Novel flexible chemical gas sensor based on poly(3,4-ethylenedioxythiophene) nanotube membrane

Poly(3,4-ethylenedioxythiophene) nanotubes (PEDOT NTs) flexible membrane was successfully fabricated by vapor deposition polymerization (VDP) mediated electrospinning for ammonia gas detection. PVA nanofibers (NFs) were electrospun as a core part and polyvinyl alcohol (PVA)/PEDOT coaxial nanocables...

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Published inTalanta (Oxford) Vol. 82; no. 4; pp. 1338 - 1343
Main Authors Kwon, Oh Seok, Park, Eunyu, Kweon, O. Young, Park, Seon Joo, Jang, Jyongsik
Format Journal Article
LanguageEnglish
Published Amsterdam Elsevier B.V 15.09.2010
Elsevier
Subjects
Adsorption
Ammonia gas
Analytical chemistry
Bridged Bicyclo Compounds, Heterocyclic - chemistry
Chemistry
Conducting polymer
Electrospun
Exact sciences and technology
Flexible sensor
Gases - analysis
General, instrumentation
Membrane
Membranes, Artificial
Microscopy, Electron, Scanning
Microscopy, Electron, Transmission
Nanotubes
PEDOT nanotubes
Polymers - chemistry
Flexible sensor
Membrane
Electrospun
PEDOT nanotubes
Conducting polymer
Ammonia gas
Trace analysis
Water
Performance evaluation
Polymerization
Alcohol
Polymer
Method
Chemical sensor
Chemical enrichment
Thickness
Transducer
Ammonia
Sensitivity
Adsorption
Response time
Detection
Deposition
Gas detector
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Abstract Poly(3,4-ethylenedioxythiophene) nanotubes (PEDOT NTs) flexible membrane was successfully fabricated by vapor deposition polymerization (VDP) mediated electrospinning for ammonia gas detection. PVA nanofibers (NFs) were electrospun as a core part and polyvinyl alcohol (PVA)/PEDOT coaxial nanocables (NCs) were prepared by VDP method via EDOT monomer adsorption onto the electrospun PVA NFs as templates. To obtain the PEDOT NTs membrane, the PVA NFs were removed from PVA/PEDOT coaxial NCs with distilled water. PVA/PEDOT coaxial NCs and PEDOT NTs had the conductivities of 71 and 61 S cm −1 and were applied as a transducer for ammonia gas detection in the range of 1–100 parts per million (ppm) of NH 3 gas. They exhibited the minimum detectable level of ca. 5 parts per million (ppm) and fast response time (less than 1 s) towards ammonia gas. In a recovery time, the PEDOT NTs membrane sensor was ca. 30 s and shorter compared to that of the membrane sensor based on the PVA/PEDOT NCs ( ca. 50 s). In addition, sensor performance of PEDOT NTs membrane was also undertaken as a function of membrane thickness. Thick membrane sensor (30 μm) had the enhanced sensitivity and the sensitivity on the membrane thickness was in the order of 30 μm > 20 μm > 10 μm at 60 ppm of NH 3 gas.
AbstractList Poly(3,4-ethylenedioxythiophene) nanotubes (PEDOT NTs) flexible membrane was successfully fabricated by vapor deposition polymerization (VDP) mediated electrospinning for ammonia gas detection. PVA nanofibers (NFs) were electrospun as a core part and polyvinyl alcohol (PVA)/PEDOT coaxial nanocables (NCs) were prepared by VDP method via EDOT monomer adsorption onto the electrospun PVA NFs as templates. To obtain the PEDOT NTs membrane, the PVA NFs were removed from PVA/PEDOT coaxial NCs with distilled water. PVA/PEDOT coaxial NCs and PEDOT NTs had the conductivities of 71 and 61 Scm(-1) and were applied as a transducer for ammonia gas detection in the range of 1-100 parts per million (ppm) of NH(3) gas. They exhibited the minimum detectable level of ca. 5 parts per million (ppm) and fast response time (less than 1s) towards ammonia gas. In a recovery time, the PEDOT NTs membrane sensor was ca. 30s and shorter compared to that of the membrane sensor based on the PVA/PEDOT NCs (ca. 50s). In addition, sensor performance of PEDOT NTs membrane was also undertaken as a function of membrane thickness. Thick membrane sensor (30 microm) had the enhanced sensitivity and the sensitivity on the membrane thickness was in the order of 30 microm>20 microm>10 microm at 60 ppm of NH(3) gas.
