A review on recent developments in electrochemical hydrogen peroxide synthesis with a critical assessment of perspectives and strategies

Electrochemical hydrogen peroxide synthesis using two-electron oxygen electrochemistry is an intriguing alternative to currently dominating environmentally unfriendly and potentially hazardous anthraquinone process and noble metals catalysed direct synthesis. Electrocatalytic two-electron oxygen red...

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Published inAdvances in colloid and interface science Vol. 287; p. 102331
Main Authors Anantharaj, Sengeni, Pitchaimuthu, Sudhagar, Noda, Suguru
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier B.V 01.01.2021
Subjects
Electrocatalysis
Electrochemical synthesis
H2O2 generation
Oxygen reduction reaction
Water oxidation reaction
Electrocatalysis
Water oxidation reaction
H2O2 generation
Oxygen reduction reaction
Electrochemical synthesis
HO generation
Online AccessGet full text
ISSN0001-8686
1873-3727
1873-3727
DOI10.1016/j.cis.2020.102331

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Abstract Electrochemical hydrogen peroxide synthesis using two-electron oxygen electrochemistry is an intriguing alternative to currently dominating environmentally unfriendly and potentially hazardous anthraquinone process and noble metals catalysed direct synthesis. Electrocatalytic two-electron oxygen reduction reaction (ORR) and water oxidation reaction (WOR) are the source of electrochemical hydrogen peroxide generation. Various electrocatalysts have been used for the same and were characterized using several electroanalytical, chemical, spectroscopic and chromatographic tools. Though there have been a few reviews summarizing the recent developments in this field, none of them have unified the approaches in catalysts' design, criticized the ambiguities and flaws in the methods of evaluation, and emphasized the role of electrolyte engineering. Hence, we dedicated this review to discuss the recent trends in the catalysts' design, performance optimization, evaluation perspectives and their appropriateness and opportunities with electrolyte engineering. In addition, particularized discussions on fundamental oxygen electrochemistry, additional methods for precise screening, and the role of solution chemistry of synthesized hydrogen peroxide are also presented. Thus, this review discloses the state-of-the-art in an unpresented view highlighting the challenges, opportunities, and alternative perspectives. This review analyzes the recent developments of electrochemical synthesis of H2O2 in terms of both catalysts' design and evaluation perspectives while predicting the direction of future growth. [Display omitted] •Trends in 2 electron ORR and WOR catalysts are critically analyzed.•Ambiguities in evaluation perspectives are criticized and alternatives are proposed.•Fundamentals of oxygen interfacial electrochemistry is elaborated to understand the trends.•Advantages of 2 electron WOR over 2 electron ORR in H2O2 electrosynthesis is emphasized.•Need for electrolyte engineering strategies to improve productivity and selectivity is discussed.
AbstractList Electrochemical hydrogen peroxide synthesis using two-electron oxygen electrochemistry is an intriguing alternative to currently dominating environmentally unfriendly and potentially hazardous anthraquinone process and noble metals catalysed direct synthesis. Electrocatalytic two-electron oxygen reduction reaction (ORR) and water oxidation reaction (WOR) are the source of electrochemical hydrogen peroxide generation. Various electrocatalysts have been used for the same and were characterized using several electroanalytical, chemical, spectroscopic and chromatographic tools. Though there have been a few reviews summarizing the recent developments in this field, none of them have unified the approaches in catalysts' design, criticized the ambiguities and flaws in the methods of evaluation, and emphasized the role of electrolyte engineering. Hence, we dedicated this review to discuss the recent trends in the catalysts' design, performance optimization, evaluation perspectives and their appropriateness and opportunities with electrolyte engineering. In addition, particularized discussions on fundamental oxygen electrochemistry, additional methods for precise screening, and the role of solution chemistry of synthesized hydrogen peroxide are also presented. Thus, this review discloses the state-of-the-art in an unpresented view highlighting the challenges, opportunities, and alternative perspectives.Electrochemical hydrogen peroxide synthesis using two-electron oxygen electrochemistry is an intriguing alternative to currently dominating environmentally unfriendly and potentially hazardous anthraquinone process and noble metals catalysed direct synthesis. Electrocatalytic two-electron oxygen reduction reaction (ORR) and water oxidation reaction (WOR) are the source of electrochemical hydrogen peroxide generation. Various electrocatalysts have been used for the same and were characterized using several electroanalytical, chemical, spectroscopic and chromatographic tools. Though there have been a few reviews summarizing the recent developments in this field, none of them have unified the approaches in catalysts' design, criticized the ambiguities and flaws in the methods of evaluation, and emphasized the role of electrolyte engineering. Hence, we dedicated this review to discuss the recent trends in the catalysts' design, performance optimization, evaluation perspectives and their appropriateness and opportunities with electrolyte engineering. In addition, particularized discussions on fundamental oxygen electrochemistry, additional methods for precise screening, and the role of solution chemistry of synthesized hydrogen peroxide are also presented. Thus, this review discloses the state-of-the-art in an unpresented view highlighting the challenges, opportunities, and alternative perspectives.
