Synthesis of Iron Oxide Yellow from Spent Pickling Solutions
This paper demonstrates a simple environment-friendly synthesis route of iron oxide yellow (α-FeOOH) using spent pickling solutions as raw material. After abundant laboratory experiments, we finally pinned down the best procedure. The research showed that α-FeOOH nanometer material with average diam...
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Published in | MATEC Web of Conferences Vol. 67; p. 6091 |
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Main Authors | , , , |
Format | Journal Article Conference Proceeding |
Language | English |
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Abstract | This paper demonstrates a simple environment-friendly synthesis route of iron oxide yellow (α-FeOOH) using spent pickling solutions as raw material. After abundant laboratory experiments, we finally pinned down the best procedure. The research showed that α-FeOOH nanometer material with average diameter of 50nm and average length of 400 nm was prepared at the optimal technique. And the FeOOH content of the sample was as high as 90%, which is higher than the 86% of GB/T1863-2008. The structure, morphology and size distribution of the product was characterized by X-ray diffraction (XRD), Transmission electron microscope (TEM), Scanning electron microscope (SEM) and Malvern lazer particle analyzer, respectively. The test results show that all the indices of as-prepared iron oxide yellow are completely in conformity with and even better than national primes standard. |
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AbstractList | This paper demonstrates a simple environment-friendly synthesis route of iron oxide yellow (α-FeOOH) using spent pickling solutions as raw material. After abundant laboratory experiments, we finally pinned down the best procedure. The research showed that α-FeOOH nanometer material with average diameter of 50nm and average length of 400 nm was prepared at the optimal technique. And the FeOOH content of the sample was as high as 90%, which is higher than the 86% of GB/T1863-2008. The structure, morphology and size distribution of the product was characterized by X-ray diffraction (XRD), Transmission electron microscope (TEM), Scanning electron microscope (SEM) and Malvern lazer particle analyzer, respectively. The test results show that all the indices of as-prepared iron oxide yellow are completely in conformity with and even better than national primes standard. |
Author | Wan, Guangqin Lv, Feifei Yang, Yaqiang Wang, Xingyao |
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Cites_doi | 10.1016/j.hydromet.2010.01.003 10.1016/j.resconrec.2011.11.010 10.1016/j.powtec.2013.04.034 10.1016/j.matlet.2013.04.004 10.1016/j.materresbull.2006.04.030 10.1016/j.matlet.2005.12.053 10.1080/00986440500192238 10.1016/S0304-386X(96)00066-7 10.1063/1.4849273 10.1016/j.psep.2010.11.005 10.1016/j.jallcom.2005.09.043 10.1021/ja01107a510 10.1016/j.matlet.2004.10.066 10.1149/1.2424416 10.1016/j.ceramint.2014.06.051 10.1021/jp909072m 10.1016/j.hydromet.2006.03.058 10.1007/s11051-008-9467-z 10.1016/0921-3449(94)90047-7 10.1016/j.jece.2013.05.007 10.1016/S0167-577X(01)00546-8 |
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SubjectTerms | Electron microscopes Iron oxides Morphology Particle size distribution Pickling Synthesis X-ray diffraction |
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Title | Synthesis of Iron Oxide Yellow from Spent Pickling Solutions |
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