Facile construction of flower-like bismuth oxybromide/bismuth oxide formate p-n heterojunctions with significantly enhanced photocatalytic performance under visible light

[Display omitted] Visible-light harvesting ability and charge separation efficiency are two pivotal factors for the design and construction of photocatalysts with an efficient ability for degrading toxic pollutants. Herein, visible-light-driven (VLD) BiOBr/BiOCOOH p-n heterojunction photocatalysts w...

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Published inJournal of colloid and interface science Vol. 548; pp. 12 - 19
Main Authors Li, Shijie, Chen, Jialin, Jiang, Wei, Liu, Yanping, Ge, Yaming, Liu, Jianshe
Format Journal Article
LanguageEnglish
Published United States Elsevier Inc 15.07.2019
Subjects
Anion exchange
BiOBr/BiOCOOH
p-n Heterojunction
Photocatalysis
Visible light
Anion exchange
Visible light
Photocatalysis
BiOBr/BiOCOOH
p-n Heterojunction
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Abstract [Display omitted] Visible-light harvesting ability and charge separation efficiency are two pivotal factors for the design and construction of photocatalysts with an efficient ability for degrading toxic pollutants. Herein, visible-light-driven (VLD) BiOBr/BiOCOOH p-n heterojunction photocatalysts were prepared via an in-situ anion-exchange route. Through controlling the addition of KBr, we synthesized a series of BiOBr/BiOCOOH p-n heterojunctions with a different BiOBr loading. During the process, BiOBr production and homogeneous deposition on BiOCOOH with close interfacial interactions were realized by employing BiOCOOH microspheres as the self-sacrificing template. Compared to bare BiOBr and BiOCOOH, such p-n heterojunctions displayed dramatically strengthened performance in decomposing the industrial dye (rhodamine B, RhB) and antibiotic (tetracycline chloride, TC) under the irradiation of visible light. Among them, BiOBr/BiOCOOH p-n heterojunction with a BiOBr/BiOCOOH theoretical molar ratio of 0.6/0.4 (0.6Br-Bi) achieved the highest performance. Moreover, 0.6Br-Bi showed a good durability, indicating BiOBr/BiOCOOH p-n heterojunction possessed an excellently stable photocatalytic activity. Such an efficient and stable photocatalytic performance was mainly due to the formation of p-n heterojunctions which can profoundly improve the visible-light absorption and significantly depress the recombination of charge carriers. Trapping experiments and ESR tests verified that superoxide free radicals (O2−) and photogenerated hole (h+) played a significant role in RhB degradation. This research affords a promising p-n heterojunction catalyst for wastewater treatment.
AbstractList Visible-light harvesting ability and charge separation efficiency are two pivotal factors for the design and construction of photocatalysts with an efficient ability for degrading toxic pollutants. Herein, visible-light-driven (VLD) BiOBr/BiOCOOH p-n heterojunction photocatalysts were prepared via an in-situ anion-exchange route. Through controlling the addition of KBr, we synthesized a series of BiOBr/BiOCOOH p-n heterojunctions with a different BiOBr loading. During the process, BiOBr production and homogeneous deposition on BiOCOOH with close interfacial interactions were realized by employing BiOCOOH microspheres as the self-sacrificing template. Compared to bare BiOBr and BiOCOOH, such p-n heterojunctions displayed dramatically strengthened performance in decomposing the industrial dye (rhodamine B, RhB) and antibiotic (tetracycline chloride, TC) under the irradiation of visible light. Among them, BiOBr/BiOCOOH p-n heterojunction with a BiOBr/BiOCOOH theoretical molar ratio of 0.6/0.4 (0.6Br-Bi) achieved the highest performance. Moreover, 0.6Br-Bi showed a good durability, indicating BiOBr/BiOCOOH p-n heterojunction possessed an excellently stable photocatalytic activity. Such an efficient and stable photocatalytic performance was mainly due to the formation of p-n heterojunctions which can profoundly improve the visible-light absorption and significantly depress the recombination of charge carriers. Trapping experiments and ESR tests verified that superoxide free radicals (O ) and photogenerated hole (h ) played a significant role in RhB degradation. This research affords a promising p-n heterojunction catalyst for wastewater treatment.
