory calculations demonstrate that the exposed edges in EE-NiFe-LDH contain abundant iron and oxygen vacancies, which optimized the electronic state of the NiFe-LDH and enhanced the adsorption of oxygenated intermediates, resulting in the high catalytic activity for OER. |
| ArticleNumber | 120580 |
| Author | Yang, Can Wang, Bingqing Han, Aijuan Wang, Dingsheng Liu, Junfeng Guo, Chong Jing, Jin Han, Xu Li, Yaping |
| Author_xml | – sequence: 1 givenname: Bingqing surname: Wang fullname: Wang, Bingqing organization: State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China – sequence: 2 givenname: Xu surname: Han fullname: Han, Xu organization: State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China – sequence: 3 givenname: Chong surname: Guo fullname: Guo, Chong organization: Department of Chemistry, Tsinghua University, Beijing, 100084, PR China – sequence: 4 givenname: Jin surname: Jing fullname: Jing, Jin organization: State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China – sequence: 5 givenname: Can surname: Yang fullname: Yang, Can organization: State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China – sequence: 6 givenname: Yaping surname: Li fullname: Li, Yaping organization: State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China – sequence: 7 givenname: Aijuan surname: Han fullname: Han, Aijuan organization: State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China – sequence: 8 givenname: Dingsheng surname: Wang fullname: Wang, Dingsheng organization: Department of Chemistry, Tsinghua University, Beijing, 100084, PR China – sequence: 9 givenname: Junfeng surname: Liu fullname: Liu, Junfeng email: ljf@mail.buct.edu.cn organization: State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, PR China |
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•A structure inheritance strategy to synthesize edge-enriched nanostructures is reported.•An edge-enriched NiFe-LDH nanoarray with high OER... The rational design of advanced nanostructures for catalysts to fully expose the edge or corner sites is highly desirable to optimize their electrocatalytic... |
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| SubjectTerms | Absorption spectroscopy Arrays Catalysts Catalytic activity Defects Density functional theory Edges Electron states Heredity Inheritances Intermediates Intermetallic compounds Iron compounds LDH Metal-organic frameworks Nanostructure Nickel compounds OER Oxygen Oxygen enrichment Oxygen evolution reactions Unsaturated sites X ray absorption X-ray absorption spectroscopy |
| Title | Structure inheritance strategy from MOF to edge-enriched NiFe-LDH array for enhanced oxygen evolution reaction |
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