Poly(3,4-ethylenedioxythiophene) nanotubes (PEDOT NTs) flexible membrane was successfully fabricated by vapor deposition polymerization (VDP) mediated electrospinning for ammonia gas detection. PVA nanofibers (NFs) were electrospun as a core part and polyvinyl alcohol (PVA)/PEDOT coaxial nanocables (NCs) were prepared by VDP method via EDOT monomer adsorption onto the electrospun PVA NFs as templates. To obtain the PEDOT NTs membrane, the PVA NFs were removed from PVA/PEDOT coaxial NCs with distilled water. PVA/PEDOT coaxial NCs and PEDOT NTs had the conductivities of 71 and 61 Scm(-1) and were applied as a transducer for ammonia gas detection in the range of 1-100 parts per million (ppm) of NH(3) gas. They exhibited the minimum detectable level of ca. 5 parts per million (ppm) and fast response time (less than 1s) towards ammonia gas. In a recovery time, the PEDOT NTs membrane sensor was ca. 30s and shorter compared to that of the membrane sensor based on the PVA/PEDOT NCs (ca. 50s). In addition, sensor performance of PEDOT NTs membrane was also undertaken as a function of membrane thickness. Thick membrane sensor (30 microm) had the enhanced sensitivity and the sensitivity on the membrane thickness was in the order of 30 microm>20 microm>10 microm at 60 ppm of NH(3) gas.
Poly(3,4-ethylenedioxythiophene) nanotubes (PEDOT NTs) flexible membrane was successfully fabricated by vapor deposition polymerization (VDP) mediated electrospinning for ammonia gas detection. PVA nanofibers (NFs) were electrospun as a core part and polyvinyl alcohol (PVA)/PEDOT coaxial nanocables (NCs) were prepared by VDP method via EDOT monomer adsorption onto the electrospun PVA NFs as templates. To obtain the PEDOT NTs membrane, the PVA NFs were removed from PVA/PEDOT coaxial NCs with distilled water. PVA/PEDOT coaxial NCs and PEDOT NTs had the conductivities of 71 and 61 S cm −1 and were applied as a transducer for ammonia gas detection in the range of 1–100 parts per million (ppm) of NH 3 gas. They exhibited the minimum detectable level of ca. 5 parts per million (ppm) and fast response time (less than 1 s) towards ammonia gas. In a recovery time, the PEDOT NTs membrane sensor was ca. 30 s and shorter compared to that of the membrane sensor based on the PVA/PEDOT NCs ( ca. 50 s). In addition, sensor performance of PEDOT NTs membrane was also undertaken as a function of membrane thickness. Thick membrane sensor (30 μm) had the enhanced sensitivity and the sensitivity on the membrane thickness was in the order of 30 μm > 20 μm > 10 μm at 60 ppm of NH 3 gas.
Author Kwon, Oh Seok
Jang, Jyongsik
Park, Seon Joo
Park, Eunyu
Kweon, O. Young
Author_xml – sequence: 1
  givenname: Oh Seok
  surname: Kwon
  fullname: Kwon, Oh Seok
– sequence: 2
  givenname: Eunyu
  surname: Park
  fullname: Park, Eunyu
– sequence: 3
  givenname: O. Young
  surname: Kweon
  fullname: Kweon, O. Young
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  givenname: Seon Joo
  surname: Park
  fullname: Park, Seon Joo
– sequence: 5
  givenname: Jyongsik
  surname: Jang
  fullname: Jang, Jyongsik
  email: jsjang@plaza.snu.ac.kr
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https://www.ncbi.nlm.nih.gov/pubmed/20801338$$D View this record in MEDLINE/PubMed
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Issue 4
Keywords Flexible sensor
Membrane
Electrospun
PEDOT nanotubes
Conducting polymer
Ammonia gas
Trace analysis
Water
Performance evaluation
Polymerization
Alcohol
Polymer
Method
Chemical sensor
Chemical enrichment
Thickness
Transducer
Ammonia
Sensitivity
Adsorption
Response time
Detection
Deposition
Gas detector
Language English
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Snippet Poly(3,4-ethylenedioxythiophene) nanotubes (PEDOT NTs) flexible membrane was successfully fabricated by vapor deposition polymerization (VDP) mediated...
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SubjectTerms Adsorption
Ammonia gas
Analytical chemistry
Bridged Bicyclo Compounds, Heterocyclic - chemistry
Chemistry
Conducting polymer
Electrospun
Exact sciences and technology
Flexible sensor
Gases - analysis
General, instrumentation
Membrane
Membranes, Artificial
Microscopy, Electron, Scanning
Microscopy, Electron, Transmission
Nanotubes
PEDOT nanotubes
Polymers - chemistry
Title Novel flexible chemical gas sensor based on poly(3,4-ethylenedioxythiophene) nanotube membrane
URI https://dx.doi.org/10.1016/j.talanta.2010.06.058
https://www.ncbi.nlm.nih.gov/pubmed/20801338
https://search.proquest.com/docview/754013832
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