Electrical, morphological and rheological properties of carbon nanotube composites with polyethylene and poly(phenylene sulfide) by melt mixing
Electrical, morphological and rheological properties of polyethylene (PE)/multi-walled carbon nanotube (MWCNT) and poly(phenylene sulfide) (PPS)/MWCNT composites were studied with the MWCNT content using vector network analyzer, scanning electron microscopy and rotational rheometry. From the results...
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| Published in | Chemical engineering science Vol. 64; no. 22; pp. 4649 - 4656 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
16.11.2009
Elsevier |
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| Abstract | Electrical, morphological and rheological properties of polyethylene (PE)/multi-walled carbon nanotube (MWCNT) and poly(phenylene sulfide) (PPS)/MWCNT composites were studied with the MWCNT content using vector network analyzer, scanning electron microscopy and rotational rheometry. From the results of electrical conductivity and electromagnetic interference shielding efficiency (EMI SE) of the PE/MWCNT and PPS/MWCNT composites, the electrical percolation threshold of the composites has found to be 5 and 3
wt% MWCNT, respectively. From the results of the EMI SE of the composites, it was suggested that the increase in homogeneous dispersion of the MWCNT in the PPS matrix has been attributed to the increase in connectivity of the MWCNT–MWCNT network structure of the composite. Therefore, the higher values of the EMI SE with the MWCNT content were observed in the PPS/MWCNT than the PE/MWCNT composites. From the results of the rheological properties of the PE/MWCNT and PPS/MWCNT composites, the increase in the complex viscosity was observed for the PPS/MWCNT than the PE/MWCNT composites. The increase in complex viscosity maybe due to the increase in homogeneous dispersion of the MWCNT in the PPS matrix than that in the PE matrix. From the results of the rheological properties of the PE/MWCNT and PPS/MWCNT composites, it was suggested that the homogeneous dispersion of the MWCNT in the polymer matrix has affected the increase in complex viscosity of the PPS/MWCNT composite. This result of rheological behavior is consistent with the results of the EMI SE of the PE/MWCNT and PPS/MWCNT composites. |
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| AbstractList | Electrical, morphological and rheological properties of polyethylene (PE)/multi-walled carbon nanotube (MWCNT) and poly(phenylene sulfide) (PPS)/MWCNT composites were studied with the MWCNT content using vector network analyzer, scanning electron microscopy and rotational rheometry. From the results of electrical conductivity and electromagnetic interference shielding efficiency (EMI SE) of the PE/MWCNT and PPS/MWCNT composites, the electrical percolation threshold of the composites has found to be 5 and 3
wt% MWCNT, respectively. From the results of the EMI SE of the composites, it was suggested that the increase in homogeneous dispersion of the MWCNT in the PPS matrix has been attributed to the increase in connectivity of the MWCNT–MWCNT network structure of the composite. Therefore, the higher values of the EMI SE with the MWCNT content were observed in the PPS/MWCNT than the PE/MWCNT composites. From the results of the rheological properties of the PE/MWCNT and PPS/MWCNT composites, the increase in the complex viscosity was observed for the PPS/MWCNT than the PE/MWCNT composites. The increase in complex viscosity maybe due to the increase in homogeneous dispersion of the MWCNT in the PPS matrix than that in the PE matrix. From the results of the rheological properties of the PE/MWCNT and PPS/MWCNT composites, it was suggested that the homogeneous dispersion of the MWCNT in the polymer matrix has affected the increase in complex viscosity of the PPS/MWCNT composite. This result of rheological behavior is consistent with the results of the EMI SE of the PE/MWCNT and PPS/MWCNT composites. Electrical, morphological and rheological properties of polyethylene (PE)/multi-walled carbon nanotube (MWCNT) and poly(phenylene sulfide) (PPS)/MWCNT composites were studied with the MWCNT content using vector network analyzer, scanning electron microscopy and rotational rheometry. From the results of electrical conductivity and electromagnetic interference shielding efficiency (EMI SE) of the PE/MWCNT and PPS/MWCNT composites, the electrical percolation threshold of the composites has found to be 5 and 3 wt% MWCNT, respectively. From the results of the EMI SE of the composites, it was suggested that the increase in homogeneous dispersion of the MWCNT in the PPS matrix has been attributed to the increase in connectivity of the MWCNT-MWCNT network structure of the composite. Therefore, the higher values of the EMI SE with the MWCNT content were observed in the PPS/MWCNT than the PE/MWCNT composites. From the results of the rheological properties of the PE/MWCNT and PPS/MWCNT composites, the increase in the complex viscosity was observed for the PPS/MWCNT than the PE/MWCNT composites. The increase in complex viscosity maybe due to the increase in homogeneous dispersion of the MWCNT in the PPS matrix than that in the PE matrix. From the results of the rheological properties of the PE/MWCNT and PPS/MWCNT composites, it was suggested that the homogeneous dispersion of the MWCNT in the polymer matrix has affected the increase in complex viscosity of the PPS/MWCNT composite. This result of rheological behavior is consistent with the results of the EMI SE of the PE/MWCNT and PPS/MWCNT composites. |
| Author | Han, Mi Sun Lee, Yun Kyun Lee, Heon Sang Yun, Chang Hun Kim, Woo Nyon |
| Author_xml | – sequence: 1 givenname: Mi Sun surname: Han fullname: Han, Mi Sun organization: Department of Chemical and Biological Engineering, Korea University, Anam-dong, Seoul 136-701, Republic of Korea – sequence: 2 givenname: Yun Kyun surname: Lee fullname: Lee, Yun Kyun organization: Department of Chemical and Biological Engineering, Korea University, Anam-dong, Seoul 136-701, Republic of Korea – sequence: 3 givenname: Heon Sang surname: Lee fullname: Lee, Heon Sang organization: Department of Chemical Engineering, Dong-A University, 840 Hadan2-dong, Saha-gu, Busan 604-714, Republic of Korea – sequence: 4 givenname: Chang Hun surname: Yun fullname: Yun, Chang Hun organization: Tech. Center, LG Chemical Ltd., 84 Jang–dong, Yusung–ku, Daejeon 305-343, Republic of Korea – sequence: 5 givenname: Woo Nyon surname: Kim fullname: Kim, Woo Nyon email: kimwn@korea.ac.kr organization: Department of Chemical and Biological Engineering, Korea University, Anam-dong, Seoul 136-701, Republic of Korea |
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| Keywords | Extrusion Composites Polymers Rheology Dispersion Viscosity Scanning electron microscopy Mixing Electrical conductivity Composite material Rheological properties |
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