Quantification of sex pheromone from Anocentor nitens by gas chromatography–mass spectrometry–selected ion monitoring
Two highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC–MS) in the selected ion monitoring (SIM) mode have been developed for the quantification of 2,6-dichlorophenol (2,6-DCP), a sex pheromone of the tick females of Anocentor nitens. Standard addition...
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Published in | Talanta (Oxford) Vol. 62; no. 3; pp. 637 - 641 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
Amsterdam
Elsevier B.V
27.02.2004
Oxford Elsevier |
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Abstract | Two highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC–MS) in the selected ion monitoring (SIM) mode have been developed for the quantification of 2,6-dichlorophenol (2,6-DCP), a sex pheromone of the tick females of
Anocentor nitens. Standard addition method and calibration curve techniques using 5-bromine-4-hydroxy-3-methoxybenzaldehyde (5-BrV) as internal standard (IS) afforded detection limit of 0.1
ng
ml
−1. The calibration curve was linear over the concentration range from 0.5 to 500
ng
ml
−1 for 2,6-DCP. Results show that the concentration range of sex pheromone in the extracts samples was 1.08–10.35
ng
ml
−1. The methods developed provided reliable procedures to determine amounts of 2,6-DCP present in ticks. |
---|---|
AbstractList | Two highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC-MS) in the selected ion monitoring (SIM) mode have been developed for the quantification of 2,6-dichlorophenol (2,6-DCP), a sex pheromone of the tick females of Anocentor nitens. Standard addition method and calibration curve techniques using 5-bromine-4-hydroxy-3-methoxybenzaldehyde (5-BrV) as internal standard (IS) afforded detection limit of 0.1ngml(-1). The calibration curve was linear over the concentration range from 0.5 to 500ngml(-1) for 2,6-DCP. Results show that the concentration range of sex pheromone in the extracts samples was 1.08-10.35ngml(-1). The methods developed provided reliable procedures to determine amounts of 2,6-DCP present in ticks. Two highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC–MS) in the selected ion monitoring (SIM) mode have been developed for the quantification of 2,6-dichlorophenol (2,6-DCP), a sex pheromone of the tick females of Anocentor nitens. Standard addition method and calibration curve techniques using 5-bromine-4-hydroxy-3-methoxybenzaldehyde (5-BrV) as internal standard (IS) afforded detection limit of 0.1 ng ml −1. The calibration curve was linear over the concentration range from 0.5 to 500 ng ml −1 for 2,6-DCP. Results show that the concentration range of sex pheromone in the extracts samples was 1.08–10.35 ng ml −1. The methods developed provided reliable procedures to determine amounts of 2,6-DCP present in ticks. |
Author | Rodrigues, Clenilson M Borges, Lı́gia M.F Ferri, Pedro H Faria, Lourival C |
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Keywords | Anocentor nitens GC–MS–SIM 2,6-Dichlorophenol Parasitiformes Standard addition method Sex pheromone GC-MS-SIM Gas chromatography Arachnida Sample preparation Acari Ixodida Arthropoda Detection limit Standard curve Invertebrata Mass spectrometry Ixodidae Monitoring Quantitative analysis |
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Snippet | Two highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC–MS) in the selected ion monitoring (SIM) mode have been... Two highly sensitive and selective methods based on gas chromatography coupled to mass spectrometry (GC-MS) in the selected ion monitoring (SIM) mode have been... |
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SubjectTerms | 2,6-Dichlorophenol Analytical chemistry Anocentor nitens Chemistry Chromatographic methods and physical methods associated with chromatography Exact sciences and technology Gas chromatographic methods GC–MS–SIM Spectrometric and optical methods |
Title | Quantification of sex pheromone from Anocentor nitens by gas chromatography–mass spectrometry–selected ion monitoring |
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