Solution combustion synthesis and magnetic property of rock-salt (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O high-entropy oxide nanocrystalline powder
•The (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O nanocrystalline powder was synthesizes by SCS method.•Synthesis temperature of single-phase rock-salt structure was above 1123 K.•The material exhibits long-range antiferromagnetic behavior below TN.•The material shows lower TN. A facile solution combustion synthesi...
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| Published in | Journal of magnetism and magnetic materials Vol. 484; pp. 245 - 252 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
15.08.2019
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | •The (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O nanocrystalline powder was synthesizes by SCS method.•Synthesis temperature of single-phase rock-salt structure was above 1123 K.•The material exhibits long-range antiferromagnetic behavior below TN.•The material shows lower TN.
A facile solution combustion synthesis method was successfully applied to synthesize single rock-salt structural (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O high-entropy oxide (HEO) nanocrystalline powder with chemical homogeneity. The XRD patterns with Rietveld refinement reveal the formation of single-phase rock-salt structure occurs only at the synthesis temperatures ≥ 1123 K, and the average nanocrystalline size is about 43 nm. Moreover, two series of experiments confirm the effect of configurational entropy on phase stabilization. Furthermore, the as-synthesized single-phase (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O nanocrystalline powder exhibits long-range antiferromagnetic behavior below Néel temperature (TN = 106 K), which can be well understood by the super-exchange interactions in the rock-salt HEO. The powder also shows lower TN due to the significant amount of nonmagnetic ions suppressing the antiferromagnetic order. |
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| AbstractList | •The (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O nanocrystalline powder was synthesizes by SCS method.•Synthesis temperature of single-phase rock-salt structure was above 1123 K.•The material exhibits long-range antiferromagnetic behavior below TN.•The material shows lower TN.
A facile solution combustion synthesis method was successfully applied to synthesize single rock-salt structural (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O high-entropy oxide (HEO) nanocrystalline powder with chemical homogeneity. The XRD patterns with Rietveld refinement reveal the formation of single-phase rock-salt structure occurs only at the synthesis temperatures ≥ 1123 K, and the average nanocrystalline size is about 43 nm. Moreover, two series of experiments confirm the effect of configurational entropy on phase stabilization. Furthermore, the as-synthesized single-phase (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O nanocrystalline powder exhibits long-range antiferromagnetic behavior below Néel temperature (TN = 106 K), which can be well understood by the super-exchange interactions in the rock-salt HEO. The powder also shows lower TN due to the significant amount of nonmagnetic ions suppressing the antiferromagnetic order. A facile solution combustion synthesis method was successfully applied to synthesize single rock-salt structural (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O high-entropy oxide (HEO) nanocrystalline powder with chemical homogeneity. The XRD patterns with Rietveld refinement reveal the formation of single-phase rock-salt structure occurs only at the synthesis temperatures ≥ 1123 K, and the average nanocrystalline size is about 43 nm. Moreover, two series of experiments confirm the effect of configurational entropy on phase stabilization. Furthermore, the as-synthesized single-phase (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O nanocrystalline powder exhibits long-range antiferromagnetic behavior below Néel temperature (TN = 106 K), which can be well understood by the super-exchange interactions in the rock-salt HEO. The powder also shows lower TN due to the significant amount of nonmagnetic ions suppressing the antiferromagnetic order. |
| Author | Ran, Songlin Zhang, Zhan-Guo Mao, Aiqin Kuramoto, Koji Xiang, Hou-Zheng Yu, Haiyun |
| Author_xml | – sequence: 1 givenname: Aiqin surname: Mao fullname: Mao, Aiqin email: maoaiqinmaq@163.com organization: School of Materials Science and Engineering, Anhui University of Technology, Maxiang Road, Ma’anshan 243002, China – sequence: 2 givenname: Hou-Zheng surname: Xiang fullname: Xiang, Hou-Zheng organization: School of Materials Science and Engineering, Anhui University of Technology, Maxiang Road, Ma’anshan 243002, China – sequence: 3 givenname: Zhan-Guo surname: Zhang fullname: Zhang, Zhan-Guo email: z.zhang@aist.go.jp organization: National Institute of Advanced Industrial Science and Technology (AIST), 16-1 Onogawa, Tsukuba 305-8569, Ibaraki, Japan – sequence: 4 givenname: Koji surname: Kuramoto fullname: Kuramoto, Koji organization: National Institute of Advanced Industrial Science and Technology (AIST), 16-1 Onogawa, Tsukuba 305-8569, Ibaraki, Japan – sequence: 5 givenname: Haiyun surname: Yu fullname: Yu, Haiyun organization: School of Materials Science and Engineering, Anhui University of Technology, Maxiang Road, Ma’anshan 243002, China – sequence: 6 givenname: Songlin surname: Ran fullname: Ran, Songlin organization: Key Laboratory of Metallurgical Emission Reduction & Resources Recycling (Anhui University of Technology) Ministry of Education, No. 59 Hudong Road, Ma’anshan 243002, China |
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| Keywords | Antiferromagnetism (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O Nanocrystalline powder Solution combustion synthesis High-entropy oxide |
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| Snippet | •The (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O nanocrystalline powder was synthesizes by SCS method.•Synthesis temperature of single-phase rock-salt structure was above... A facile solution combustion synthesis method was successfully applied to synthesize single rock-salt structural (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O high-entropy... |
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| SubjectTerms | (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O Antiferromagnetism Combustion synthesis Crystals Entropy High-entropy oxide Magnetic properties Nanocrystalline powder Nanocrystals Organic chemistry Solution combustion synthesis |
| Title | Solution combustion synthesis and magnetic property of rock-salt (Co0.2Cu0.2Mg0.2Ni0.2Zn0.2)O high-entropy oxide nanocrystalline powder |
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