Fabrication of xanthate-modified chitosan/poly(N-isopropylacrylamide) composite hydrogel for the selective adsorption of Cu(II), Pb(II) and Ni(II) metal ions

[Display omitted] •X-CS/NIPAAm composite hydrogel was fabricated as a good adsorbent for adsorption of Cu(II), Pb(II) and Ni(II).•The adsorption data fitted well to Langmuir model and the adsorption kinetics followed the pseudo-second order model.•Thermodynamics indicated the adsorption was an exoth...

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Published inChemical engineering research & design Vol. 139; pp. 197 - 210
Main Authors Wu, Shuping, Wang, Fan, Yuan, Haikuan, Zhang, Lijuan, Mao, Shimin, Liu, Xijian, Alharbi, Njud S., Rohani, Sohrab, Lu, Jie
Format Journal Article
LanguageEnglish
Published Rugby Elsevier B.V 01.11.2018
Elsevier Science Ltd
Subjects
Adsorption
Adsorption isotherm
Aqueous solutions
Chitosan
Copper
Equilibrium
Hydrogels
Isopropylacrylamide
Kinetics
Lead
Metal ions
Nickel
Selective adsorption
Systems analysis
Thermodynamics
X ray photoelectron spectroscopy
X-CS/NIPAAm composite
X-CS/NIPAAm composite
Kinetics
Adsorption
Adsorption isotherm
Metal ions
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Abstract [Display omitted] •X-CS/NIPAAm composite hydrogel was fabricated as a good adsorbent for adsorption of Cu(II), Pb(II) and Ni(II).•The adsorption data fitted well to Langmuir model and the adsorption kinetics followed the pseudo-second order model.•Thermodynamics indicated the adsorption was an exothermic and spontaneous process.•X-CS/NIPAAm could be reused and regenerated at least five recycles. A novel xanthate-modified chitosan/poly(N-isopropylacrylamide) (X-CS/NIPAAm) composite hydrogel was fabricated by a facile two-step method for the selective adsorption of Cu(II), Pb(II) and Ni(II) metal ions from aqueous solutions. The equilibrium adsorption data fitted well to the Langmuir model and the adsorption kinetic data followed the pseudo-second-order model. The maximum equilibrium adsorption capacities of composite hydrogel to Cu(II), Pb(II) and Ni(II) at 293K were about 115.1, 172.0 and 66.9mgg−1, respectively. The thermodynamics parameters showed that the adsorption processes to Cu(II), Pb(II) and Ni(II) were spontaneous and exothermic. The interactions between metal ions for multi-components systems were evaluated by the values of Qb/Qs and Qt/Qs. The adsorption mechanism was analyzed by XPS spectra and the Hard–Soft, Acids–Bases (HSAB) theory. The X-CS/NIPAAm composite hydrogel could be regenerated and repeatedly utilized at least five cycles without obvious adsorption capacity loss.
AbstractList A novel xanthate-modified chitosan/poly(N-isopropylacrylamide) (X-CS/NIPAAm) composite hydrogel was fabricated by a facile two-step method for the selective adsorption of Cu(II), Pb(II) and Ni(II) metal ions from aqueous solutions. The equilibrium adsorption data fitted well to the Langmuir model and the adsorption kinetic data followed the pseudo-second-order model. The maximum equilibrium adsorption capacities of composite hydrogel to Cu(II), Pb(II) and Ni(II) at 293 K were about 115.1, 172.0 and 66.9 mg g−1, respectively. The thermodynamics parameters showed that the adsorption processes to Cu(II), Pb(II) and Ni(II) were spontaneous and exothermic. The interactions between metal ions for multi-components systems were evaluated by the values of Qb/Qs and Qt/Qs. The adsorption mechanism was analyzed by XPS spectra and the Hard–Soft, Acids–Bases (HSAB) theory. The X-CS/NIPAAm composite hydrogel could be regenerated and repeatedly utilized at least five cycles without obvious adsorption capacity loss.
