Low temperature selective catalytic reduction of nitric oxide with urea over activated carbon supported metal oxide catalysts

Selective catalytic reduction of nitrogen oxides (SCR) with loaded urea is a method for removing NO under oxygen-rich and low-temperature conditions, which can solve the inhibitory effect of oxygen on the catalyst and the slip of ammonia. In present study, a series of activated carbon (wo-AC, co-AC,...

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Published in	Environmental technology Vol. 41; no. 7; pp. 808 - 821
Main Authors	Liu, Kaijie, Yu, Qingbo, Wang, Baolan, Qin, Qin, Wei, Mengqi, Fu, Qi
Format	Journal Article
Language	English
Published	England Taylor & Francis 20.03.2020 Taylor & Francis Ltd
Subjects	Activated carbon Ammonia Carbon Catalysis catalyst Catalysts Catalytic activity Catalytic converters Charcoal Conversion Copper Gases Hydroxyl groups Iron Low temperature Manganese metal oxide Metal oxides Nitric Oxide Nitrogen oxides Oxidation-Reduction Oxides Oxygen oxygen-rich Photochemicals Selective catalytic reduction Temperature Urea X ray photoelectron spectroscopy Zinc low-temperature oxygen-rich Selective catalytic reduction catalyst metal oxide
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Abstract	Selective catalytic reduction of nitrogen oxides (SCR) with loaded urea is a method for removing NO under oxygen-rich and low-temperature conditions, which can solve the inhibitory effect of oxygen on the catalyst and the slip of ammonia. In present study, a series of activated carbon (wo-AC, co-AC, cs-AC and nu-AC) supported metal (Mn, Fe, Co, Cu and Zn) oxide catalysts with loading urea were prepared by ultrasonic assisted impregnation. The catalysts were used for NO removal at 50-120°C and characterized by XRD, SEM, GFAAS, EDS, XPS, BET and FTIR techniques. The effects of activated carbon type, loaded active element, metal oxides loading, temperature fluctuation on catalytic activity and the catalytic stability were also studied in this paper. The results indicated that nutshell-based activated carbon was more suitable as a carrier than other activated carbons, and urea-10Mn/nu-AC catalyst yielded a higher NO conversion than other catalysts. Besides, for used activated carbons, the larger specific surface area, more micropores distribution and the larger number of hydroxyl group and cyano terminal group are beneficial to the catalytic process. Moreover, the downward trend of NO conversion with increasing temperature suggested the adsorption of reactant gases played a crucial role in the catalytic process of urea-SCR.
AbstractList	Selective catalytic reduction of nitrogen oxides (SCR) with loaded urea is a method for removing NO under oxygen-rich and low-temperature conditions, which can solve the inhibitory effect of oxygen on the catalyst and the slip of ammonia. In present study, a series of activated carbon (wo-AC, co-AC, cs-AC and nu-AC) supported metal (Mn, Fe, Co, Cu and Zn) oxide catalysts with loading urea were prepared by ultrasonic assisted impregnation. The catalysts were used for NO removal at 50-120°C and characterized by XRD, SEM, GFAAS, EDS, XPS, BET and FTIR techniques. The effects of activated carbon type, loaded active element, metal oxides loading, temperature fluctuation on catalytic activity and the catalytic stability were also studied in this paper. The results indicated that nutshell-based activated carbon was more suitable as a carrier than other activated carbons, and urea-10Mn/nu-AC catalyst yielded a higher NO conversion than other catalysts. Besides, for used activated carbons, the larger specific surface area, more micropores distribution and the larger number of hydroxyl group and cyano terminal group are beneficial to the catalytic process. Moreover, the downward trend of NO conversion with increasing temperature suggested the adsorption of reactant gases played a crucial role in the catalytic process of urea-SCR. Selective catalytic reduction of nitrogen oxides (SCR) with loaded urea is a method for removing NO under oxygen-rich and low-temperature conditions, which can solve the inhibitory effect of oxygen on the catalyst and the slip of ammonia. In present study, a series of activated carbon (wo-AC, co-AC, cs-AC and nu-AC) supported metal (Mn, Fe, Co, Cu and Zn) oxide catalysts with loading urea were