Two-dimensional correlation analysis of continuous online in situ ATR-FTIR on the adsorption of butyl xanthate at the surface of α-PbO

The adsorption behavior of butyl xanthate on the surface of lead oxide was investigated using continuous online in situ attenuated total reflectance Fourier transform infrared（ATR-FTIR） spectroscopy technique and two dimensional（2D） correlation analysis.The adsorbed layer studied was prepared by coa...

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Published inChinese chemical letters Vol. 26; no. 2; pp. 193 - 196
Main Authors Shen, Qi, Fan, Ying-Ju, Zhang, Wei-Min, Zhu, Bo-Li, Wang, Ru, Sun, Zhong-Xi
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.02.2015
Subjects
ATR-FTIR
Butyl xanthate
Continuous online in situ
Two-dimensional correlation analysis
α-PbO
丁基黄药
二维
原位
吸附行为
氧化铅
相关性分析
表面
Continuous online in situ
Two-dimensional correlation analysis
α-PbO
ATR-FTIR
Butyl xanthate
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Abstract The adsorption behavior of butyl xanthate on the surface of lead oxide was investigated using continuous online in situ attenuated total reflectance Fourier transform infrared（ATR-FTIR） spectroscopy technique and two dimensional（2D） correlation analysis.The adsorbed layer studied was prepared by coating α-PbO particles onto the surfaces of the ZnSe crystal.The appearance of spectral peaks at 1203 cm^-1,1033 cm^-1 and their red shift indicated the formation and aggregation of xanthate at the surface of α-PbO.According to 1R intensity changes after rinsing with deionized water and a NaOH solution,the adsorption was proved to be a chemisorption type.The competition between xanthate and OH^- for the surfaces leads to desorption of xanthate at higher pH.The technique of 2D correlation ATR-FTIR spectroscopy was used to evaluate the changing order of spectral intensities in the adsorption process,and the results indicated that xanthate micelles were formed at the surfaces.The adsorption kinetics of butyl xanthate was found to be a pseudo-second-order reaction model and the adsorption capacity of butyl xanthate at α-PbO was as high as 281 mg g^-1 after 150 min.
AbstractList The appearance of spectral peaks at 1203cm−1, 1033cm−1 and their red shift indicated the formation and aggregation of xanthate at the surface of α-PbO. The adsorption behavior of butyl xanthate on the surface of lead oxide was investigated using continuous online in situ attenuated total reflectance Fourier transform infrared (ATR-FTIR) spectroscopy technique and two dimensional (2D) correlation analysis. The adsorbed layer studied was prepared by coating α-PbO particles onto the surfaces of the ZnSe crystal. The appearance of spectral peaks at 1203cm−1, 1033cm−1 and their red shift indicated the formation and aggregation of xanthate at the surface of α-PbO. According to IR intensity changes after rinsing with deionized water and a NaOH solution, the adsorption was proved to be a chemisorption type. The competition between xanthate and OH− for the surfaces leads to desorption of xanthate at higher pH. The technique of 2D correlation ATR-FTIR spectroscopy was used to evaluate the changing order of spectral intensities in the adsorption process, and the results indicated that xanthate micelles were formed at the surfaces. The adsorption kinetics of butyl xanthate was found to be a pseudo-second-order reaction model and the adsorption capacity of butyl xanthate at α-PbO was as high as 281mgg−1 after 150min.
The adsorption behavior of butyl xanthate on the surface of lead oxide was investigated using continuous online in situ attenuated total reflectance Fourier transform infrared（ATR-FTIR） spectroscopy technique and two dimensional（2D） correlation analysis.The adsorbed layer studied was prepared by coating α-PbO particles onto the surfaces of the ZnSe crystal.The appearance of spectral peaks at 1203 cm^-1,1033 cm^-1 and their red shift indicated the formation and aggregation of xanthate at the surface of α-PbO.According to 1R intensity changes after rinsing with deionized water and a NaOH solution,the adsorption was proved to be a chemisorption type.The competition between xanthate and OH^- for the surfaces leads to desorption of xanthate at higher pH.The technique of 2D correlation ATR-FTIR spectroscopy was used to evaluate the changing order of spectral intensities in the adsorption process,and the results indicated that xanthate micelles were formed at the surfaces.The adsorption kinetics of butyl xanthate was found to be a pseudo-second-order reaction model and the adsorption capacity of butyl xanthate at α-PbO was as high as 281 mg g^-1 after 150 min.
Author Qi Shen Ying-Ju Fan Wei-Min Zhang Bo-Li Zhu Ru Wang Zhong-Xi Sun
AuthorAffiliation School of Chemistry and Chemical Engineering, University of Ji＇nan, Ji＇nan 250022, China
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Keywords Continuous online in situ
Two-dimensional correlation analysis
α-PbO
ATR-FTIR
Butyl xanthate
Language English
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Notes Two-dimensional correlation analysis Continuous online in situ ATR-FTIR Butyl xanthate α-PbO
11-2710/O6
The adsorption behavior of butyl xanthate on the surface of lead oxide was investigated using continuous online in situ attenuated total reflectance Fourier transform infrared（ATR-FTIR） spectroscopy technique and two dimensional（2D） correlation analysis.The adsorbed layer studied was prepared by coating α-PbO particles onto the surfaces of the ZnSe crystal.The appearance of spectral peaks at 1203 cm^-1,1033 cm^-1 and their red shift indicated the formation and aggregation of xanthate at the surface of α-PbO.According to 1R intensity changes after rinsing with deionized water and a NaOH solution,the adsorption was proved to be a chemisorption type.The competition between xanthate and OH^- for the surfaces leads to desorption of xanthate at higher pH.The technique of 2D correlation ATR-FTIR spectroscopy was used to evaluate the changing order of spectral intensities in the adsorption process,and the results indicated that xanthate micelles were formed at the surfaces.The adsorption kinetics of butyl xanthate was found to be a pseudo-second-order reaction model and the adsorption capacity of butyl xanthate at α-PbO was as high as 281 mg g^-1 after 150 min.
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Snippet The adsorption behavior of butyl xanthate on the surface of lead oxide was investigated using continuous online in situ attenuated total reflectance Fourier...
The appearance of spectral peaks at 1203cm−1, 1033cm−1 and their red shift indicated the formation and aggregation of xanthate at the surface of α-PbO. The...
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elsevier
chongqing
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Publisher
StartPage 193
SubjectTerms ATR-FTIR
Butyl xanthate
Continuous online in situ
Two-dimensional correlation analysis
α-PbO
丁基黄药
二维
原位
吸附行为
氧化铅
相关性分析
表面
Title Two-dimensional correlation analysis of continuous online in situ ATR-FTIR on the adsorption of butyl xanthate at the surface of α-PbO
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