Preconcentration and voltammetric analysis of mercury(II) at a carbon paste electrode modified with natural smectite-type clays grafted with organic chelating groups

This study is devoted to the evaluation of a carbon paste electrode modified by a natural 2:1 phyllosilicate clay functionalized with either amine or thiol groups as a sensor for mercury(II). Functionalization was achieved by grafting the pristine clay via its reaction with 3-aminopropyltriethoxysil...

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Published inSensors and actuators. B, Chemical Vol. 110; no. 2; pp. 195 - 203
Main Authors Tonle, Ignas K., Ngameni, Emmanuel, Walcarius, Alain
Format Journal Article
LanguageEnglish
Published Elsevier B.V 14.10.2005
Elsevier
Subjects
Actuators
Analytical chemistry
Carbon
Chemical Sciences
Clay modified electrode
Clays
Concentration (composition)
Electroanalysis
Electrodes
Grafting
Mercury(II)
Organo-clay
Pastes
Preconcentration
Sensors
Voltammetry
Clay modified electrode
Preconcentration
Voltammetry
Organo-clay
Electroanalysis
Mercury(II)
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Abstract This study is devoted to the evaluation of a carbon paste electrode modified by a natural 2:1 phyllosilicate clay functionalized with either amine or thiol groups as a sensor for mercury(II). Functionalization was achieved by grafting the pristine clay via its reaction with 3-aminopropyltriethoxysilane (APTES) or 3-mercaptopropyltrimethoxysilane (MPTMS), respectively. The electroanalytical procedure comprises two steps: the chemical accumulation of the analyte under open-circuit conditions followed by the electrochemical detection of the preconcentrated species using differential pulse anodic stripping voltammetry. The different parameters that govern the two steps (accumulation time, concentration of the analyte, composition of the detection medium, potential and duration of electrolysis) were studied in detail. After optimization, a linear response was obtained in the concentration range from 0.1 to 0.7 μM Hg(II). In these conditions, the detection limits of the method were found to be 8.7 × 10 −8 and 6.8 × 10 −8 M, respectively, for the amine- and thiol-functionalized clays, on the basis of a signal-to-noise ratio of 3. The effect of potential interference on the determination of Hg(II) by the carbon paste electrode modified with the thiol-functionalized clay was also studied and the applicability of the method to real sample analysis was evaluated.
AbstractList This study is devoted to the evaluation of a carbon paste electrode modified by a natural 2:1 phyllosilicate clay functionalized with either amine or thiol groups as a sensor for mercury(II). Functionalization was achieved by grafting the pristine clay via its reaction with 3-aminopropyltriethoxysilane (APTES) or 3-mercaptopropyltrimethoxysilane (MPTMS), respectively. The electroanalytical procedure comprises two steps: the chemical accumulation of the analyte under open-circuit conditions followed by the electrochemical detection of the preconcentrated species using differential pulse anodic stripping voltammetry. The different parameters that govern the two steps (accumulation time, concentration of the analyte, composition of the detection medium, potential and duration of electrolysis) were studied in detail. After optimization, a linear response was obtained in the concentration range from 0DDT1 to 0DDT7D*mM Hg(II). In these conditions, the detection limits of the method were found to be 8DDT7x10-8and 6DDT8x10-8M, respectively, for the amine- and thiol-functionalized clays, on the basis of a signal-to-noise ratio of 3. The effect of potential interference on the determination of Hg(II) by the carbon paste electrode modified with the thiol-functionalized clay was also studied and the applicability of the method to real sample analysis was evaluated.
This study is devoted to the evaluation of a carbon paste electrode modified by a natural 2:1 phyllosilicate clay functionalized with either amine or thiol groups as a sensor for mercury(II). Functionalization was achieved by grafting the pristine clay via its reaction with 3-aminopropyltriethoxysilane (APTES) or 3-mercaptopropyltrimethoxysilane (MPTMS), respectively. The electroanalytical procedure comprises two steps: the chemical accumulation of the analyte under open-circuit conditions followed by the electrochemical detection of the preconcentrated species using differential pulse anodic stripping voltammetry. The different parameters that govern the two steps (accumulation time, concentration of the analyte, composition of the detection medium, potential and duration of electrolysis) were studied in detail. After optimization, a linear response was obtained in the concentration range from 0.1 to 0.7 kM Hg(II). In these conditions, the detection limits of the method were found to be 8.7 x 10 super(-8) and 6.8 x 10 super(-8) M, respectively, for the amine- and thiol- functionalized clays, on the basis of a signal-to-noise ratio of 3. The effect of potential interference on the determination of Hg(II) by the carbon paste electrode modified with the thiol-functionalized clay was also studied and the applicability of the method to real sample analysis was evaluated.
