Silicon nitride foams from emulsions sintered by rapid intense thermal radiation
Open cell Si3N4 foams were fabricated by an emulsification process and subsequent sintering. Emulsification took place in an aqueous environment by using octane as alkane phase and a surfactant as stabilizer. Effects of different octane concentrations (50vol% and 70vol%) and stirring velocities (700...
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Published in | Journal of the European Ceramic Society Vol. 35; no. 12; pp. 3263 - 3272 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
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Elsevier Ltd
01.10.2015
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Abstract | Open cell Si3N4 foams were fabricated by an emulsification process and subsequent sintering. Emulsification took place in an aqueous environment by using octane as alkane phase and a surfactant as stabilizer. Effects of different octane concentrations (50vol% and 70vol%) and stirring velocities (700rpm and 1000rpm) on porosity and pore size distribution were investigated. The shaped foams were pressureless sintered at 1600°C inside a modified SPS set-up. Si3N4 foams decorated with SiC nanowires and with an average cell size of 8–41μm and total porosity of 80–86vol% were obtained. The compressive strength ranged from 2.0MPa up to 9.9MPa. Both the foaming and sintering processes contributed to the development of different microstructures. |
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AbstractList | Open cell Si3N4 foams were fabricated by an emulsification process and subsequent sintering. Emulsification took place in an aqueous environment by using octane as alkane phase and a surfactant as stabilizer. Effects of different octane concentrations (50 vol% and 70 vol%) and stirring velocities (700 rpm and 1000 rpm) on porosity and pore size distribution were investigated. The shaped foams were pressureless sintered at 1600 degrees C inside a modified SPS set-up. Si3N4 foams decorated with SiC nanowires and with an average cell size of 8-41 mu m and total porosity of 80-86 vol% were obtained. The compressive strength ranged from 2.0 MPa up to 9.9 MPa. Both the foaming and sintering processes contributed to the development of different microstructures. Open cell Si3N4 foams were fabricated by an emulsification process and subsequent sintering. Emulsification took place in an aqueous environment by using octane as alkane phase and a surfactant as stabilizer. Effects of different octane concentrations (50vol% and 70vol%) and stirring velocities (700rpm and 1000rpm) on porosity and pore size distribution were investigated. The shaped foams were pressureless sintered at 1600°C inside a modified SPS set-up. Si3N4 foams decorated with SiC nanowires and with an average cell size of 8–41μm and total porosity of 80–86vol% were obtained. The compressive strength ranged from 2.0MPa up to 9.9MPa. Both the foaming and sintering processes contributed to the development of different microstructures. |
Author | Colombo, Paolo de Moraes, Elisângela Guzi Li, Duan Shen, Zhijian |
Author_xml | – sequence: 1 givenname: Elisângela Guzi surname: de Moraes fullname: de Moraes, Elisângela Guzi email: elisangela.guzidemoraes@studenti.unipd.it organization: Dipartimento di Ingegneria Industriale, University of Padova, Via Marzolo 9, 35131 Padova, Italy – sequence: 2 givenname: Duan surname: Li fullname: Li, Duan organization: Department of Materials and Environmental Chemistry, Arrhenius Laboratory, Stockholm University, S-106 91 Stockholm, Sweden – sequence: 3 givenname: Paolo surname: Colombo fullname: Colombo, Paolo organization: Dipartimento di Ingegneria Industriale, University of Padova, Via Marzolo 9, 35131 Padova, Italy – sequence: 4 givenname: Zhijian surname: Shen fullname: Shen, Zhijian organization: Department of Materials and Environmental Chemistry, Arrhenius Laboratory, Stockholm University, S-106 91 Stockholm, Sweden |
BackLink | https://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-119277$$DView record from Swedish Publication Index |
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Keywords | Foams Spark plasma sintering Emulsification Silicon nitride Sintering by intense thermal radiation |
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SubjectTerms | Emulsification Foams Silicon nitride Sintering by intense thermal radiation Spark plasma sintering |
Title | Silicon nitride foams from emulsions sintered by rapid intense thermal radiation |
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