Partially amorphous nickel–iron layered double hydroxide nanosheet arrays for robust bifunctional electrocatalysis
Bifunctional electrocatalysts that can boost energy-related reactions are urgently in demand for pursual of dual and even multiple targets towards practical applications such as energy conversion, clean fuel production and pollution treatment. Herein, we highlight that an in situ grown nickel–iron l...
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| Published in | Journal of materials chemistry. A, Materials for energy and sustainability Vol. 6; no. 33; pp. 16121 - 16129 |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Cambridge
Royal Society of Chemistry
2018
|
| Subjects | |
| Online Access | Get full text |
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| Abstract | Bifunctional electrocatalysts that can boost energy-related reactions are urgently in demand for pursual of dual and even multiple targets towards practical applications such as energy conversion, clean fuel production and pollution treatment. Herein, we highlight that an
in situ
grown nickel–iron layered double hydroxide (NiFe LDH) nanosheet array catalyst with partially amorphous characteristics, rich native Ni
3+
ions and an optimal Ni : Fe ratio can exhibit robust performances on both the oxygen evolution reaction (OER) and the urea oxidation reaction (UOR). Benefitting from the partially amorphous feature, the catalytically active high-valence species are easy to generate and stabilize, thus further realizing enhanced electrooxidation activity with the aid of an internal 2D charge transfer pathway and native Ni
3+
ions. As expected, the partially amorphous catalyst exhibits a higher OER current of 284.4 mA cm
−2
at an overpotential of 500 mV, which shows 2.2–10.0 times enhancement than the counterparts with various Ni : Fe ratios. In addition, the UOR current density of the partially amorphous catalyst at 1.8 V
vs.
RHE shows 1.6 and 2.4 times increment relative to fully amorphous and highly crystalline catalysts, and 2.7–9.4 fold larger than the catalysts with other Ni : Fe ratios. The optimization strategy of designing the partially amorphous bifunctional catalyst in this work may broaden the way of searching for advanced electrocatalysts for simultaneous waste water treatment and clean energy production. |
|---|---|
| AbstractList | Bifunctional electrocatalysts that can boost energy-related reactions are urgently in demand for pursual of dual and even multiple targets towards practical applications such as energy conversion, clean fuel production and pollution treatment. Herein, we highlight that an in situ grown nickel–iron layered double hydroxide (NiFe LDH) nanosheet array catalyst with partially amorphous characteristics, rich native Ni3+ ions and an optimal Ni : Fe ratio can exhibit robust performances on both the oxygen evolution reaction (OER) and the urea oxidation reaction (UOR). Benefitting from the partially amorphous feature, the catalytically active high-valence species are easy to generate and stabilize, thus further realizing enhanced electrooxidation activity with the aid of an internal 2D charge transfer pathway and native Ni3+ ions. As expected, the partially amorphous catalyst exhibits a higher OER current of 284.4 mA cm−2 at an overpotential of 500 mV, which shows 2.2–10.0 times enhancement than the counterparts with various Ni : Fe ratios. In addition, the UOR current density of the partially amorphous catalyst at 1.8 V vs. RHE shows 1.6 and 2.4 times increment relative to fully amorphous and highly crystalline catalysts, and 2.7–9.4 fold larger than the catalysts with other Ni : Fe ratios. The optimization strategy of designing the partially amorphous bifunctional catalyst in this work may broaden the way of searching for advanced electrocatalysts for simultaneous waste water treatment and clean energy production. Bifunctional electrocatalysts that can boost energy-related reactions are urgently in demand for pursual of dual and even multiple targets towards practical applications such as energy conversion, clean fuel production and pollution treatment. Herein, we highlight that an in situ grown nickel–iron layered double hydroxide (NiFe LDH) nanosheet array catalyst with partially amorphous characteristics, rich native Ni³⁺ ions and an optimal Ni : Fe ratio can exhibit robust performances on both the oxygen evolution reaction (OER) and the urea oxidation reaction (UOR). Benefitting from the partially amorphous feature, the catalytically active high-valence species are easy to generate and stabilize, thus further realizing enhanced electrooxidation activity with the aid of an internal 2D charge transfer pathway and native Ni³⁺ ions. As expected, the partially amorphous