Novel use of a hand-held laser induced breakdown spectroscopy instrument to monitor hydride corrosion in uranium

Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstruct...

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Published inSpectrochimica acta. Part B: Atomic spectroscopy Vol. 159; no. C; p. 105651
Main Authors Garlea, E., Bennett, B.N., Martin, M.Z., Bridges, R.L., Powell, G.L., Leckey, J.H.
Format Journal Article
LanguageEnglish
Published Oxford Elsevier B.V 01.09.2019
Elsevier BV
Elsevier
Subjects
Ablation
Analytical methods
Bulk sampling
Carbon
Control equipment
Corrosion
Damage assessment
Depleted uranium
Glove boxes
Hand-held LIBS
High temperature
High temperature effects
Hydride corrosion
Hydrides
Hydrogen
hydrogen embrittlement
Hydrogen storage
Laser ablation
Laser damage
Laser induced breakdown spectroscopy
Lasers
Light microscopy
MATERIALS SCIENCE
Microscopy
NUCLEAR PHYSICS AND RADIATION PHYSICS
Optical microscopy
Oxidation
Oxidation process
Oxygen
Oxygen content
Radioisotopes
Spectroscopy
Spectrum analysis
Surface damage
Surface damage, hydrogen embrittlement
Temperature effects
Uranium
Hand-held LIBS
Uranium
Surface damage, hydrogen embrittlement
Hydride corrosion
Laser-induced breakdown spectroscopy
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Abstract Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were studied by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy. [Display omitted] •Compact hand-held LIBS instrument (eye safe system) for UH3 corrosion studies from surface into bulk of sample•Samples in pre-corrosion states prepared by hydrogen charging with controlled hydrogen concentration•Quantitative evaluation of uranium surface damage from laser ablation•Consistent variation in atomic emission signal for hydrogen with sample's state•Systematic increase in oxygen peak intensity (concentration) associated with oxidation of uranium and UH3
AbstractList Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were studied by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy. [Display omitted] •Compact hand-held LIBS instrument (eye safe system) for UH3 corrosion studies from surface into bulk of sample•Samples in pre-corrosion states prepared by hydrogen charging with controlled hydrogen concentration•Quantitative evaluation of uranium surface damage from laser ablation•Consistent variation in atomic emission signal for hydrogen with sample's state•Systematic increase in oxygen peak intensity (concentration) associated with oxidation of uranium and UH3
Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were studied by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy.
With a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were performed on specimens of uranium charged with controlled hydrogen concentrations for a qualitative evaluation of hydride corrosion. Four samples of depleted uranium with two different starting microstructures (cast and rolled) were used for this study. The hydrogen charged samples (rolled 1.8 wppm H and cast 14 wppm H by weight) are representative of the pre-corrosion states with hydrides distributed throughout the bulk. In-depth LIBS measurements were carried out, after the thick surface corrosion layer was removed, by applying 100 laser pulses from sample surface into the bulk on five different sample locations. Three additional areas on each sample were investigated by laser ablation using a 12-point grid approach. The atomic emission signals of elemental uranium, carbon, hydrogen, and oxygen were identified and analyzed. All four samples showed similar uranium and carbon concentrations, as expected. Hydrogen content was consistent with each sample's specification, such that the hydrogen charged samples exhibited higher hydrogen concentration than their references. Both specimens charged with hydrogen showed elevated oxygen content as well, due to rapid oxidation of uranium and uranium hydrides. The oxidation process was facilitated by the laser ablation and plasma plume's high temperature effects on the sample combined with the glovebox environment. The uranium surface damage produced by laser ablation was quantitatively evaluated by optical microscopy.
ArticleNumber 105651
Author Leckey, J.H.
Bennett, B.N.
Powell, G.L.
Garlea, E.
Martin, M.Z.
Bridges, R.L.
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Issue C
Keywords Hand-held LIBS
Uranium
Surface damage, hydrogen embrittlement
Hydride corrosion
Laser-induced breakdown spectroscopy
Language English
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SSID ssj0002525
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Snippet Using a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were conducted on specimens of uranium charged with controlled...
With a compact hand-held laser-induced breakdown spectroscopy (LIBS) instrument, studies were performed on specimens of uranium charged with controlled...
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StartPage 105651
SubjectTerms Ablation
Analytical methods
Bulk sampling
Carbon
Control equipment
Corrosion
Damage assessment
Depleted uranium
Glove boxes
Hand-held LIBS
High temperature
High temperature effects
Hydride corrosion
Hydrides
Hydrogen
hydrogen embrittlement
Hydrogen storage
Laser ablation
Laser damage
Laser induced breakdown spectroscopy
Lasers
Light microscopy
MATERIALS SCIENCE
Microscopy
NUCLEAR PHYSICS AND RADIATION PHYSICS
Optical microscopy
Oxidation
Oxidation process
Oxygen
Oxygen content
Radioisotopes
Spectroscopy
Spectrum analysis
Surface damage
Surface damage, hydrogen embrittlement
Temperature effects
Uranium
Title Novel use of a hand-held laser induced breakdown spectroscopy instrument to monitor hydride corrosion in uranium
URI https://dx.doi.org/10.1016/j.sab.2019.105651
https://www.proquest.com/docview/2303820707
https://www.osti.gov/servlets/purl/1546542
Volume 159
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