prepared by ultrasonic assisted impregnation. The catalysts were used for NO removal at 50-120°C and characterized by XRD, SEM, GFAAS, EDS, XPS, BET and FTIR techniques. The effects of activated carbon type, loaded active element, metal oxides loading, temperature fluctuation on catalytic activity and the catalytic stability were also studied in this paper. The results indicated that nutshell-based activated carbon was more suitable as a carrier than other activated carbons, and urea-10Mn/nu-AC catalyst yielded a higher NO conversion than other catalysts. Besides, for used activated carbons, the larger specific surface area, more micropores distribution and the larger number of hydroxyl group and cyano terminal group are beneficial to the catalytic process. Moreover, the downward trend of NO conversion with increasing temperature suggested the adsorption of reactant gases played a crucial role in the catalytic process of urea-SCR.Selective catalytic reduction of nitrogen oxides (SCR) with loaded urea is a method for removing NO under oxygen-rich and low-temperature conditions, which can solve the inhibitory effect of oxygen on the catalyst and the slip of ammonia. In present study, a series of activated carbon (wo-AC, co-AC, cs-AC and nu-AC) supported metal (Mn, Fe, Co, Cu and Zn) oxide catalysts with loading urea were prepared by ultrasonic assisted impregnation. The catalysts were used for NO removal at 50-120°C and characterized by XRD, SEM, GFAAS, EDS, XPS, BET and FTIR techniques. The effects of activated carbon type, loaded active element, metal oxides loading, temperature fluctuation on catalytic activity and the catalytic stability were also studied in this paper. The results indicated that nutshell-based activated carbon was more suitable as a carrier than other activated carbons, and urea-10Mn/nu-AC catalyst yielded a higher NO conversion than other catalysts. Besides, for used activated carbons, the larger specific surface area, more micropores distribution and the larger number of hydroxyl group and cyano terminal group are beneficial to the catalytic process. Moreover, the downward trend of NO conversion with increasing temperature suggested the adsorption of reactant gases played a crucial role in the catalytic process of urea-SCR.
Author	Qin, Qin Yu, Qingbo Fu, Qi Wang, Baolan Liu, Kaijie Wei, Mengqi
Author_xml	– sequence: 1 givenname: Kaijie surname: Liu fullname: Liu, Kaijie organization: State Environmental Protection Key Laboratory of Eco-Industry, School of Metallurgy, Northeastern University – sequence: 2 givenname: Qingbo surname: Yu fullname: Yu, Qingbo email: yuqb@smm.neu.edu.cn organization: State Environmental Protection Key Laboratory of Eco-Industry, School of Metallurgy, Northeastern University – sequence: 3 givenname: Baolan surname: Wang fullname: Wang, Baolan organization: State Environmental Protection Key Laboratory of Eco-Industry, School of Metallurgy, Northeastern University – sequence: 4 givenname: Qin surname: Qin fullname: Qin, Qin organization: State Environmental Protection Key Laboratory of Eco-Industry, School of Metallurgy, Northeastern University – sequence: 5 givenname: Mengqi surname: Wei fullname: Wei, Mengqi organization: State Environmental Protection Key Laboratory of Eco-Industry, School of Metallurgy, Northeastern University – sequence: 6 givenname: Qi surname: Fu fullname: Fu, Qi organization: State Environmental Protection Key Laboratory of Eco-Industry, School of Metallurgy, Northeastern University
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Snippet	Selective catalytic reduction of nitrogen oxides (SCR) with loaded urea is a method for removing NO under oxygen-rich and low-temperature conditions, which can...
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SubjectTerms	Activated carbon Ammonia Carbon Catalysis catalyst Catalysts Catalytic activity Catalytic converters Charcoal Conversion Copper Gases Hydroxyl groups Iron Low temperature Manganese metal oxide Metal oxides Nitric Oxide Nitrogen oxides Oxidation-Reduction Oxides Oxygen oxygen-rich Photochemicals Selective catalytic reduction Temperature Urea X ray photoelectron spectroscopy Zinc
Title	Low temperature selective catalytic reduction of nitric oxide with urea over activated carbon supported metal oxide catalysts
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