Visible-light harvesting ability and charge separation efficiency are two pivotal factors for the design and construction of photocatalysts with an efficient ability for degrading toxic pollutants. Herein, visible-light-driven (VLD) BiOBr/BiOCOOH p-n heterojunction photocatalysts were prepared via an in-situ anion-exchange route. Through controlling the addition of KBr, we synthesized a series of BiOBr/BiOCOOH p-n heterojunctions with a different BiOBr loading. During the process, BiOBr production and homogeneous deposition on BiOCOOH with close interfacial interactions were realized by employing BiOCOOH microspheres as the self-sacrificing template. Compared to bare BiOBr and BiOCOOH, such p-n heterojunctions displayed dramatically strengthened performance in decomposing the industrial dye (rhodamine B, RhB) and antibiotic (tetracycline chloride, TC) under the irradiation of visible light. Among them, BiOBr/BiOCOOH p-n heterojunction with a BiOBr/BiOCOOH theoretical molar ratio of 0.6/0.4 (0.6Br-Bi) achieved the highest performance. Moreover, 0.6Br-Bi showed a good durability, indicating BiOBr/BiOCOOH p-n heterojunction possessed an excellently stable photocatalytic activity. Such an efficient and stable photocatalytic performance was mainly due to the formation of p-n heterojunctions which can profoundly improve the visible-light absorption and significantly depress the recombination of charge carriers. Trapping experiments and ESR tests verified that superoxide free radicals (O2-) and photogenerated hole (h+) played a significant role in RhB degradation. This research affords a promising p-n heterojunction catalyst for wastewater treatment.
[Display omitted] Visible-light harvesting ability and charge separation efficiency are two pivotal factors for the design and construction of photocatalysts with an efficient ability for degrading toxic pollutants. Herein, visible-light-driven (VLD) BiOBr/BiOCOOH p-n heterojunction photocatalysts were prepared via an in-situ anion-exchange route. Through controlling the addition of KBr, we synthesized a series of BiOBr/BiOCOOH p-n heterojunctions with a different BiOBr loading. During the process, BiOBr production and homogeneous deposition on BiOCOOH with close interfacial interactions were realized by employing BiOCOOH microspheres as the self-sacrificing template. Compared to bare BiOBr and BiOCOOH, such p-n heterojunctions displayed dramatically strengthened performance in decomposing the industrial dye (rhodamine B, RhB) and antibiotic (tetracycline chloride, TC) under the irradiation of visible light. Among them, BiOBr/BiOCOOH p-n heterojunction with a BiOBr/BiOCOOH theoretical molar ratio of 0.6/0.4 (0.6Br-Bi) achieved the highest performance. Moreover, 0.6Br-Bi showed a good durability, indicating BiOBr/BiOCOOH p-n heterojunction possessed an excellently stable photocatalytic activity. Such an efficient and stable photocatalytic performance was mainly due to the formation of p-n heterojunctions which can profoundly improve the visible-light absorption and significantly depress the recombination of charge carriers. Trapping experiments and ESR tests verified that superoxide free radicals (O2−) and photogenerated hole (h+) played a significant role in RhB degradation. This research affords a promising p-n heterojunction catalyst for wastewater treatment.
Author Liu, Jianshe
Liu, Yanping
Li, Shijie
Ge, Yaming
Jiang, Wei
Chen, Jialin
Author_xml – sequence: 1
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  surname: Li
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– sequence: 2
  givenname: Jialin
  surname: Chen
  fullname: Chen, Jialin
  organization: Key Laboratory of Key Technical Factors in Zhejiang Seafood Health Hazards, Institute of Innovation & Application, Zhejiang Ocean University, Zhoushan, Zhejiang Province 316022, China
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  givenname: Wei
  surname: Jiang
  fullname: Jiang, Wei
  email: jiangwei_zjou@163.com
  organization: Key Laboratory of Key Technical Factors in Zhejiang Seafood Health Hazards, Institute of Innovation & Application, Zhejiang Ocean University, Zhoushan, Zhejiang Province 316022, China
– sequence: 4
  givenname: Yanping
  surname: Liu
  fullname: Liu, Yanping
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  fullname: Ge, Yaming
  email: geyaming@126.com
  organization: Key Laboratory of Key Technical Factors in Zhejiang Seafood Health Hazards, Institute of Innovation & Application, Zhejiang Ocean University, Zhoushan, Zhejiang Province 316022, China
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  givenname: Jianshe
  surname: Liu
  fullname: Liu, Jianshe
  organization: State Environmental Protection Engineering Center for Pollution Treatment and Control in Textile Industry, College of Environmental Science and Engineering, Donghua University, Shanghai 201620, China
BackLink https://www.ncbi.nlm.nih.gov/pubmed/30978591$$D View this record in MEDLINE/PubMed
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Keywords Anion exchange
Visible light
Photocatalysis
BiOBr/BiOCOOH
p-n Heterojunction
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Snippet [Display omitted] Visible-light harvesting ability and charge separation efficiency are two pivotal factors for the design and construction of photocatalysts...
Visible-light harvesting ability and charge separation efficiency are two pivotal factors for the design and construction of photocatalysts with an efficient...
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SubjectTerms Anion exchange
BiOBr/BiOCOOH
p-n Heterojunction
Photocatalysis
Visible light
Title Facile construction of flower-like bismuth oxybromide/bismuth oxide formate p-n heterojunctions with significantly enhanced photocatalytic performance under visible light
URI https://dx.doi.org/10.1016/j.jcis.2019.04.024
https://www.ncbi.nlm.nih.gov/pubmed/30978591
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