Determination of carbofuran in pesticide formulations by flow injection spectrophotometry

A flow injection spectrophotometric method for the determination of carbofuran in commercial pesticide formulations was developed. The determination involves on‐line hydrolysis of the extracted carbofuran at room temperature with sodium hydroxide. The resulting carbofuran‐phenol is coupled with diaz...

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Published in	Pest management science Vol. 56; no. 9; pp. 804 - 808
Main Authors	Zanella, Renato, Dallago, Rogério M, Preste, Cristiane V
Format	Journal Article
Language	English
Published	Chichester, UK John Wiley & Sons, Ltd 01.09.2000 Wiley London :John Wiley & Sons Ltd
Subjects	analysis Biological and medical sciences carbofuran Chemical control Control flow injection spectrophotometry formulations Fundamental and applied biological sciences. Psychology Phytopathology. Animal pests. Plant and forest protection Protozoa. Invertebrates Nematicide Carbofuran Insecticide Analysis method Formulation Detection limit Pesticides Benzofuran derivatives Pesticide formulation mixture Spectrophotometry Carbamate Flow injection
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Abstract	A flow injection spectrophotometric method for the determination of carbofuran in commercial pesticide formulations was developed. The determination involves on‐line hydrolysis of the extracted carbofuran at room temperature with sodium hydroxide. The resulting carbofuran‐phenol is coupled with diazotized 4‐aminobenzoic acid in order to achieve an appropriate selectivity and sensitivity for the spectrophotometric measurements. The calibration curve is linear over the range 1–10 mg litre−1 of carbofuran. The proposed method has a detection limit of 0.15 mg litre−1 of carbofuran and a sample frequency of 120 injections per hour. The relative standard deviation of six independent determinations of a sample containing 1 mg litre−1 carbofuran was 0.6%. The suitability of the proposed procedure for the determination of carbofuran in commercial pesticide formulations was studied. The procedure provides results comparable to those obtained by liquid chromatographic analysis. © 2000 Society of Chemical Industry
AbstractList	A flow injection spectrophotometric method for the determination of carbofuran in commercial pesticide formulations was developed. The determination involves on‐line hydrolysis of the extracted carbofuran at room temperature with sodium hydroxide. The resulting carbofuran‐phenol is coupled with diazotized 4‐aminobenzoic acid in order to achieve an appropriate selectivity and sensitivity for the spectrophotometric measurements. The calibration curve is linear over the range 1–10 mg litre−1 of carbofuran. The proposed method has a detection limit of 0.15 mg litre−1 of carbofuran and a sample frequency of 120 injections per hour. The relative standard deviation of six independent determinations of a sample containing 1 mg litre−1 carbofuran was 0.6%. The suitability of the proposed procedure for the determination of carbofuran in commercial pesticide formulations was studied. The procedure provides results comparable to those obtained by liquid chromatographic analysis. © 2000 Society of Chemical Industry
Author	Zanella, Renato Preste, Cristiane V Dallago, Rogério M
Author_xml	– sequence: 1 givenname: Renato surname: Zanella fullname: Zanella, Renato organization: Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria - RS, Brazil – sequence: 2 givenname: Rogério M surname: Dallago fullname: Dallago, Rogério M organization: Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria - RS, Brazil – sequence: 3 givenname: Cristiane V surname: Preste fullname: Preste, Cristiane V organization: Departamento de Química, Universidade Federal de Santa Maria, CEP 97105-900 Santa Maria - RS, Brazil
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Keywords	Nematicide Carbofuran Insecticide Analysis method Formulation Detection limit Pesticides Benzofuran derivatives Pesticide formulation mixture Spectrophotometry Carbamate Flow injection
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Snippet	A flow injection spectrophotometric method for the determination of carbofuran in commercial pesticide formulations was developed. The determination involves...
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SubjectTerms	analysis Biological and medical sciences carbofuran Chemical control Control flow injection spectrophotometry formulations Fundamental and applied biological sciences. Psychology Phytopathology. Animal pests. Plant and forest protection Protozoa. Invertebrates
Title	Determination of carbofuran in pesticide formulations by flow injection spectrophotometry
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