Synthesis and characterization of cellulose/silica hybrid materials with chemical crosslinking
The cellulose/silica hybrid biomaterials are prepared by sol–gel covalent crosslinking process. The tetraethoxysilane (TEOS) as precursor, γ-aminopropyltriethoxylsilane (APTES) as couple agent, and 2,4,6-tri[(2-epihydrin-3-bimethyl-ammonium)propyl]-1,3,5-triazine chloride (Tri-EBAC) as crosslinking...
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| Published in | Carbohydrate polymers Vol. 78; no. 4; pp. 799 - 805 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
17.11.2009
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The cellulose/silica hybrid biomaterials are prepared by sol–gel covalent crosslinking process. The tetraethoxysilane (TEOS) as precursor, γ-aminopropyltriethoxylsilane (APTES) as couple agent, and 2,4,6-tri[(2-epihydrin-3-bimethyl-ammonium)propyl]-1,3,5-triazine chloride (Tri-EBAC) as crosslinking agent, are used in the sol–gel crosslinking process. The chemical and morphological structures of cellulose/silica covalent crosslinking hybrids are investigated with micro-FT-IR spectra, nitrogen element analysis, X-ray diffraction, SEM, AFM, and DSC. The results show that the cellulose/silica hybrids form new macromolecular structures. In sol–gel process, inorganic particles are dispersed at the nanometer scale in the cellulose host matrix, bounding to the cellulose through covalent bonds. The cellulose/silica covalent crosslinking hybrid can form good and smooth film on the cellulose. The thermal properties of organic/inorganic hybrids are improved. |
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| AbstractList | The cellulose/silica hybrid biomaterials are prepared by sol–gel covalent crosslinking process. The tetraethoxysilane (TEOS) as precursor, γ-aminopropyltriethoxylsilane (APTES) as couple agent, and 2,4,6-tri[(2-epihydrin-3-bimethyl-ammonium)propyl]-1,3,5-triazine chloride (Tri-EBAC) as crosslinking agent, are used in the sol–gel crosslinking process. The chemical and morphological structures of cellulose/silica covalent crosslinking hybrids are investigated with micro-FT-IR spectra, nitrogen element analysis, X-ray diffraction, SEM, AFM, and DSC. The results show that the cellulose/silica hybrids form new macromolecular structures. In sol–gel process, inorganic particles are dispersed at the nanometer scale in the cellulose host matrix, bounding to the cellulose through covalent bonds. The cellulose/silica covalent crosslinking hybrid can form good and smooth film on the cellulose. The thermal properties of organic/inorganic hybrids are improved. |
| Author | Xie, Kongliang Yu, Yanhong Shi, Yaqi |
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| Keywords | Hybrid Crosslinking Nanocellulose Organic/inorganic Sol–gel process Thermal transition Hybrid material Cellulose Organic silane Surface topography Triazine derivative polymer Experimental study Silica Coupling agent Quaternary ammonium compound Sol gel process Morphology Preparation Cellulose derivatives Triazine derivatives Crosslinked polymer Sol-gel process Silicon polymer Quaternary ammonium polymer |
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| SubjectTerms | Applied sciences biocompatible materials cellulose Composites Crosslinking Exact sciences and technology Forms of application and semi-finished materials Fourier transform infrared spectroscopy gelation Hybrid Nanocellulose nitrogen Organic/inorganic Polymer industry, paints, wood silica Sol–gel process synthesis Technology of polymers thermal properties X-ray diffraction |
| Title | Synthesis and characterization of cellulose/silica hybrid materials with chemical crosslinking |
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