Biobased polyelectrolyte multilayer-coated hollow mesoporous silica as a green flame retardant for epoxy resin

•A green flame retardant (HM–SiO2@CS@PCL) was successfully synthesized through layer-by-layer assembly.•The integrated effect of HM–SiO2@CS@PCL endows epoxy resin with excellent flame retardancy.•The incorporation of HM–SiO2@CS@PCL can recycle epoxy resin into high value-added hollow carbon spheres....

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Published in	Journal of hazardous materials Vol. 342; pp. 689 - 697
Main Authors	Jiang, Shu-Dong, Tang, Gang, Chen, Junmin, Huang, Zheng-Qi, Hu, Yuan
Format	Journal Article
Language	English
Published	Netherlands Elsevier B.V 15.01.2018
Subjects	carbon cellulose chitosan coatings combustion electrolytes electrostatic interactions epoxides Epoxy resin fire safety flame retardants Green flame retardant heat Hollow mesoporous silica Polyelectrolyte multilayer polymers porous media silica silicon Sustainable recycling thermal properties value added Epoxy resin Green flame retardant Hollow mesoporous silica Polyelectrolyte multilayer Sustainable recycling
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Abstract	•A green flame retardant (HM–SiO2@CS@PCL) was successfully synthesized through layer-by-layer assembly.•The integrated effect of HM–SiO2@CS@PCL endows epoxy resin with excellent flame retardancy.•The incorporation of HM–SiO2@CS@PCL can recycle epoxy resin into high value-added hollow carbon spheres. Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO2@CS@PCL) as a green flame retardant through layer-by-layer assembly using hollow mesoporous silica (HM-SiO2), chitosan (CS) and phosphorylated cellulose (PCL). The electrostatic interactions deposited the CS/PCL coating on the surface of HM-SiO2. Subsequently, this multifunctional flame retardant was used to enhance thermal properties and flame retardancy of epoxy resin. The addition of HM-SiO2@CS@PCL to the epoxy resin thermally destabilized the epoxy resin composite, but generated a higher char yield. Furthermore, HM-SiO2 played a critical role and generated synergies with CS and PCL to improve fire safety of the epoxy resin due to the multiple flame retardancy elements (P, N and Si). This multi-element, synergistic, flame-retardant system resulted in a remarkable reduction (51%) of peak heat release rate and a considerable removal of flammable decomposed products. Additionally, the incorporation of HM-SiO2@CS@PCL can sustainably recycle the epoxy resin into high value-added hollow carbon spheres during combustion. Therefore, the HM-SiO2@CS@PCL system provides a practical possibility for preparing recyclable polymer materials with multi-functions and high performances.
AbstractList	•A green flame retardant (HM–SiO2@CS@PCL) was successfully synthesized through layer-by-layer assembly.•The integrated effect of HM–SiO2@CS@PCL endows epoxy resin with excellent flame retardancy.•The incorporation of HM–SiO2@CS@PCL can recycle epoxy resin into high value-added hollow carbon spheres. Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO2@CS@PCL) as a green flame retardant through layer-by-layer assembly using hollow mesoporous silica (HM-SiO2), chitosan (CS) and phosphorylated cellulose (PCL). The electrostatic interactions deposited the CS/PCL coating on the surface of HM-SiO2. Subsequently, this multifunctional flame retardant was used to enhance thermal properties and flame retardancy of epoxy resin. The addition of HM-SiO2@CS@PCL to the epoxy resin thermally destabilized the epoxy resin composite, but generated a higher char yield. Furthermore, HM-SiO2 played a critical role and generated synergies with CS and PCL to improve fire safety of the epoxy resin due to the multiple flame retardancy elements (P, N and Si). This multi-element, synergistic, flame-retardant system resulted in a remarkable reduction (51%) of peak heat release rate and a considerable removal of flammable decomposed products. Additionally, the incorporation of HM-SiO2@CS@PCL can sustainably recycle the epoxy resin into high value-added hollow carbon spheres during combustion. Therefore, the HM-SiO2@CS@PCL system provides a practical possibility for preparing recyclable polymer materials with multi-functions and high performances. Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO₂@CS@PCL) as a green flame retardant through layer-by-layer assembly using hollow mesoporous silica (HM-SiO₂), chitosan (CS) and phosphorylated cellulose (PCL). The electrostatic interactions deposited the CS/PCL coating on the surface of HM-SiO₂. Subsequently, this multifunctional flame retardant was used to enhance thermal properties and flame retardancy of epoxy resin. The addition of HM-SiO₂@CS@PCL to the epoxy resin thermally destabilized the epoxy resin composite, but generated a higher char yield. Furthermore, HM-SiO₂ played a critical role and generated synergies with CS and PCL to improve fire safety of the epoxy resin due to the multiple flame retardancy elements (P, N and Si). This multi-element, synergistic, flame-retardant system resulted in a remarkable reduction (51%) of peak heat release rate and a considerable removal of flammable decomposed products. Additionally, the incorporation of HM-SiO₂@CS@PCL can sustainably recycle the epoxy resin into high value-added hollow carbon spheres during combustion. Therefore, the HM-SiO₂@CS@PCL system provides a practical possibility for preparing recyclable polymer materials with multi-functions and high performances. Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO @CS@PCL) as a green flame retardant through layer-by-layer assembly using hollow mesoporous silica (HM-SiO ), chitosan (CS) and phosphorylated cellulose (PCL). The electrostatic interactions deposited the CS/PCL coating on the surface of HM-SiO . Subsequently, this multifunctional flame retardant was used to enhance thermal properties and flame retardancy of epoxy resin. The addition of HM-SiO @CS@PCL to the epoxy resin thermally destabilized the epoxy resin composite, but generated a higher char yield. Furthermore, HM-SiO played a critical role and generated synergies with CS and PCL to improve fire safety of the epoxy resin due to the multiple flame retardancy elements (P, N and Si). This multi-element, synergistic, flame-retardant system resulted in a remarkable reduction (51%) of peak heat release rate and a considerable removal of flammable decomposed products. Additionally, the incorporation of HM-SiO @CS@PCL can sustainably recycle the epoxy resin into high value-added hollow carbon spheres during combustion. Therefore, the HM-SiO @CS@PCL system provides a practical possibility for preparing recyclable polymer materials with multi-functions and high performances. Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO2@CS@PCL) as a green flame retardant through layer-by-layer assembly using hollow mesoporous silica (HM-SiO2), chitosan (CS) and phosphorylated cellulose (PCL). The electrostatic interactions deposited the CS/PCL coating on the surface of HM-SiO2. Subsequently, this multifunctional flame retardant was used to enhance thermal properties and flame retardancy of epoxy resin. The addition of HM-SiO2@CS@PCL to the epoxy resin thermally destabilized the epoxy resin composite, but generated a higher char yield. Furthermore, HM-SiO2 played a critical role and generated synergies with CS and PCL to improve fire safety of the epoxy resin due to the multiple flame retardancy elements (P, N and Si). This multi-element, synergistic, flame-retardant system resulted in a remarkable reduction (51%) of peak heat release rate and a considerable removal of flammable decomposed products. Additionally, the incorporation of HM-SiO2@CS@PCL can sustainably recycle the epoxy resin into high value-added hollow carbon spheres during combustion. Therefore, the HM-SiO2@CS@PCL system provides a practical possibility for preparing recyclable polymer materials with multi-functions and high performances.Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO2@CS@PCL) as a green flame retardant through layer-by-layer assembly using hollow mesoporous silica (HM-SiO2), chitosan (CS) and phosphorylated cellulose (PCL). The electrostatic interactions deposited the CS/PCL coating on the surface of HM-SiO2. Subsequently, this multifunctional flame retardant was used to enhance thermal properties and flame retardancy of epoxy resin. The addition of HM-SiO2@CS@PCL to the epoxy resin thermally destabilized the epoxy resin composite, but generated a higher char yield. Furthermore, HM-SiO2 played a critical role and generated synergies with CS and PCL to improve fire safety of the epoxy resin due to the multiple flame retardancy elements (P, N and Si). This multi-element, synergistic, flame-retardant system resulted in a remarkable reduction (51%) of peak heat release rate and a considerable removal of flammable decomposed products. Additionally, the incorporation of HM-SiO2@CS@PCL can sustainably recycle the epoxy resin into high value-added hollow carbon spheres during combustion. Therefore, the HM-SiO2@CS@PCL system provides a practical possibility for preparing recyclable polymer materials with multi-functions and high performances.
Author	Huang, Zheng-Qi Tang, Gang Hu, Yuan Jiang, Shu-Dong Chen, Junmin
Author_xml	– sequence: 1 givenname: Shu-Dong surname: Jiang fullname: Jiang, Shu-Dong email: shudj@mail.ustc.edu.cn organization: Department of Fire Protection Engineering, Faculty of Geosciences and Environmental Engineering, Southwest Jiaotong University, The Western Park of the Hi-Tech Industrial Development Zone, Chengdu, Sichuan, PR China – sequence: 2 givenname: Gang surname: Tang fullname: Tang, Gang organization: School of Architecture and Civil Engineering, Anhui University of Technology, 59 Hudong Road, Ma’anshan, Anhui 243002, PR China – sequence: 3 givenname: Junmin surname: Chen fullname: Chen, Junmin organization: Department of Fire Protection Engineering, Faculty of Geosciences and Environmental Engineering, Southwest Jiaotong University, The Western Park of the Hi-Tech Industrial Development Zone, Chengdu, Sichuan, PR China – sequence: 4 givenname: Zheng-Qi surname: Huang fullname: Huang, Zheng-Qi organization: State Key Laboratory of Fire Science, University of Science and Technology of China, 96 Jinzhai Road, Hefei, Anhui 230026, PR China – sequence: 5 givenname: Yuan surname: Hu fullname: Hu, Yuan organization: School of Architecture and Civil Engineering, Anhui University of Technology, 59 Hudong Road, Ma’anshan, Anhui 243002, PR China
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Keywords	Epoxy resin Green flame retardant Hollow mesoporous silica Polyelectrolyte multilayer Sustainable recycling
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Snippet	•A green flame retardant (HM–SiO2@CS@PCL) was successfully synthesized through layer-by-layer assembly.•The integrated effect of HM–SiO2@CS@PCL endows epoxy... Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO @CS@PCL) as a green flame retardant through... Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO2@CS@PCL) as a green flame retardant through... Here, we describe a multifunctional biobased polyelectrolyte multilayer-coated hollow mesoporous silica (HM-SiO₂@CS@PCL) as a green flame retardant through...
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SubjectTerms	carbon cellulose chitosan coatings combustion electrolytes electrostatic interactions epoxides Epoxy resin fire safety flame retardants Green flame retardant heat Hollow mesoporous silica Polyelectrolyte multilayer polymers porous media silica silicon Sustainable recycling thermal properties value added
Title	Biobased polyelectrolyte multilayer-coated hollow mesoporous silica as a green flame retardant for epoxy resin
URI	https://dx.doi.org/10.1016/j.jhazmat.2017.09.001 https://www.ncbi.nlm.nih.gov/pubmed/28910653 https://www.proquest.com/docview/1957772728 https://www.proquest.com/docview/2101318316
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