[Display omitted] •X-CS/NIPAAm composite hydrogel was fabricated as a good adsorbent for adsorption of Cu(II), Pb(II) and Ni(II).•The adsorption data fitted well to Langmuir model and the adsorption kinetics followed the pseudo-second order model.•Thermodynamics indicated the adsorption was an exothermic and spontaneous process.•X-CS/NIPAAm could be reused and regenerated at least five recycles. A novel xanthate-modified chitosan/poly(N-isopropylacrylamide) (X-CS/NIPAAm) composite hydrogel was fabricated by a facile two-step method for the selective adsorption of Cu(II), Pb(II) and Ni(II) metal ions from aqueous solutions. The equilibrium adsorption data fitted well to the Langmuir model and the adsorption kinetic data followed the pseudo-second-order model. The maximum equilibrium adsorption capacities of composite hydrogel to Cu(II), Pb(II) and Ni(II) at 293K were about 115.1, 172.0 and 66.9mgg−1, respectively. The thermodynamics parameters showed that the adsorption processes to Cu(II), Pb(II) and Ni(II) were spontaneous and exothermic. The interactions between metal ions for multi-components systems were evaluated by the values of Qb/Qs and Qt/Qs. The adsorption mechanism was analyzed by XPS spectra and the Hard–Soft, Acids–Bases (HSAB) theory. The X-CS/NIPAAm composite hydrogel could be regenerated and repeatedly utilized at least five cycles without obvious adsorption capacity loss.
Author Liu, Xijian
Wu, Shuping
Lu, Jie
Yuan, Haikuan
Alharbi, Njud S.
Zhang, Lijuan
Rohani, Sohrab
Wang, Fan
Mao, Shimin
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  organization: School of Chemistry and Chemical Engineering, Shanghai University of Engineering Science, Shanghai 201620, China
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  organization: Department of Chemical and Biochemical Engineering, The University of Western Ontario, London, Ontario N6A 5B9, Canada
– sequence: 6
  givenname: Xijian
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  fullname: Liu, Xijian
  email: liuxijian@sues.edu.cn
  organization: School of Chemistry and Chemical Engineering, Shanghai University of Engineering Science, Shanghai 201620, China
– sequence: 7
  givenname: Njud S.
  surname: Alharbi
  fullname: Alharbi, Njud S.
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  organization: Biotechnology Research Group, Department of Biological Sciences, Faculty of Science, King Abdulaziz University, Jeddah, Saudi Arabia
– sequence: 8
  givenname: Sohrab
  surname: Rohani
  fullname: Rohani, Sohrab
  email: srohani@uwo.ca
  organization: Department of Chemical and Biochemical Engineering, The University of Western Ontario, London, Ontario N6A 5B9, Canada
– sequence: 9
  givenname: Jie
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  organization: School of Chemistry and Chemical Engineering, Shanghai University of Engineering Science, Shanghai 201620, China
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Kinetics
Adsorption
Adsorption isotherm
Metal ions
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  ident: 10.1016/j.cherd.2018.09.035_bib0105
  article-title: Chitosan/(polyvinyl alcohol)/zeolite electrospun composite nanofibrous membrane for adsorption of Cr6+, Fe3+ and Ni2+
  publication-title: J. Hazard. Mater.
  doi: 10.1016/j.jhazmat.2016.06.028
  contributor:
    fullname: Habiba
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Snippet [Display omitted] •X-CS/NIPAAm composite hydrogel was fabricated as a good adsorbent for adsorption of Cu(II), Pb(II) and Ni(II).•The adsorption data fitted...
A novel xanthate-modified chitosan/poly(N-isopropylacrylamide) (X-CS/NIPAAm) composite hydrogel was fabricated by a facile two-step method for the selective...
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SubjectTerms Adsorption
Adsorption isotherm
Aqueous solutions
Chitosan
Copper
Equilibrium
Hydrogels
Isopropylacrylamide
Kinetics
Lead
Metal ions
Nickel
Selective adsorption
Systems analysis
Thermodynamics
X ray photoelectron spectroscopy
X-CS/NIPAAm composite
Title Fabrication of xanthate-modified chitosan/poly(N-isopropylacrylamide) composite hydrogel for the selective adsorption of Cu(II), Pb(II) and Ni(II) metal ions
URI https://dx.doi.org/10.1016/j.cherd.2018.09.035
https://www.proquest.com/docview/2157467643
Volume 139
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