Encapsulated FeP nanoparticles with in-situ formed P-doped graphene layers: Boosting activity in oxygen reduction reaction
Nonprecious metal-based oxygen reduction reaction (ORR) electrocatalysts with high efficiency in both alkaline and acidic media are being intensively studied for the purpose of replacing expensive Pt-based catalysts; however, it is still a challenge to achieve superior ORR performances, especially i...
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Published in | Science China materials Vol. 64; no. 5; pp. 1159 - 1172 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
Beijing
Science China Press
01.05.2021
Springer Nature B.V |
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Abstract | Nonprecious metal-based oxygen reduction reaction (ORR) electrocatalysts with high efficiency in both alkaline and acidic media are being intensively studied for the purpose of replacing expensive Pt-based catalysts; however, it is still a challenge to achieve superior ORR performances, especially in acidic media. Herein, by pyrolysis of mixed precursors of diammonium phosphate, melamine and hemin, we prepared a nanocomposite catalyst (denoted as FeP@PGL) composed of nitrogen-doped carbon nanosheets with embedded FeP nanoparticles (NPs), which were encapsulated by
in-situ
formed phosphorus-doped graphene layers. It is found that phosphorous was preferentially doped in the coating layers on FeP NPs, instead of in the carbon nanosheets. The FeP@PGL catalyst exhibited excellent ORR performance, with the onset and half-wave potential up to 1.01 and 0.90 V
vs.
the reversible hydrogen electrode (RHE) in alkaline media, and 0.95 and 0.81 V
vs.
RHE in acidic media, respectively. By thorough microscopy and spectroscopy characterizations, the interfacial charge transfer between the encapsulated FeP NPs and P-doped graphene layers was identified, and the local work function of the catalyst surface was also reduced by the interfacial interaction. The interfacial synergy between the encapsulated FeP and phosphorus-doped graphene layers was essential to enhance the ORR performance. This study not only demonstrates the promising ORR properties of the encapsulated-FeP-based nanocomposite catalyst, but also provides direct evidence of the interfacial charge transfer effect and its role in ORR process. |
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AbstractList | Nonprecious metal-based oxygen reduction reaction (ORR) electrocatalysts with high efficiency in both alkaline and acidic media are being intensively studied for the purpose of replacing expensive Pt-based catalysts; however, it is still a challenge to achieve superior ORR performances, especially in acidic media. Herein, by pyrolysis of mixed precursors of diammonium phosphate, melamine and hemin, we prepared a nanocomposite catalyst (denoted as FeP@PGL) composed of nitrogen-doped carbon nanosheets with embedded FeP nanoparticles (NPs), which were encapsulated by in-situ formed phosphorus-doped graphene layers. It is found that phosphorous was preferentially doped in the coating layers on FeP NPs, instead of in the carbon nanosheets. The FeP@PGL catalyst exhibited excellent ORR performance, with the onset and half-wave potential up to 1.01 and 0.90 V vs. the reversible hydrogen electrode (RHE) in alkaline media, and 0.95 and 0.81 V vs. RHE in acidic media, respectively. By thorough microscopy and spectroscopy characterizations, the interfacial charge transfer between the encapsulated FeP NPs and P-doped graphene layers was identified, and the local work function of the catalyst surface was also reduced by the interfacial interaction. The interfacial synergy between the encapsulated FeP and phosphorus-doped graphene layers was essential to enhance the ORR performance. This study not only demonstrates the promising ORR properties of the encapsulated-FeP-based nanocomposite catalyst, but also provides direct evidence of the interfacial charge transfer effect and its role in ORR process. Nonprecious metal-based oxygen reduction reaction (ORR) electrocatalysts with high efficiency in both alkaline and acidic media are being intensively studied for the purpose of replacing expensive Pt-based catalysts; however, it is still a challenge to achieve superior ORR performances, especially in acidic media. Herein, by pyrolysis of mixed precursors of diammonium phosphate, melamine and hemin, we prepared a nanocomposite catalyst (denoted as FeP@PGL) composed of nitrogen-doped carbon nanosheets with embedded FeP nanoparticles (NPs), which were encapsulated by in-situ formed phosphorus-doped graphene layers. It is found that phosphorous was preferentially doped in the coating layers on FeP NPs, instead of in the carbon nanosheets. The FeP@PGL catalyst exhibited excellent ORR performance, with the onset and half-wave potential up to 1.01 and 0.90 V vs. the reversible hydrogen electrode (RHE) in alkaline media, and 0.95 and 0.81 V vs. RHE in acidic media, respectively. By thorough microscopy and spectroscopy characterizations, the interfacial charge transfer between the encapsulated FeP NPs and P-doped graphene layers was identified, and the local work function of the catalyst surface was also reduced by the interfacial interaction. The interfacial synergy between the encapsulated FeP and phosphorus-doped graphene layers was essential to enhance the ORR performance. This study not only demonstrates the promising ORR properties of the encapsulated-FeP-based nanocomposite catalyst, but also provides direct evidence of the interfacial charge transfer effect and its role in ORR process. |
Author | Wu, Luming Sun, Pingchuan Chen, Rui Chen, Tiehong Ni, Baoxia |
Author_xml | – sequence: 1 givenname: Baoxia surname: Ni fullname: Ni, Baoxia organization: Institute of New Catalytic Materials Science, School of Materials Science and Engineering, Key Laboratory of Advanced Energy Materials Chemistry (MOE), Nankai University – sequence: 2 givenname: Rui surname: Chen fullname: Chen, Rui organization: Institute of New Catalytic Materials Science, School of Materials Science and Engineering, Key Laboratory of Advanced Energy Materials Chemistry (MOE), Nankai University – sequence: 3 givenname: Luming surname: Wu fullname: Wu, Luming organization: Institute of New Catalytic Materials Science, School of Materials Science and Engineering, Key Laboratory of Advanced Energy Materials Chemistry (MOE), Nankai University – sequence: 4 givenname: Pingchuan surname: Sun fullname: Sun, Pingchuan organization: Key Laboratory of Functional Polymer Materials (MOE), College of Chemistry, Nankai University – sequence: 5 givenname: Tiehong surname: Chen fullname: Chen, Tiehong email: chenth@nankai.edu.cn organization: Institute of New Catalytic Materials Science, School of Materials Science and Engineering, Key Laboratory of Advanced Energy Materials Chemistry (MOE), Nankai University |
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DocumentTitle_FL | 磷氮掺杂石墨烯层封装FeP纳米颗粒的增强ORR 催化性能 |
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Snippet | Nonprecious metal-based oxygen reduction reaction (ORR) electrocatalysts with high efficiency in both alkaline and acidic media are being intensively studied... |
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SubjectTerms | Carbon Catalysts Charge transfer Chemistry and Materials Science Chemistry/Food Science Electrocatalysts Encapsulation Graphene Materials Science Melamine Nanocomposites Nanoparticles Nanostructure Oxygen reduction reactions Phosphorus Pyrolysis Work functions |
Title | Encapsulated FeP nanoparticles with in-situ formed P-doped graphene layers: Boosting activity in oxygen reduction reaction |
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