Electrochemical hydrogen peroxide synthesis using two-electron oxygen electrochemistry is an intriguing alternative to currently dominating environmentally unfriendly and potentially hazardous anthraquinone process and noble metals catalysed direct synthesis. Electrocatalytic two-electron oxygen reduction reaction (ORR) and water oxidation reaction (WOR) are the source of electrochemical hydrogen peroxide generation. Various electrocatalysts have been used for the same and were characterized using several electroanalytical, chemical, spectroscopic and chromatographic tools. Though there have been a few reviews summarizing the recent developments in this field, none of them have unified the approaches in catalysts' design, criticized the ambiguities and flaws in the methods of evaluation, and emphasized the role of electrolyte engineering. Hence, we dedicated this review to discuss the recent trends in the catalysts' design, performance optimization, evaluation perspectives and their appropriateness and opportunities with electrolyte engineering. In addition, particularized discussions on fundamental oxygen electrochemistry, additional methods for precise screening, and the role of solution chemistry of synthesized hydrogen peroxide are also presented. Thus, this review discloses the state-of-the-art in an unpresented view highlighting the challenges, opportunities, and alternative perspectives. This review analyzes the recent developments of electrochemical synthesis of H2O2 in terms of both catalysts' design and evaluation perspectives while predicting the direction of future growth. [Display omitted] •Trends in 2 electron ORR and WOR catalysts are critically analyzed.•Ambiguities in evaluation perspectives are criticized and alternatives are proposed.•Fundamentals of oxygen interfacial electrochemistry is elaborated to understand the trends.•Advantages of 2 electron WOR over 2 electron ORR in H2O2 electrosynthesis is emphasized.•Need for electrolyte engineering strategies to improve productivity and selectivity is discussed.
Electrochemical hydrogen peroxide synthesis using two-electron oxygen electrochemistry is an intriguing alternative to currently dominating environmentally unfriendly and potentially hazardous anthraquinone process and noble metals catalysed direct synthesis. Electrocatalytic two-electron oxygen reduction reaction (ORR) and water oxidation reaction (WOR) are the source of electrochemical hydrogen peroxide generation. Various electrocatalysts have been used for the same and were characterized using several electroanalytical, chemical, spectroscopic and chromatographic tools. Though there have been a few reviews summarizing the recent developments in this field, none of them have unified the approaches in catalysts' design, criticized the ambiguities and flaws in the methods of evaluation, and emphasized the role of electrolyte engineering. Hence, we dedicated this review to discuss the recent trends in the catalysts' design, performance optimization, evaluation perspectives and their appropriateness and opportunities with electrolyte engineering. In addition, particularized discussions on fundamental oxygen electrochemistry, additional methods for precise screening, and the role of solution chemistry of synthesized hydrogen peroxide are also presented. Thus, this review discloses the state-of-the-art in an unpresented view highlighting the challenges, opportunities, and alternative perspectives.
ArticleNumber 102331
Author Anantharaj, Sengeni
Pitchaimuthu, Sudhagar
Noda, Suguru
Author_xml – sequence: 1
  givenname: Sengeni
  surname: Anantharaj
  fullname: Anantharaj, Sengeni
  email: anantharaj1402@gmail.com, w.iac19088@kurenai.waseda.jp
  organization: Department of Applied Chemistry, School of Advanced Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
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  givenname: Sudhagar
  surname: Pitchaimuthu
  fullname: Pitchaimuthu, Sudhagar
  email: S.Pitchaimuthu@swansea.ac.uk
  organization: Multi-functional Photocatalyst and Coatings Group, SPECIFIC, Materials Research Center, College of Engineering, Swansea University (Bay Campus), Swansea SA1 8EN, Wales, United Kingdom
– sequence: 3
  givenname: Suguru
  surname: Noda
  fullname: Noda, Suguru
  email: noda@waseda.jp
  organization: Department of Applied Chemistry, School of Advanced Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
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Keywords Electrocatalysis
Water oxidation reaction
H2O2 generation
Oxygen reduction reaction
Electrochemical synthesis
HO generation
Language English
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Snippet Electrochemical hydrogen peroxide synthesis using two-electron oxygen electrochemistry is an intriguing alternative to currently dominating environmentally...
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SubjectTerms Electrocatalysis
Electrochemical synthesis
H2O2 generation
Oxygen reduction reaction
Water oxidation reaction
Title A review on recent developments in electrochemical hydrogen peroxide synthesis with a critical assessment of perspectives and strategies
URI https://dx.doi.org/10.1016/j.cis.2020.102331
https://www.ncbi.nlm.nih.gov/pubmed/33321333
https://www.proquest.com/docview/2470629426
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