catalyst exhibits a higher OER current of 284.4 mA cm⁻² at an overpotential of 500 mV, which shows 2.2–10.0 times enhancement than the counterparts with various Ni : Fe ratios. In addition, the UOR current density of the partially amorphous catalyst at 1.8 V vs. RHE shows 1.6 and 2.4 times increment relative to fully amorphous and highly crystalline catalysts, and 2.7–9.4 fold larger than the catalysts with other Ni : Fe ratios. The optimization strategy of designing the partially amorphous bifunctional catalyst in this work may broaden the way of searching for advanced electrocatalysts for simultaneous waste water treatment and clean energy production. Bifunctional electrocatalysts that can boost energy-related reactions are urgently in demand for pursual of dual and even multiple targets towards practical applications such as energy conversion, clean fuel production and pollution treatment. Herein, we highlight that an in situ grown nickel–iron layered double hydroxide (NiFe LDH) nanosheet array catalyst with partially amorphous characteristics, rich native Ni 3+ ions and an optimal Ni : Fe ratio can exhibit robust performances on both the oxygen evolution reaction (OER) and the urea oxidation reaction (UOR). Benefitting from the partially amorphous feature, the catalytically active high-valence species are easy to generate and stabilize, thus further realizing enhanced electrooxidation activity with the aid of an internal 2D charge transfer pathway and native Ni 3+ ions. As expected, the partially amorphous catalyst exhibits a higher OER current of 284.4 mA cm −2 at an overpotential of 500 mV, which shows 2.2–10.0 times enhancement than the counterparts with various Ni : Fe ratios. In addition, the UOR current density of the partially amorphous catalyst at 1.8 V vs. RHE shows 1.6 and 2.4 times increment relative to fully amorphous and highly crystalline catalysts, and 2.7–9.4 fold larger than the catalysts with other Ni : Fe ratios. The optimization strategy of designing the partially amorphous bifunctional catalyst in this work may broaden the way of searching for advanced electrocatalysts for simultaneous waste water treatment and clean energy production. |
| Author | Liu, Weiwei Xie, Junfeng Tang, Bo Lei, Fengcai Peng, Xu Gao, Li Qu, Haichao Hao, Pin Cui, Guanwei |
| Author_xml | – sequence: 1 givenname: Junfeng orcidid: 0000-0002-5775-3084 surname: Xie fullname: Xie, Junfeng organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science – sequence: 2 givenname: Haichao surname: Qu fullname: Qu, Haichao organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science – sequence: 3 givenname: Fengcai surname: Lei fullname: Lei, Fengcai organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science – sequence: 4 givenname: Xu orcidid: 0000-0001-9502-6382 surname: Peng fullname: Peng, Xu organization: Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials, Ministry-of-Education Key Laboratory for the Synthesis and Application of Organic Functional Molecules, College of Chemistry and Chemical Engineering, Hubei University, Wuhan – sequence: 5 givenname: Weiwei surname: Liu fullname: Liu, Weiwei organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science – sequence: 6 givenname: Li surname: Gao fullname: Gao, Li organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science – sequence: 7 givenname: Pin surname: Hao fullname: Hao, Pin organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science – sequence: 8 givenname: Guanwei surname: Cui fullname: Cui, Guanwei organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science – sequence: 9 givenname: Bo orcidid: 0000-0002-8712-7025 surname: Tang fullname: Tang, Bo organization: College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Molecular and Nano Probes (Ministry of Education), Collaborative Innovation Center of Functionalized Probes for Chemical Imaging in Universities of Shandong, Institute of Molecular and Nano Science |
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| Snippet | Bifunctional electrocatalysts that can boost energy-related reactions are urgently in demand for pursual of dual and even multiple targets towards practical... |
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| SubjectTerms | Catalysis Catalysts Charge transfer Clean energy Electrocatalysts Energy conversion Fuel production Hydroxides Intermetallic compounds Ions Iron Iron compounds Nanosheets Nickel Nickel compounds Oxidation Oxygen evolution reactions oxygen production pollution Urea Wastewater Wastewater treatment Water pollution Water treatment |
| Title | Partially amorphous nickel–iron layered double hydroxide nanosheet arrays for robust bifunctional electrocatalysis |
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