Few-layer MoS2-encapsulated Cu nanoparticle hybrids fabricated by two-step annealing process for surface enhanced Raman scattering
Here we designed a new kind of SERS substrate referred to as a MoS2-coated Cu nanopaticles (MoS2@CuNPs) substrate for R6G detection. The Cu nanoparticles wrapped by a thin MoS2 film were directly synthesized on flat quartz by two annealing process in a mixture of argon and hydrogen. Signals from a M...
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| Published in | Sensors and actuators. B, Chemical Vol. 230; pp. 645 - 652 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
01.07.2016
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| Abstract | Here we designed a new kind of SERS substrate referred to as a MoS2-coated Cu nanopaticles (MoS2@CuNPs) substrate for R6G detection. The Cu nanoparticles wrapped by a thin MoS2 film were directly synthesized on flat quartz by two annealing process in a mixture of argon and hydrogen. Signals from a MoS2@CuNPs SERS substrate were also demonstrated to have interesting advantages over pure CuNPs SERS, in terms of the excellent linear relationship between Raman intensity and analyte concentration, strongly background fluorescence quenching and being more stable against photo-induced damage and oxidation. The minimum detectable concentrations of R6G on MoS2@CuNPs hybrids can be as low as 10−9M which is one order lower than that on the pure CuNPs substrates. This synthetic approach is facile, scalable and applicable to the MoS2 film compound with other metals such as Ag, Au etc. |
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| AbstractList | Here we designed a new kind of SERS substrate referred to as a MoS2-coated Cu nanopaticles (MoS2uNPs) substrate for R6G detection. The Cu nanoparticles wrapped by a thin MoS2 film were directly synthesized on flat quartz by two annealing process in a mixture of argon and hydrogen. Signals from a MoS2uNPs SERS substrate were also demonstrated to have interesting advantages over pure CuNPs SERS, in terms of the excellent linear relationship between Raman intensity and analyte concentration, strongly background fluorescence quenching and being more stable against photo-induced damage and oxidation. The minimum detectable concentrations of R6G on MoS2uNPs hybrids can be as low as 10-9 M which is one order lower than that on the pure CuNPs substrates. This synthetic approach is facile, scalable and applicable to the MoS2 film compound with other metals such as Ag, Au etc. Here we designed a new kind of SERS substrate referred to as a MoS2-coated Cu nanopaticles (MoS2@CuNPs) substrate for R6G detection. The Cu nanoparticles wrapped by a thin MoS2 film were directly synthesized on flat quartz by two annealing process in a mixture of argon and hydrogen. Signals from a MoS2@CuNPs SERS substrate were also demonstrated to have interesting advantages over pure CuNPs SERS, in terms of the excellent linear relationship between Raman intensity and analyte concentration, strongly background fluorescence quenching and being more stable against photo-induced damage and oxidation. The minimum detectable concentrations of R6G on MoS2@CuNPs hybrids can be as low as 10−9M which is one order lower than that on the pure CuNPs substrates. This synthetic approach is facile, scalable and applicable to the MoS2 film compound with other metals such as Ag, Au etc. |
| Author | Qiu, Hengwei Yang, Cheng Li, Zhen Huo, Yanyan Xu, Shicai Zhang, Chao Jiang, Shouzhen Li, Chonghui Sheng, Yingqiang Man, Baoyuan |
| Author_xml | – sequence: 1 givenname: Zhen surname: Li fullname: Li, Zhen organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 2 givenname: Shouzhen surname: Jiang fullname: Jiang, Shouzhen organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 3 givenname: Shicai surname: Xu fullname: Xu, Shicai organization: College of Physics and Electronic Information, Shandong Provincial Key Laboratory of Functional Macromolecular Biophysics, Dezhou University, Dezhou 253023, China – sequence: 4 givenname: Chao surname: Zhang fullname: Zhang, Chao organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 5 givenname: Hengwei surname: Qiu fullname: Qiu, Hengwei organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 6 givenname: Chonghui surname: Li fullname: Li, Chonghui organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 7 givenname: Yingqiang surname: Sheng fullname: Sheng, Yingqiang organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 8 givenname: Yanyan surname: Huo fullname: Huo, Yanyan organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 9 givenname: Cheng surname: Yang fullname: Yang, Cheng organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China – sequence: 10 givenname: Baoyuan surname: Man fullname: Man, Baoyuan email: byman@sdnu.edu.cn organization: College of Physics and Electronics, Shandong Normal University, Jinan 250014, China |
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| Snippet | Here we designed a new kind of SERS substrate referred to as a MoS2-coated Cu nanopaticles (MoS2@CuNPs) substrate for R6G detection. The Cu nanoparticles... Here we designed a new kind of SERS substrate referred to as a MoS2-coated Cu nanopaticles (MoS2uNPs) substrate for R6G detection. The Cu nanoparticles wrapped... |
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| SubjectTerms | Annealing ANNEALING PROCESSES Cu nanoparticle FABRICATION Fluorescence Hydrogen MICROSTRUCTURES Molybdenum disulfide MoS2 Nanostructure PARTICLES QUENCHING MECHANISMS R6G Raman scattering SCATTERING SERS Silver Substrates |
| Title | Few-layer MoS2-encapsulated Cu nanoparticle hybrids fabricated by two-step annealing process for surface enhanced Raman scattering |
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