This study is devoted to the evaluation of a carbon paste electrode modified by a natural 2:1 phyllosilicate clay functionalized with either amine or thiol groups as a sensor for mercury(II). Functionalization was achieved by grafting the pristine clay via its reaction with 3-aminopropyltriethoxysilane (APTES) or 3-mercaptopropyltrimethoxysilane (MPTMS), respectively. The electroanalytical procedure comprises two steps: the chemical accumulation of the analyte under open-circuit conditions followed by the electrochemical detection of the preconcentrated species using differential pulse anodic stripping voltammetry. The different parameters that govern the two steps (accumulation time, concentration of the analyte, composition of the detection medium, potential and duration of electrolysis) were studied in detail. After optimization, a linear response was obtained in the concentration range from 0.1 to 0.7 μM Hg(II). In these conditions, the detection limits of the method were found to be 8.7 × 10−8 and 6.8 × 10−8 M, respectively, for the amine- and thiol-functionalized clays, on the basis of a signal-to-noise ratio of 3. The effect of potential interference on the determination of Hg(II) by the carbon paste electrode modified with the thiol-functionalized clay was also studied and the applicability of the method to real sample analysis was evaluated
This study is devoted to the evaluation of a carbon paste electrode modified by a natural 2:1 phyllosilicate clay functionalized with either amine or thiol groups as a sensor for mercury(II). Functionalization was achieved by grafting the pristine clay via its reaction with 3-aminopropyltriethoxysilane (APTES) or 3-mercaptopropyltrimethoxysilane (MPTMS), respectively. The electroanalytical procedure comprises two steps: the chemical accumulation of the analyte under open-circuit conditions followed by the electrochemical detection of the preconcentrated species using differential pulse anodic stripping voltammetry. The different parameters that govern the two steps (accumulation time, concentration of the analyte, composition of the detection medium, potential and duration of electrolysis) were studied in detail. After optimization, a linear response was obtained in the concentration range from 0.1 to 0.7 μM Hg(II). In these conditions, the detection limits of the method were found to be 8.7 × 10 −8 and 6.8 × 10 −8 M, respectively, for the amine- and thiol-functionalized clays, on the basis of a signal-to-noise ratio of 3. The effect of potential interference on the determination of Hg(II) by the carbon paste electrode modified with the thiol-functionalized clay was also studied and the applicability of the method to real sample analysis was evaluated.
Author Walcarius, Alain
Ngameni, Emmanuel
Tonle, Ignas K.
Author_xml – sequence: 1
  givenname: Ignas K.
  surname: Tonle
  fullname: Tonle, Ignas K.
  email: itonle@yahoo.com
  organization: Laboratoire de Chimie Analytique, Faculté des sciences, Université de Yaoundé I, B. P. 812, Yaoundé, Cameroun
– sequence: 2
  givenname: Emmanuel
  surname: Ngameni
  fullname: Ngameni, Emmanuel
  email: engameni@uycdc.uninet.cm
  organization: Laboratoire de Chimie Analytique, Faculté des sciences, Université de Yaoundé I, B. P. 812, Yaoundé, Cameroun
– sequence: 3
  givenname: Alain
  surname: Walcarius
  fullname: Walcarius, Alain
  email: walcariu@lcpe.cnrs-nancy.fr
  organization: Laboratoire de Chimie Physique et Microbiologie pour l’Environnement, UMR 7564, CNRS– Université Henri Poincaré Nancy I, 405 Rue de Vandoeuvre, F-54600 Villers-les-Nancy, France
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Issue 2
Keywords Clay modified electrode
Preconcentration
Voltammetry
Organo-clay
Electroanalysis
Mercury(II)
Language English
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Snippet This study is devoted to the evaluation of a carbon paste electrode modified by a natural 2:1 phyllosilicate clay functionalized with either amine or thiol...
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SubjectTerms Actuators
Analytical chemistry
Carbon
Chemical Sciences
Clay modified electrode
Clays
Concentration (composition)
Electroanalysis
Electrodes
Grafting
Mercury(II)
Organo-clay
Pastes
Preconcentration
Sensors
Voltammetry
Title Preconcentration and voltammetric analysis of mercury(II) at a carbon paste electrode modified with natural smectite-type clays grafted with organic chelating groups
URI https://dx.doi.org/10.1016/j.snb.2005.01.027
https://search.proquest.com/docview/1082175106
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Volume 110
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