Novel use of a hand-held laser induced breakdown spectroscopy instrument to monitor hydride corrosion in uranium
Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstruct...
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Published in | Spectrochimica acta. Part B: Atomic spectroscopy Vol. 159; no. C; p. 105651 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
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Oxford
Elsevier B.V
01.09.2019
Elsevier BV Elsevier |
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Abstract | Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were studied by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy.
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•Compact hand-held LIBS instrument (eye safe system) for UH3 corrosion studies from surface into bulk of sample•Samples in pre-corrosion states prepared by hydrogen charging with controlled hydrogen concentration•Quantitative evaluation of uranium surface damage from laser ablation•Consistent variation in atomic emission signal for hydrogen with sample's state•Systematic increase in oxygen peak intensity (concentration) associated with oxidation of uranium and UH3 |
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AbstractList | Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were studied by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy.
[Display omitted]
•Compact hand-held LIBS instrument (eye safe system) for UH3 corrosion studies from surface into bulk of sample•Samples in pre-corrosion states prepared by hydrogen charging with controlled hydrogen concentration•Quantitative evaluation of uranium surface damage from laser ablation•Consistent variation in atomic emission signal for hydrogen with sample's state•Systematic increase in oxygen peak intensity (concentration) associated with oxidation of uranium and UH3 Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were studied by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy. With a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were performed on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were investigated by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy. |
ArticleNumber | 105651 |
Author | Leckey, J.H. Bennett, B.N. Powell, G.L. Garlea, E. Martin, M.Z. Bridges, R.L. |
Author_xml | – sequence: 1 givenname: E. surname: Garlea fullname: Garlea, E. email: garleae@y12.doe.gov organization: CNS/Y-12 National Security Complex, Development Division, Oak Ridge, TN 37831, USA – sequence: 2 givenname: B.N. surname: Bennett fullname: Bennett, B.N. organization: CNS/Y-12 National Security Complex, Development Division, Oak Ridge, TN 37831, USA – sequence: 3 givenname: M.Z. surname: Martin fullname: Martin, M.Z. organization: Oak Ridge National Laboratory, Biosciences Division, Oak Ridge, TN 37831, USA – sequence: 4 givenname: R.L. surname: Bridges fullname: Bridges, R.L. organization: CNS/Y-12 National Security Complex, Development Division, Oak Ridge, TN 37831, USA – sequence: 5 givenname: G.L. surname: Powell fullname: Powell, G.L. organization: CNS/Y-12 National Security Complex, Development Division, Oak Ridge, TN 37831, USA – sequence: 6 givenname: J.H. surname: Leckey fullname: Leckey, J.H. organization: CNS/Y-12 National Security Complex, Development Division, Oak Ridge, TN 37831, USA |
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CitedBy_id | crossref_primary_10_1016_j_sab_2020_105796 crossref_primary_10_1364_AO_482533 crossref_primary_10_1039_D0JA00416B crossref_primary_10_1007_s10967_021_07819_4 crossref_primary_10_1016_j_sab_2023_106650 crossref_primary_10_1039_D0JA90067B crossref_primary_10_1016_j_mtla_2023_101737 crossref_primary_10_1016_j_sab_2021_106283 crossref_primary_10_1155_2023_2502152 crossref_primary_10_1007_s40194_023_01677_2 |
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Keywords | Hand-held LIBS Uranium Surface damage, hydrogen embrittlement Hydride corrosion Laser-induced breakdown spectroscopy |
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Snippet | Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled... With a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were performed on specimens of uranium charged with controlled... |
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SubjectTerms | Ablation Analytical methods Bulk sampling Carbon Control equipment Corrosion Damage assessment Depleted uranium Glove boxes Hand-held LIBS High temperature High temperature effects Hydride corrosion Hydrides Hydrogen hydrogen embrittlement Hydrogen storage Laser ablation Laser damage Laser induced breakdown spectroscopy Lasers Light microscopy MATERIALS SCIENCE Microscopy NUCLEAR PHYSICS AND RADIATION PHYSICS Optical microscopy Oxidation Oxidation process Oxygen Oxygen content Radioisotopes Spectroscopy Spectrum analysis Surface damage Surface damage, hydrogen embrittlement Temperature effects Uranium |
Title | Novel use of a hand-held laser induced breakdown spectroscopy instrument to monitor hydride corrosion in uranium |
URI | https://dx.doi.org/10.1016/j.sab.2019.105651 https://www.proquest.com/docview/2303820707 https://www.osti.gov/servlets/purl/1546542 |
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