Development, validation of QuEChERS-based method for simultaneous determination of multiclass pesticide residue in milk, and evaluation of the matrix effect

• Published in: Journal of environmental science and health. Part B, Pesticides, food contaminants, and agricultural wastes Vol. 54; no. 5; pp. 394 - 406
• Main Authors: Tripathy, Vandana, Sharma, Krishan Kumar, Yadav, Rajbir, Devi, Suneeta, Tayade, Amol, Sharma, Khushbu, Pandey, Priya, Singh, Gitansh, Patel, Amar Nath, Gautam, Rahul, Gupta, Ruchi, Kalra, Shobhita, Shukla, Poonam, Walia, Suresh, Shakil, Najam Akhtar
• Format: Journal Article
• Language: English
• Published: England Taylor & Francis 04.05.2019; Taylor & Francis Ltd
• Subjects: Animals; Beta decay; Chemists; Chromatography; Chromatography, Gas - methods; dispersive solid-phase extraction; Electron capture; Electron capture detectors; Food Analysis - methods; Food Contamination - analysis; Gas chromatography; Gas Chromatography-Mass Spectrometry - methods; GC-ECD; Limit of Detection; Milk; Milk - chemistry; Multiclass pesticide residues; Organic chemistry; Pesticide residues; Pesticide Residues - analysis; Pesticides; Quantitation; QuEChERS; Recovery; Reproducibility; Reproducibility of Results; Sensitivity and Specificity; Sorbents; Temperature; GC-ECD; milk; dispersive solid-phase extraction; Multiclass pesticide residues; QuEChERS

Extraction and quantification of pesticide residue from the milk matrix at or below the established maximum residue limit (MRL) is a challenging task for both analytical chemists and the regulatory institutions to take corrective actions for the human health and safety. The main aim of the study is...