Vanadium phosphorus oxide catalyst modified by silver doping for mild oxidation of styrene to benzaldehyde
A series of silver-doped vanadium phosphorus oxides (Ag-VPO) catalysts were prepared by in situ synthesis, the catalytic tests showed that silver component significantly increased the overall activity for the oxidation of styrene by tert-butyl hydroperoxide (TBHP). It is interesting that Ag-VPO cata...
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| Published in | Chemical engineering journal (Lausanne, Switzerland : 1996) Vol. 151; no. 1; pp. 319 - 323 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Elsevier B.V
15.08.2009
Elsevier |
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| Abstract | A series of silver-doped vanadium phosphorus oxides (Ag-VPO) catalysts were prepared by in situ synthesis, the catalytic tests showed that silver component significantly increased the overall activity for the oxidation of styrene by
tert-butyl hydroperoxide (TBHP). It is interesting that Ag-VPO catalysts show no epoxidation selectivity but good selectivity for benzaldehyde in this study. To investigate the origin of the silver effect, the solids were characterized using X-ray diffraction (XRD), Fourier transformed-infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS) and other instruments, the (VO)
2P
2O
7, β-VOPO
4, Ag(V
2P
2O
10) and Ag
2(VO
2)(PO
4) phases were detected in all the Ag-VPO catalysts. This study also confirms that ratios of
P/
V play a crucial role in the activity and the selectivity of the catalyst, meanwhile, the other factors, such as solvent, oxidant concentration, reaction time, also have been investigated and reaction conditions are optimized. |
|---|---|
| AbstractList | A series of silver-doped vanadium phosphorus oxides (Ag-VPO) catalysts were prepared by in situ synthesis, the catalytic tests showed that silver component significantly increased the overall activity for the oxidation of styrene by
tert-butyl hydroperoxide (TBHP). It is interesting that Ag-VPO catalysts show no epoxidation selectivity but good selectivity for benzaldehyde in this study. To investigate the origin of the silver effect, the solids were characterized using X-ray diffraction (XRD), Fourier transformed-infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS) and other instruments, the (VO)
2P
2O
7, β-VOPO
4, Ag(V
2P
2O
10) and Ag
2(VO
2)(PO
4) phases were detected in all the Ag-VPO catalysts. This study also confirms that ratios of
P/
V play a crucial role in the activity and the selectivity of the catalyst, meanwhile, the other factors, such as solvent, oxidant concentration, reaction time, also have been investigated and reaction conditions are optimized. A series of silver-doped vanadium phosphorus oxides (Ag-VPO) catalysts were prepared by in situ synthesis, the catalytic tests showed that silver component significantly increased the overall activity for the oxidation of styrene by tert-butyl hydroperoxide (TBHP). It is interesting that Ag-VPO catalysts show no epoxidation selectivity but good selectivity for benzaldehyde in this study. To investigate the origin of the silver effect, the solids were characterized using X-ray diffraction (XRD), Fourier transformed-infrared spectroscopy (FT-IR), X-ray photoelectron spectroscopy (XPS) and other instruments, the (VO)(2)P(2)O(7), b-VOPO(4), Ag(V(2)P(2)O(10)) and Ag(2)(VO(2))(PO(4)) phases were detected in all the Ag-VPO catalysts. This study also confirms that ratios of P/V play a crucial role in the activity and the selectivity of the catalyst, meanwhile, the other factors, such as solvent, oxidant concentration, reaction time, also have been investigated and reaction conditions are optimized. |
| Author | Wang, Fang Xu, Xianlun Liu, Junhua Gu, Zhenggui |
| Author_xml | – sequence: 1 givenname: Junhua surname: Liu fullname: Liu, Junhua email: liujh2010@yahoo.cn organization: College of Chemistry and Environmental Science, Nanjing Normal University, 122# Ninghai Road, Nanjing 210097, China – sequence: 2 givenname: Fang surname: Wang fullname: Wang, Fang organization: State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China – sequence: 3 givenname: Zhenggui surname: Gu fullname: Gu, Zhenggui organization: College of Chemistry and Environmental Science, Nanjing Normal University, 122# Ninghai Road, Nanjing 210097, China – sequence: 4 givenname: Xianlun surname: Xu fullname: Xu, Xianlun organization: State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China |
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| Keywords | Selective oxidation Silver VPO Doping Styrene Catalytic reaction Instruments In situ Oxidant X ray diffraction Epoxidation Oxidation Fourier-transformed infrared spectrometry Catalyst |
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| SubjectTerms | Applied sciences Catalysis Catalytic reactions Chemical engineering Chemistry Doping Exact sciences and technology General and physical chemistry Reactors Selective oxidation Silver Styrene Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry VPO |
| Title | Vanadium phosphorus oxide catalyst modified by silver doping for mild oxidation of styrene to benzaldehyde |
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