Comparative SAXS study of heated and alkali-treated sisal fibers

The present investigation deals with the fine structural characteristics of heated and alkali‐treated sisal fiber using small‐angle X‐ray scattering (SAXS) technique for nonideal two‐phase systems. The SAXS intensities of heated and alkali‐treated sisal fibers deviate from Porod's law, indicati...

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Published inJournal of applied polymer science Vol. 125; no. 3; pp. 2356 - 2362
Main Authors Khan, Md. N., Bisoyi, D. K., Shukla, J.
Format Journal Article
LanguageEnglish
Published Hoboken Wiley Subscription Services, Inc., A Wiley Company 05.08.2012
Wiley
Wiley Subscription Services, Inc
Subjects
Applied sciences
correlation functions
Electron density
Exact sciences and technology
Fibers
Fibers and threads
Forms of application and semi-finished materials
lamellar model
Materials science
Phase boundaries
Polymer industry, paints, wood
Polymers
Reproduction
SAXS
Sisal
sisal fiber
Slits
Technology of polymers
Three dimensional
transverse periodicity
Mercerization
Heat treatment
sisal fiber
transverse periodicity
Plant fiber
Crystallinity
Sisal
Experimental study
correlation functions
SAXS
Structure processing relationship
lamellar model
Chemical treatment
Natural fiber
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Abstract The present investigation deals with the fine structural characteristics of heated and alkali‐treated sisal fiber using small‐angle X‐ray scattering (SAXS) technique for nonideal two‐phase systems. The SAXS intensities of heated and alkali‐treated sisal fibers deviate from Porod's law, indicating that the samples belong to nonideal two‐phase systems characterized by continuous variation of electron density at the phase boundary. The macromolecular parameters such as the average periodicity transverse to layers, specific inner surface, volume fractions of void and matter phases, and so on of the samples were evaluated by using one‐ and three‐dimensional correlation functions, which reveal all the information concealed in the slit smeared SAXS patterns. As all the samples under our purview of study have two‐phase structure with diffuse phase boundaries, the average thickness of the transition region have been determined. This analysis throws some light on the structural changes that occurred in the dewaxed sisal fiber treated by NaOH solutions and subject to heat treatments. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012
AbstractList The present investigation deals with the fine structural characteristics of heated and alkali‐treated sisal fiber using small‐angle X‐ray scattering (SAXS) technique for nonideal two‐phase systems. The SAXS intensities of heated and alkali‐treated sisal fibers deviate from Porod's law, indicating that the samples belong to nonideal two‐phase systems characterized by continuous variation of electron density at the phase boundary. The macromolecular parameters such as the average periodicity transverse to layers, specific inner surface, volume fractions of void and matter phases, and so on of the samples were evaluated by using one‐ and three‐dimensional correlation functions, which reveal all the information concealed in the slit smeared SAXS patterns. As all the samples under our purview of study have two‐phase structure with diffuse phase boundaries, the average thickness of the transition region have been determined. This analysis throws some light on the structural changes that occurred in the dewaxed sisal fiber treated by NaOH solutions and subject to heat treatments. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012
The present investigation deals with the fine structural characteristics of heated and alkali-treated sisal fiber using small-angle X-ray scattering (SAXS) technique for nonideal two-phase systems. The SAXS intensities of heated and alkali-treated sisal fibers deviate from Porod's law, indicating that the samples belong to nonideal two-phase systems characterized by continuous variation of electron density at the phase boundary. The macromolecular parameters such as the average periodicity transverse to layers, specific inner surface, volume fractions of void and matter phases, and so on of the samples were evaluated by using one- and three-dimensional correlation functions, which reveal all the information concealed in the slit smeared SAXS patterns. As all the samples under our purview of study have two-phase structure with diffuse phase boundaries, the average thickness of the transition region have been determined. This analysis throws some light on the structural changes that occurred in the dewaxed sisal fiber treated by NaOH solutions and subject to heat treatments. [copy 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012
The present investigation deals with the fine structural characteristics of heated and alkali-treated sisal fiber using small-angle X-ray scattering (SAXS) technique for nonideal two-phase systems. The SAXS intensities of heated and alkali-treated sisal fibers deviate from Porod's law, indicating that the samples belong to nonideal two-phase systems characterized by continuous variation of electron density at the phase boundary. The macromolecular parameters such as the average periodicity transverse to layers, specific inner surface, volume fractions of void and matter phases, and so on of the samples were evaluated by using one- and three-dimensional correlation functions, which reveal all the information concealed in the slit smeared SAXS patterns. As all the samples under our purview of study have two-phase structure with diffuse phase boundaries, the average thickness of the transition region have been determined. This analysis throws some light on the structural changes that occurred in the dewaxed sisal fiber treated by NaOH solutions and subject to heat treatments. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012 [PUBLICATION ABSTRACT]
Author Khan, Md. N.
Bisoyi, D. K.
Shukla, J.
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Issue 3
Keywords Mercerization
Heat treatment
sisal fiber
transverse periodicity
Plant fiber
Crystallinity
Sisal
Experimental study
correlation functions
SAXS
Structure processing relationship
lamellar model
Chemical treatment
Natural fiber
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Snippet The present investigation deals with the fine structural characteristics of heated and alkali‐treated sisal fiber using small‐angle X‐ray scattering (SAXS)...
The present investigation deals with the fine structural characteristics of heated and alkali-treated sisal fiber using small-angle X-ray scattering (SAXS)...
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SubjectTerms Applied sciences
correlation functions
Electron density
Exact sciences and technology
Fibers
Fibers and threads
Forms of application and semi-finished materials
lamellar model
Materials science
Phase boundaries
Polymer industry, paints, wood
Polymers
Reproduction
SAXS
Sisal
sisal fiber
Slits
Technology of polymers
Three dimensional
transverse periodicity
Title Comparative SAXS study of heated and alkali-treated sisal fibers
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https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fapp.36460
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https://www.proquest.com/docview/1439729014
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