A Facile Microwave Avenue to Electrochemiluminescent Two-Color Graphene Quantum Dots
With the assistance of microwave irradiation, greenish‐yellow luminescent graphene quantum dots (gGQDs) with a quantum yield (QY) up to 11.7% are successfully prepared via cleaving graphene oxide (GO) under acid conditions. The cleaving and reduction processes are accomplished simultaneously using m...
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| Published in | Advanced functional materials Vol. 22; no. 14; pp. 2971 - 2979 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
24.07.2012
WILEY‐VCH Verlag |
| Subjects | |
| Online Access | Get full text |
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| Abstract | With the assistance of microwave irradiation, greenish‐yellow luminescent graphene quantum dots (gGQDs) with a quantum yield (QY) up to 11.7% are successfully prepared via cleaving graphene oxide (GO) under acid conditions. The cleaving and reduction processes are accomplished simultaneously using microwave treatment without additional reducing agent. When the gGQDs are further reduced with NaBH4, bright blue luminescent graphene quantum dots (bGQDs) are obtained with a QY as high as 22.9%. Both GQDs show well‐known excitation‐dependent PL behavior, which could be ascribed to the transition from the lowest unoccupied molecular orbital (LUMO) to the highest occupied molecular orbital (HOMO) with a carbene‐like triplet ground state. Electrochemiluminescence (ECL) is observed from the graphene quantum dots for the first time, suggesting promising applications in ECL biosensing and imaging. The ECL mechanism is investigated in detail. Furthermore, a novel sensor for Cd2+ is proposed based on Cd2+ induced ECL quenching with cysteine (Cys) as the masking agent.
Two‐color graphene quantum dots are prepared using a facile microwave‐assisted approach to have fluorescent quantum yields as high as 22.9%. The graphene quantum dots are demonstrated to be electrochemiluminescent. A novel electrochemiluminescence sensor for Cd2+ is proposed based on the competitive coordination between cysteine and graphene quantum dots for metal ions. |
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| AbstractList | With the assistance of microwave irradiation, greenish‐yellow luminescent graphene quantum dots (gGQDs) with a quantum yield (QY) up to 11.7% are successfully prepared via cleaving graphene oxide (GO) under acid conditions. The cleaving and reduction processes are accomplished simultaneously using microwave treatment without additional reducing agent. When the gGQDs are further reduced with NaBH
4
, bright blue luminescent graphene quantum dots (bGQDs) are obtained with a QY as high as 22.9%. Both GQDs show well‐known excitation‐dependent PL behavior, which could be ascribed to the transition from the lowest unoccupied molecular orbital (LUMO) to the highest occupied molecular orbital (HOMO) with a carbene‐like triplet ground state. Electrochemiluminescence (ECL) is observed from the graphene quantum dots for the first time, suggesting promising applications in ECL biosensing and imaging. The ECL mechanism is investigated in detail. Furthermore, a novel sensor for Cd
2+
is proposed based on Cd
2+
induced ECL quenching with cysteine (Cys) as the masking agent. With the assistance of microwave irradiation, greenish‐yellow luminescent graphene quantum dots (gGQDs) with a quantum yield (QY) up to 11.7% are successfully prepared via cleaving graphene oxide (GO) under acid conditions. The cleaving and reduction processes are accomplished simultaneously using microwave treatment without additional reducing agent. When the gGQDs are further reduced with NaBH4, bright blue luminescent graphene quantum dots (bGQDs) are obtained with a QY as high as 22.9%. Both GQDs show well‐known excitation‐dependent PL behavior, which could be ascribed to the transition from the lowest unoccupied molecular orbital (LUMO) to the highest occupied molecular orbital (HOMO) with a carbene‐like triplet ground state. Electrochemiluminescence (ECL) is observed from the graphene quantum dots for the first time, suggesting promising applications in ECL biosensing and imaging. The ECL mechanism is investigated in detail. Furthermore, a novel sensor for Cd2+ is proposed based on Cd2+ induced ECL quenching with cysteine (Cys) as the masking agent. Two‐color graphene quantum dots are prepared using a facile microwave‐assisted approach to have fluorescent quantum yields as high as 22.9%. The graphene quantum dots are demonstrated to be electrochemiluminescent. A novel electrochemiluminescence sensor for Cd2+ is proposed based on the competitive coordination between cysteine and graphene quantum dots for metal ions. |
| Author | Wang, Chong-Zhi Lu, Qian Li, Ling-Ling Jiang, Li-Ping Zhang, Jian-Rong Ji, Jing Zhu, Jun-Jie Fei, Rong |
| Author_xml | – sequence: 1 givenname: Ling-Ling surname: Li fullname: Li, Ling-Ling organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China – sequence: 2 givenname: Jing surname: Ji fullname: Ji, Jing organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China – sequence: 3 givenname: Rong surname: Fei fullname: Fei, Rong organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China – sequence: 4 givenname: Chong-Zhi surname: Wang fullname: Wang, Chong-Zhi organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China – sequence: 5 givenname: Qian surname: Lu fullname: Lu, Qian organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China – sequence: 6 givenname: Jian-Rong surname: Zhang fullname: Zhang, Jian-Rong organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China – sequence: 7 givenname: Li-Ping surname: Jiang fullname: Jiang, Li-Ping email: Jianglp@nju.edu.cn organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China – sequence: 8 givenname: Jun-Jie surname: Zhu fullname: Zhu, Jun-Jie email: jjzhu@nju.edu.cn organization: State Key Laboratory of Analytical Chemistry for Life Science, School of Chemistry and Chemical Engineering, Nanjing University Nanjing, 210093, P. R. China |
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| ContentType | Journal Article |
| Copyright | Copyright © 2012 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim |
| Copyright_xml | – notice: Copyright © 2012 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim |
| DBID | BSCLL AAYXX CITATION |
| DOI | 10.1002/adfm.201200166 |
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| Snippet | With the assistance of microwave irradiation, greenish‐yellow luminescent graphene quantum dots (gGQDs) with a quantum yield (QY) up to 11.7% are successfully... |
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| Title | A Facile Microwave Avenue to Electrochemiluminescent Two-Color Graphene Quantum Dots |
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